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DOE OSTI2022

Generic National Nuclear Forensics Library Implementation

This document provides instructions for the database implementation for national nuclear forensic library (NNFL) using a relational database. While there are many software options that can be used to implement an NNFL database, in this document we reference an Oracle database for the implementation. The principles related here can be applied to any relational database structure. The design revolves around two main types of data: Samples and Results. Samples are materials or descriptions of materials; results are the results of analyses of those samples. All additional tables exist as a result of the normalization process. The remaining tables/entities have keys that are referenced by the Result/Sample tables via foreign key constraints. This allows for the enforcement of different relationships between the tables such as one-to-one, one-to-many, many-to-many. This process helps to ensure that valid data is entered, optimizes database performance and avoids data redundancies.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRS1973

Elemental abundances of Apollo 16 samples

Results are presented for the multielement analysis of samples of lunar soil (60501 and 64501), igneous rock (60315), and the light portion of breccia 60017. A mixing model for soil compositions has been proposed consisting of linear combinations of the KREEP basalt 60315 and the anorthositic gabbroic sample 60017. A comparison of trace elements in lunar soils from different missions indicates the marked depletion of the LIL elements in the Apollo 16 samples.

Morrison, G. H.↗

NASA NTRS1993

Radiation and temperature effects on LDEF fiber optic samples

Results obtained from the JPL Fiber Optics Long Duration Exposure Facility (LDEF) Experiment since the June 1991 Experimenters' Workshop are addressed. Radiation darkening of laboratory control samples and the subsequent annealing was measured in the laboratory for the control samples. The long-time residual loss was compared to the LDEF flight samples and found to be in agreement. The results of laboratory temperature tests on the flight samples, extending over a period of about nine years, including the pre-flight and post-flight analysis periods, are described. The temperature response of the different cable samples varies widely, and appears in two samples to be affected by polymer aging. Conclusions to date are summarized.

Johnston, A. R.↗

NASA NTRS1976

Uranium in NIMROC standard igneous rock samples

Results are reported for analysis of the uranium in multiple samples of each of six igneous-rock standards (dunite, granite, lujavrite, norite, pyroxenite, and syenite) prepared as geochemical reference standards for elemental and isotopic compositions. Powdered rock samples were examined by measuring delayed neutron emission after irradiation with a flux of the order of 10 to the 13th power neutrons/sq cm per sec in a nuclear reactor. The measurements are shown to compare quite favorably with previous uranium determinations for other standard rock samples.

Rowe, M. W.↗

NASA NTRS1974

Igneous rocks from Apollo 16 rake samples

Results are reported for a study of seven holocrystalline feldspathic rocks (including a spinel troctolite and six melt rocks) and one mare basalt clast from the Apollo-16 rake samples. The composition and grain structure of each rock is described in detail. Only the spinel troctolite is considered a good candidate for a primary igneous cumulate formed during the original differentiation of the lunar crust. It is shown that the melt rocks probably resulted from shock melting followed by rapid crystallization of heterogeneous highland material and that compositional variations are probably due to mixing of various amounts of heterogeneous cumulates and KREEP components. It is suggested that the mare basalt clast may have been derived from Mare Fecunditatis, although the nearest mare to the Apollo-16 site is Nectaris.

Dowty, E.↗

NASA NTRS1973

Co-60 in lunar samples.

Results obtained for Co-60 in lunar soils and rocks of different depths are discussed. These results are compared to a production calculation based on the work of Lingenfelter et al. (1972). The measurement of Co-60 activities can give information about the present-day equilibrium neutron flux in the lunar regolith. The most important quantity which can be derived from these data is the absolute present-day lunar neutron production rate.

Wahlen, M.↗

NASA NTRS1973

Report on Skylab -M552 samples

Results of examining the M522 specimens are reported. The visual examination, location of sectioning planes, and microstructure are described. It is concluded that no specific effects of the zero gravity processing can be identified.

Source record↗

DOE OSTI2020

GADRAS Batch Inject Tool User Guide

Gamma Detector Response and Analysis Software (GADRAS) is used by the radiation detection and emergency response community to perform modeling and spectral analysis for gamma detector systems. Built into GADRAS is the ability to define a detector, geometry, background characteristics and source composition to generate synthetic spectra for drills and exercises (injects). Consequence Management is currently in development of a sample result data simulator tool in which a deposition model is probed for source conditions at moments in time and locations in space. These values are used to generate realistic sample results for use in drills and exercises. In addition to sample results, there is a need to simulate the actual spectra that would be observed in the field by downlooking HPGe instruments given a deposition activity. This way, the FRMAC Gamma Spectroscopist can practice their process of generating quantified results from spectra on realistic data as well. Recognizing the decades of work done in GADRAS to accurately generate synthetic spectra, this team decided to build a link between the new simulator and GADRAS to generate these spectra quickly and easily. The simulator tool will generate a file that specifies the name of the spectra, its location, date/time of measurement, duration of measurement, height off the ground, and the deposition activity and age for every radionuclide in the simulation. Then, a new tool within the Inject Tab of GADRAS was developed to read in this file given a detector selection and generate In-Situ spectra for each row in the file in any file format the user chooses. This way, simulation cell staff can take these files and then upload them to the appropriate data system (RAMS or RadResponder) for use during drills and exercises. An advanced feature of this tool allows for generating any spectra given an appropriate model and mapping of source to model layer in the batch inject tool. This way, spectra from field sample counts, mobile laboratories, or even fixed laboratories can be generated in bulk given an estimate of the radioactivity concentration or total radioactivity in an import file. This expands the capabilities of this tool a great deal and will make it a more useful tool for CM and others to help estimate detector response for nearly any situation. This user guide will explain the steps needed to perform a batch inject file generation.

61 RADIATION PROTECTION AND DOSIMETRY↗

NASA NTRS1974

Comparison of interference-free numerical results with sample experimental data for the AEDC wall-interference model at transonic and subsonic flow conditions

Numerical results obtained from two computer programs recently developed with NASA support and now available for use by others are compared with some sample experimental data taken on a rectangular-wing configuration in the AEDC 16-Foot Transonic Tunnel at transonic and subsonic flow conditions. This data was used in an AEDC investigation as reference data to deduce the tunnel-wall interference effects for corresponding data taken in a smaller tunnel. The comparisons were originally intended to see how well a current state-of-the-art transonic flow calculation for a simple 3-D wing agreed with data which was felt by experimentalists to be relatively interference-free. As a result of the discrepancies between the experimental data and computational results at the quoted angle of attack, it was then deduced from an approximate stress analysis that the sting had deflected appreciably. Thus, the comparisons themselves are not so meaningful, since the calculations must be repeated at the proper angle of attack. Of more importance, however, is a demonstration of the utility of currently available computational tools in the analysis and correlation of transonic experimental data.

Newman, P. A.↗

NASA NTRS2020

First Detections of Dichlorobenzene Isomers and Trichloromethylpropane from Organic Matter Indigenous to Mars Mudstone in Gale Crater, Mars: Results from the Sample Analysis at Mars Instrument Onboard the Curiosity Rover

Chromatographic analysis of the Cumberland mudstone in Gale crater by the Sample Analysis at Mars (SAM) instrument revealed the detection of two to three isomers of dichlorobenzene. Their individual concentrations were estimated to be in the 0.5–17 ppbw range relative to the sample mass. We also report the first detection of trichloromethylpropane and the confirmation of the detection of chlorobenzene previously reported. Supporting laboratory experiments excluded the SAM internal background as the source of those compounds, thus confirming the organic carbon and chlorine of the newly detected chlorohydrocarbons are indigenous to the mudstone sample. Laboratory experiments also demonstrated that the chlorohydrocarbons were mainly produced from chemical reactions occurring in the SAM ovens between organic molecules and oxychlorines contained in the sample. The results we obtained show that meteoritic organics and tested chemical species (a polycyclic aromatic hydrocarbon, an amino acid, and a carboxylic acid) were plausible organic precursors of the chlorinated aromatic molecules detected with SAM, thus suggesting that they could be among the organic molecules present in the mudstone. Results from this study coupled with previously reported detections of chlorinated aromatics (<300 ppbw) indigenous to the same mudstone highlight that organics can be preserved from the harsh surface conditions even at shallow depth. The detection of new chlorohydrocarbons with SAM confirms that organic molecules should have been available in an environment favorable to life forms, strengthening the habitability aspect of Gale crater. Key Words: Mars—Chlorinated organic molecules—In situ measurements—Sample Analysis at Mars— Mudstone—Gale crater. Astrobiology 20, 292–306.

Szopa, Cyril↗

NASA NTRS2007

Fluid Mechanics and Heat Transfer in Transitional Boundary Layers

Experiments have been performed to investigate the effects of elevated free-stream turbulence and streamwise acceleration on flow and thermal structures in transitional boundary layers. The free-stream turbulence ranges from 0.5 to 6.4% and the streamwise acceleration ranges from K = 0 to 0.8 x 10(exp -6). The onset of transition, transition length and the turbulent spot formation rate are determined. The statistical results and conditionally sampled results of th streamwise and cross-stream velocity fluctuations, temperature fluctuations, Reynolds stress and Reynolds heat fluxes are presented.

Wang, Ting↗

NASA NTRS2001

Flying the TRMM Satellite in a GCM

By incorporating the Tropical Rainfall Measurement Mission (TRMM) satellite orbital information into the Colorado State University General Circulation Model (CSU GCM), we are able to 'fly' a satellite in the GCM, and sample the simulated atmosphere in the same way as the TRMM sensors sample the real atmosphere. The TRMM-sampled statistics for precipitation and radiative fluxes at annual, intraseasonal, monthly-mean and seasonal-mean diurnal time scales are evaluated by comparing the satellite-sampled against fully-sampled simulated atmospheres. The sampling rates of the TRMM sensors are significantly affected by the sensors' swath widths. The TRMM Microwave Imager (TMI) and the Visible Infrared Scanner (VIRS) sample each 2.25 x 2.25 degree grid box in the Tropics and subtropics about once per day, but at a different local time every day, while the Precipitation Radar (PR) and the Clouds and the Earth's Radiant Energy System (CERES) sensor visit each grid box about once every three days and twice per day, respectively. Besides inadequate samplings resulting from sensors' swath widths, there is a large, systematic diurnal undersampling associated with TRMM's orbital geometry for grid boxes away from the Equator. When only one month of TRMM data are used, this diurnal undersampling can lead to more daytime samples relative to nighttime samples in one hemisphere, and more nighttime samples relative to daytime samples in the other hemisphere. The resulting sampling biases (3-6 W m(exp-2)) are very pronounced in outgoing longwave radiation (OLR) over the subtropical land masses. The sampling errors in OLR monthly- and seasonal-means are less than 8 W m(exp-2) (5%) for each 2.25 x 2.25 degree grid box. The OLR monthly- and seasonal-means are not sensitive to diurnal undersamplings associated with the TRMM orbits and sensors' swath widths. However, this is not the case for total precipitation. Diurnal undersampling could produce errors as large as 20% in the Tropics and 40% in the subtropics, for the zonally averaged monthly-mean rain rates. The TRMM orbits sample each 2.25 x 2.25 degree grid box in the Tropics and subtropics 1-6 times for each hour of the day within a single season. The seasonal-mean diurnal cycles of precipitation and OLR are not well sampled for any one grid box. By either accumulating the satellite data for a long enough period, or averaging the data over a large area with a relatively uniform diurnal signal, the diurnal cycles of precipitation and OLR can be satisfactorily sampled. The effects TRMM sampling errors on the inferred tropical-mean hydrologic cycle and radiative fluxes are also evaluated. There are strong spurious oscillations associated with TRMM's orbital geometry, with periods of 23 days and 3-4 months, in tropical-mean daily and monthly precipitation. While the relative fluctuations of the sampled-OLR are negligible, the relative fluctuations of the sampled precipitation have magnitudes similar to those of the observed climate variability. Caution must therefore be used when applying TRMM observations of tropical-mean precipitation to interpret climate variations at intraseasonal and interannual scales.

Lin, Xin↗

NASA NTRS2018

Three Proposed Compendia for Genesis Solar Wind Samples: Science Results, Collector Materials Characterization and Cleaning Techniques

Final Paper and not the abstract is attached. Introduction: Planetary material and cosmochemistry research using Genesis solar wind samples (including the development and implementation of cleaning and analytical techniques) has matured sufficiently that compilations on several topics, if made publically accessible, would be beneficial for researchers and reviewers. We propose here three compendia based on content, organization and source of documents (e.g. published peer-reviewed, published, internal memos, archives). For planning purposes, suggestions are solicited from potential users of Genesis solar wind samples for the type of science content and/or organizational style that would be most useful to them. These compendia are proposed as living documents, periodically updated. Similar to the existing compendia described below, the curation compendia are like library or archival finding aids, they are guides to published or archival documents and should not be cited as primary sources.

Allton, J. H.↗

NASA NTRS1978

The analysis of high spatial resolution UV and X-ray images by computational modeling

Very high resolution stereoscopic images of high temperature loop structures observed at UV and X-ray wavelengths in the solar corona can be used to understand physical processes in the corona. An existing computational model is described and sample results are given to demonstrate that computational modeling of coronal structures can indeed take advantage of very high resolution images. The sample results include the run of temperature and number density along a typical loop and the variation of the differential emission measure with temperature. The integration of the differential emission measure with temperature along a column commensurate with an instrument's spatial resolution is the relevant parameter obtained from UV and X-ray observations. The effects of loop geometry and energy input are examined.

Vesecky, J. F.↗

DOE OSTI2021

Exceedance Response Action (ERA) Level 1 Report and ERA Level 2 Action Plan

This report consolidates the requirements for an Exceedance Response Action (ERA) Level 1 and ERA Level 2 Action Plan for pH. A discharger’s baseline status for any given parameter changes to Level 1 status if sampling results indicate a Numeric Action Level (NAL) exceedance for that same parameter. NAL exceedance can be either of the following: (1) Instantaneous maximum NAL exceedance: Occurs when two or more analytical results for any single parameter within a reporting year exceed the instantaneous maximum NAL (for example for pH a value less than 6 or a value greater than 9); and (2) Annual NAL exceedance: Occurs when the average of all the analytical results for a parameter within a reporting year exceeds the annual NAL. A Discharger’s Level 1 status for any given parameter changes to Level 2 status if sampling results indicate a Numeric Action Level (NAL) exceedance for the same parameter while a Discharger is in Level 1.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2020

Summary of Expedited Results from Samples Supporting Tank Closure Cesium Removal (TCCR) Batch 3

Savannah River Remediation (SRR) is currently operating the Tank Closure Cesium Removal (TCCR) process to remove 137 Cs from tank waste supernate using an ion exchange process. As part of that process, Savannah River National Laboratory (SRNL) receives and analyzes samples in support of the qualification of each batch to be processed. SRNL recently received supernate samples retrieved from Tank 10H as well as in-tank batch contact samples for characterization in support of qualifying Batch 3 for processing through the TCCR unit. SRNL received and characterized a set of dip samples collected from Tank 10H (one surface and one variable depth sample). No solids were observed in either sample and therefore the samples were combined, and a suite of analyses were performed on the composite sample. The density of the combined sample was 1.174 g/mL (0.18 %RSD), which was consistent with the measured sodium concentration of 3.54 M (0.08 %RSD). The 137Cs activity in the sample was 4.75E+07 dpm/mL (4.28 %RSD) and the total Cs concentration was calculated to be 1.54 mg/L (1.16E-05 M). The in-tank batch contact samples consist of 0.1 g of crystalline silicotitanate (CST) contained within a teabag device. Duplicate samples were submerged in Tank 10H supernate for a period of about 13 days, after which time they were retrieved and transferred to SRNL for analysis. At SRNL the CST was rinsed to remove excess salt solution and the CST was then air dried before being digested for analysis. Results of the analysis indicated a 137 Cs loading of 3.66E+10 ± 1.40E+09 dpm/g or 16.5 ± 0.63 Ci/kg CST . This value represents a bounding upper limit as it includes the addition of two sigma uncertainty from replicate analysis of the individual teabag samples as well as the addition of the small amount of 137 Cs activity measured in the rinse solutions. The above values are based on the air-dried mass of CST. Correcting to the true dry mass using a F-factor of 0.8191 results in a maximum loading of 20.2 ± 0.77 Ci/kg CST .

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NASA NTRS1986

Measurements with an airborne, autotracking, external-head sunphotometer

Design and performance features and sample results from use of a NASA airborne tracking sunphotometer (ATS) are described. The ATS was devised to obtain continuous vertical profiles of the optical depth and transmissivity, first from a CV-990 aircraft and then from a modified DC-8 aircraft. Sample results are presented from a 1985 flight as part of the SAGE-II calibration mission, which featured detectors frequencies of 380, 450, 600, 860, 940, and 1020 microns and covered flight altitudes from ground to 10 km.

Russell, P. B.↗

NASA NTRS2003

The Burst and Transient Source Experiment(BATSE)Earth Occultation Catalog of Low-Energy Gamma-Ray Sources. Short title: BATSE Earth Occultation Catalog v2.0

The Burst and Transient Source Experiment (BATSE), aboard the Compton Gamma Ray Observatory (CGRO), provided a record of the low-energy gamma-ray sky (approx. 20-1000 keV) between 1991 April and 2000 May (9.1y). BATSE monitored the high energy sky using the Earth occultation technique (EOT) for point sources whose emission extended for times on the order of the CGRO orbital period (approx. 92m) or greater. Using the EOT to extract flux - 2 - information, a catalog of sources using data from the BATSE large area detectors has been prepared. The first part of the catalog consists of results from the all-sky monitoring of 58 sources, mostly Galactic, with intrinsic variability on timescales of hours to years. For these sources, we have included tables of flux and spectral data, and outburst times for transients. Light curves (or flux histories) covering the entire nine mission are being placed on the world wide web. We then performed a deep-sampling of these 58 objects, plus a selection of 121 more objects, combining data from the entire 9.ly BATSE dataset. Source types considered were primarily accreting binaries, but a small number of representative active galaxies, X-ray-emitting stars, and supernova remnants were also included. The sample represents a compilation of sources monitored and/or discovered with BATSE and other high energy instruments between 1991 and 2000, known sources taken from the HEAO 1 A-4 (Levine et al. 1984) and Macomb and Gehrels (1999) catalogs. The deep sample results include definite detections of 82 objects and possible detections of 36 additional objects. The definite detections spanned three classes of sources: accreting black hole and neutron star binaries, active galaxies and supernova remnants. The average fluxes measured for the fourth class, the X-ray emitting stars, were below the confidence limit for definite detection. Flux data for the deep sample are presented in four energy bands: 20-40, 40-70, 70-160, and 160-430 keV. The limiting average flux level (9.1 y) for the sample varies from 3.5 to 20 mCrab (5delta) between 20 and 430 keV, depending on systematic error, which in turn is primarily dependent on the sky location. To strengthen the credibility of detection of weaker sources (approx.5-25 mCrab), we generated Earth occultation images, searched for periodic behavior using FFT and epoch folding methods, and critically evaluated the energy-dependent emission in the four flux bands. The deep sample results are intended for guidance in performing future all-sky surveys or pointed observations in the hard X-ray and low-energy gamma-ray band, as well as more detailed studies with the BATSE EOT.

Harmon, B. A.↗