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At least 37 records · Page 2

Numerical and experimental investigation of the bending response of thin-walled composite cylinders

A numerical and experimental investigation of the bending behavior of six eight-ply graphite-epoxy circular cylinders is presented. Bending is induced by applying a known end-rotation to each end of the cylinders, analogous to a beam in bending. The cylinders have a nominal radius of 6 inches, a length-to-radius ratio of 2 and 5, and a radius-to-thickness ratio of approximately 160. A (+/- 45/0/90)S quasi-isotropic layup and two orthotropic layups, (+/- 45/0 sub 2)S and (+/- 45/90 sub 2)S, are studied. A geometrically nonlinear special-purpose analysis, based on Donnell's nonlinear shell equations, is developed to study the prebuckling responses and gain insight into the effects of non-ideal boundary conditions and initial geometric imperfections. A geometrically nonlinear finite element analysis is utilized to compare with the prebuckling solutions of the special-purpose analysis and to study the buckling and post buckling responses of both geometrically perfect and imperfect cylinders. The imperfect cylinder geometries are represented by an analytical approximation of the measured shape imperfections. Extensive experimental data are obtained from quasi-static tests of the cylinders using a test fixture specifically designed for the present investigation. A description of the test fixture is included. The experimental data are compared to predictions for both perfect and imperfect cylinder geometries. Prebuckling results are presented in the form of displacement and strain profiles. Buckling end-rotations, moments, and strains are reported, and predicted mode shapes are presented. Observed and predicted moment vs. end-rotation relations, deflection patterns, and strain profiles are illustrated for the post buckling responses. It is found that a geometrically nonlinear boundary layer behavior characterizes the prebuckling responses. The boundary layer behavior is sensitive to laminate orthotropy, cylinder geometry, initial geometric imperfections, applied end-rotation, and non-ideal boundary conditions. Buckling end-rotations, strains, and moments are influenced by laminate orthotropy and initial geometric imperfections. Measured buckling results correlate well with predictions for the geometrically imperfect specimens. The postbuckling analyses predict equilibrium paths with a number of scallop-shaped branches that correspond to unique deflection patterns. The observed postbuckling deflection patterns and measured strain profiles show striking similarities to the predictions in some cases. Ultimate failure of the cylinders is attributed to an interlaminar shear failure mode along the nodal lines of the postbuckling deflection patterns.

Fuchs, J. P.

Damage Tolerance of Candidate Sandwich Structure for the Space Launch System (SLS) Payload Adapter Fitting (PAF)

This Technical Memorandum presents results from a damage tolerance study undertaken in support of the payload adapter fitting (PAF) for the Space Launch System (SLS) program at NASA’s Marshall Space Flight Center (MSFC). The study consisted of determining the compression-after-impact (CAI) strength of candidate carbon/epoxy face sheet sandwich structure that has been identified for potential use to manufacture the PAF hardware. Two types of core material that have been considered for use on the PAF structure were used in this study. One was an aluminum honeycomb and the other was a Rohacell foam. Levels of barely visible impact damage (BVID) were determined for the types of sandwich structure tested in this study and this level of damage was used for CAI strength testing. It was found that the honeycomb core sandwich structure failed by face sheet failure and the foam core sandwich structure failed by core shear failure. CAI strength values were normalized by weight of the sandwich structure since lower mass is desirable for this structure.

sandwich structure

Low-velocity impact damage in graphite-fiber reinforced epoxy laminates

An experimental investigation was conducted to identify the failure mechanisms and to understand damage propagation in compression-loaded composite structures. The tests were conducted on several laminates of different ply orientation with thickness that ranged from 0.56 to 0.75 cm. The panels were damaged by 1.27-cm-diameter aluminum spheres propelled normal to the specimen surface at velocities ranging from 30 m/s to 140 m/s. Results indicate that there is significant internal laminate damage due to low-velocity impact with no surface damage. The internal damage consists of delamination and intraply cracking. Three damage propagation modes were identified as causing specimen failure; which are delamination, axial load-lateral deformation coupling, and local shear failure.

Rhodes, M. D.

Design and Characterization of Thin Stainless Steel Burst Disks for Increasing Two-Stage Light Gas Launcher Efficiency

Laser etched 300 series Stainless Steel Burst Disks (SSBD) ranging between 0.178 mm (0.007-in.) and 0.508mm (0.020-in.) thick were designed for use in a 17-caliber two-stage light gas launcher. First, a disk manufacturing method was selected using a combination of wire electrical discharge machining (EDM) to form the blank disks and laser etching to define the pedaling fracture pattern. Second, a replaceable insert was designed to go between the SSDB and the barrel. This insert reduced the stress concentration between the SSBD and the barrel, providing a place for the petals of the SSDB to open, and protecting the rifling on the inside of the barrel. Thereafter, a design of experiments was implemented to test and characterize the burst characteristics of SSBDs. Extensive hydrostatic burst testing of the SSBDs was performed to complete the design of experiments study with one-hundred and seven burst tests. The experiment simultaneously tested the effects of the following: two SSBD material states (full hard, annealed); five SSBD thicknesses 0.178, 0.254, 0.305, 0.381 mm (0.007, 0.010, 0.012, 0.015, 0.020-in.); two grain directions relative); number of times the laser etch pattern was repeated (varies between 5-200 times); two heat sink configurations (with and without heat sink); and, two barrel configurations (with and without insert). These tests resulted in the quantification of the relationship between SSBD thickness, laser etch parameters, and desired burst pressure. Of the factors investigated only thickness and number of laser etches were needed to develop a mathematical relationship predicting hydrostatic burst pressure of disks using the same barrel configuration. The fracture surfaces of two representative SSBD bursts were then investigated with a scanning electron microscope, one burst hydrostatically in a fixture and another dynamically in the launcher. The fracture analysis verified that both burst conditions resulted in a ductile overload failure indicated by transgranular microvoid coalescence, non-fragmenting rupture and mixed tensile and shear failure modes, regardless of the material states tested. More testing is underway to determine the relationship between SSBD burst pressure and projectile velocity.

Tylka, Jonathan M.

Fracture and crack growth in orthotropic laminates

Solutions are developed for the two dimensional region containing unidirectional fibers with initial damage in the form of a notch, a rectangular cut out, and a circular hole. An ultimate stress failure criterion is used for both the fibers and the matrix, simple tension for the fibers, and shear failure for the matrix. Models which account for longitudinal matrix yielding and splitting as well as transverse matrix yielding and fiber breakage as a function of initial damage, material properties, and applied stress are presented. For ductile matrix composites the results indicate that longitudinal matrix yielding and transverse notch extension are the most significant forms of damage. The extent of the stable transverse damage is shown to be approximately constant, independent of initial notch length. In the case of brittle matrix composites (graphite/epoxy) longitudinal splitting is shown to be the dominant form of damage.

Goree, J. G.

Failure of Non-Circular Composite Cylinders

In this study, a progressive failure analysis is used to investigate leakage in internally pressurized non-circular composite cylinders. This type of approach accounts for the localized loss of stiffness when material failure occurs at some location in a structure by degrading the local material elastic properties by a certain factor. The manner in which this degradation of material properties takes place depends on the failure modes, which are determined by the application of a failure criterion. The finite-element code STAGS, which has the capability to perform progressive failure analysis using different degradation schemes and failure criteria, is utilized to analyze laboratory scale, graphite-epoxy, elliptical cylinders with quasi-isotropic, circumferentially-stiff, and axially-stiff material orthotropies. The results are divided into two parts. The first part shows that leakage, which is assumed to develop if there is material failure in every layer at some axial and circumferential location within the cylinder, does not occur without failure of fibers. Moreover before fibers begin to fail, only matrix tensile failures, or matrix cracking, takes place, and at least one layer in all three cylinders studied remain uncracked, preventing the formation of a leakage path. That determination is corroborated by the use of different degradation schemes and various failure criteria. Among the degradation schemes investigated are the degradation of different engineering properties, the use of various degradation factors, the recursive or non-recursive degradation of the engineering properties, and the degradation of material properties using different computational approaches. The failure criteria used in the analysis include the noninteractive maximum stress criterion and the interactive Hashin and Tsai-Wu criteria. The second part of the results shows that leakage occurs due to a combination of matrix tensile and compressive, fiber tensile and compressive, and inplane shear failure modes in all three cylinders. Leakage develops after a relatively low amount of fiber damage, at about the same pressure for three material orthotropies, and at approximately the same location.

Hyer, M. W.

Postbuckling and failure characteristics of selected flat rectangular graphite-epoxy plates loaded in compression

Results of an experimental study of the postbuckling response and failure characteristics of 16- and 24-ply quasi-isotropic and 24-ply orthotropic flat rectangular graphite-epoxy plates loaded in compression are examined. Some of the specimens had circular drilled holes or were subjected to low-speed impact damage. The ratio of failure load to buckling load was found to be higher for specimens with lower initial buckling strains than for specimens with higher initial buckling strains. Some specimens supported more than five times their initial buckling load before failing. The specimens failed along a nodal line of the buckling mode in an induced shear failure mode. Holes and impact damage had a more adverse effect on the postbuckling strength of specimens with high initial buckling strains than on the strength of specimens with lower initial buckling strains.

Starnes, J. H., Jr.

A micrographic study of bending failure in five thermoplastic/carbon fiber composite laminates

The local deformation and failure sequences of five thermoplastic matrix composites were microscopically observed while bending the samples in a small fixture attached to a microscope stage. The themoplastics are polycarbonate, polysulfone, polyphenylsulfide, polyethersulfone, and polyetheretherketone. Comparison was made to an epoxy matrix composite, 5208/T-300. Laminates tested are (0/90) sub 2S, with outer ply fibers parallel to the beam axis. Four point bending was used at a typical span-to-thickness ratio of 39:1. It was found that all of the thermoplastic composites failed by abrupt longitudinal compression buckling of the outer ply. Very little precursory damage was observed. Micrographs reveal typical fiber kinking associated with longitudinal compression failure. Curved fracture surfaces on the fibers suggest they failed in bending rather than direct compression. Delamination was suppressed in the thermoplastic composites, and the delamination that did occur was found to be the result of compression buckling, rather than visa-versa. Microbuckling also caused other subsequent damage such as ply splitting, transverse ply shear failure, fiber tensile failure, and transverse ply cracking.

Yurgartis, S. W.

A micrographic study of bending failure in five thermoplastic-carbon fibre composite laminates

The local deformation and failure sequences of five thermoplastic matrix composites were microscopically observed while bending the samples in a small fixture attached to a microscope stage. The thermoplastics are polycarbonate, polysulfane, polyphenylsulfide, polyethersulfane, and polyetheretherketone. Comparison was made to an epoxy matrix composite, 5208/T-300. Laminates tested are (0/90) sub 2S, with outer ply fibers parallel to the beam axis. Four point bending was used at a typical span-to-thickness ratio of 39:1. It was found that all of the thermoplastic composites failed by abrupt longitudinal compression buckling of the outer ply. Very little precursory damage was observed. Micrographs reveal typical fiber kinking associated with longitudinal compression failure. Curved fracture surfaces on the fibers suggest they failed in bending rather than direct compression. Delamination was suppressed in the thermoplastic composites, and the delamination that did occur was found to be the result of compression buckling, rather than vice-versa. Microbuckling also caused other subsequent damage such as ply splitting, transverse ply shear failure, fiber tensile failure, and transverse ply cracking.

Yurgartis, S. W.

Observations, models, and mechanisms of failure of surface rocks surrounding planetary surface loads

Geophysical models of flexural stresses in an elastic lithosphere due to an axisymmetric surface load typically predict a transition with increased distance from the center of the load of radial thrust faults to strike-slip faults to concentric normal faults. These model predictions are in conflict with the absence of annular zones of strike-slip faults around prominent loads such as lunar maria, Martian volcanoes, and the Martian Tharsis rise. We suggest that this paradox arises from difficulties in relating failure criteria for brittle rocks to the stress models. Indications that model stresses are inappropriate for use in fault-type prediction include (1) tensile principal stresses larger than realistic values of rock tensile strength, and/or (2) stress differences significantly larger than those allowed by rock-strength criteria. Predictions of surface faulting that are consistent with observations can be obtained instead by using tensile and shear failure criteria, along with calculated stress differences and trajectories, with model stress states not greatly in excess of the maximum allowed by rock fracture criteria.

Schultz, R. A.

DECOVALEX-2023: Task A Final Report

Task A, also known as HGFrac, examines the fracturing processes that may occur in the Callovo-Oxfordian claystone (COx) in the context of the high-level (HLW) and intermediate-level long-lived (ILW-LL) radioactive waste repository in France. Understanding these processes and improving numerical models to reproduce them will aid in the design, optimization, and safety of the repository. Heat and gas fracturing are studied in two independent subtasks following a stepwise approach: laboratory tests/benchmark exercises, in-situ experiment, and finally, an application case. The in-situ heater experiment aimed to thermally induce a hydraulic fracture; temperature and pore pressure were monitored to detect any evidence of fracturing. The in-situ gas injection experiment aimed to study the effect of the stress orientation and gas injection kinetics on the gas fracturing process. The occurrence of fracturing was monitored by gas pressure measured in the injection interval. In both experiments, the excavation-induced fracture network around the heater/injection boreholes played an important role in the reduction of the compressive stress state, leading to both a tensile and shear failure response of the COx. During the first two years of the project, the research teams working on each task developed and/or proposed numerical approaches for reproducing the occurrence of fracturing in the in-situ experiments. The failure criteria were defined by reproducing the measurements from laboratory extension tests for the heat fracturing subtask. In the gas fracturing subtask, their approaches were used for simulating several benchmark exercises, and an inter-comparison between models was carried out. In both tasks, the developed approaches were compared with a simplified approach considering poro-elasticity for the mechanical behaviour of the COx. Most of the developed approaches are based on a continuous medium that takes into account variations in hydraulic properties due to mechanical degradation, such as plastic deformation or damage. Other approaches implicitly modelled weak planes or embedded discontinuities to reproduce fracture propagation. The potential for fracture initiation was also studied through of a discrete approach. In the second half of the project, the research teams mainly focused on interpretative modelling of two in-situ experiments and a blind prediction exercise to test their respective approaches. The models developed by the research teams were also applied at the repository scale to evaluate fracture initiation in a case study under vi unfavourable conditions, particularly in terms of spacing between High-Level Waste cells. The results showed that the poro-elasticity approach could be an efficient tool for understanding the main processes occurring in the COx. One example is the explicit representation of the excavation-induced fracture network around the boreholes, which yielded acceptable results compared to the measurement data. However, advanced approaches were needed to evaluate the potential increase of the excavation-induced fracture network extend and better understand fracture initiation. The stress analyses carried out by the teams revealed that hydraulic boundary conditions had a strong impact on fracture initiation in the heater experiment. Furthermore, in most cases, the results required higher pore pressure increments to reach fracturing than those measured in the experiment. This implies that the measurements may have been biased by the packer’s capacity to fully isolate the piezometric chambers, leading to lower pressures. On the contrary, there was no agreement on the fracturing mode, as some reported either shear or tensile fracturing, while others reported a combination of the two modes. In the case of gas fracturing, the research teams were limited to the comparison of a single point, which complicated their task. Nonetheless, the numerical results were able to reproduce the measurements and capture processes such as longitudinal gas flow through the excavation-induced fracture network, as suggested by some evidence in the observation piezometric chambers. The numerical models also agreed with the measurements in the sense of higher probability of developing along the injection borehole than radially towards the sound rock. The approaches developed by the research teams showed that they are capable of analysing and reproducing fracture initiation in the COx. However, areas of future work should focus on the fracture propagation and fracture aperture, which were out of the scope of this task. To this end, additional data must be gathered for the parameter characterisation and validation of the numerical models. Nonetheless, various approaches showed promising results as they were able to reproduce fracture development under certain conditions.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W

Validated Reactive Force Field Quantifies MXene Interfacial Properties, Mechanics, and Thermal Transport

MXenes combine rich surface chemistry, mechanical strength, and high conductivity for a multitude of emerging applications. Predictive modeling supports accelerated materials designs and has been limited by the absence of validated and transferable force fields. Here, we introduce an interpretable, reactive INTERFACE force field (IFF and IFF-R) for Ti 3 C 2 T x MXenes that is trained based on chemical knowledge and achieves quantitative agreement with experiments across lattice parameters (<0.5%), density (<0.2%), liquid contact angles, Raman spectra, and the in-plane elastic modulus (∼320 GPa). The models cover surface terminations from hydroxyl (−OH) to fluorine (−F) groups and are extensible to other chemistries. We introduce pH-resolved surface chemistry and identify dopamine adsorption mechanisms at MXene–aqueous interfaces supported by QCM-D and UV–Vis experiments. The data reveal coplanar and perpendicular binding modes and concentration-dependent multilayer assembly. We predict previously inaccessible properties, including termination-dependent cleavage energies, interlayer shear moduli and dynamic shear failure, nanoindentation and brittle fracture, anisotropic in-plane and out-of-plane thermal conductivities, including the role of defects. Agreement with available experimental data is consistently close and exceeds DFT accuracy across the benchmark properties examined. The IFF/IFF-R model is compatible with CHARMM, AMBER, OPLS, and CVFF force fields for simulations of MXenes with diverse surface terminations, electrolyte interfaces, biointerfaces, and polymer composites without additional parameters. Parameter sets, 3D models, and analysis scripts are provided for community use. The validated, reactive, and transferable IFF framework facilitates predictive design of MXene-based films, membranes, sensing interfaces, and composites.

MXene

Precise relative magnitude measurement improves fracture characterization during hydraulic fracturing

SUMMARY Microseismic monitoring is an important technique to obtain detailed knowledge of in-situ fracture size and orientation during stimulation to maximize fluid flow throughout the rock volume and optimize production. Furthermore, considering that the frequency of earthquake magnitudes empirically follows a power law (i.e. Gutenberg–Richter), the accuracy of microseismic event magnitude distributions is potentially crucial for seismic risk management. In this study, we analyse microseismicity observed during four hydraulic fracture treatments of the legacy Cotton Valley experiment in 1997 at the Carthage gas field of East Texas, where fractures were activated at the base of the sand-shale Upper Cotton Valley formation. We perform waveform cross-correlation to detect similar event clusters, measure relative amplitude from aligned waveform pairs with a principal component analysis, then measure precise relative magnitudes. The new magnitudes significantly reduce the deviations between magnitude differences and relative amplitudes of event pairs. This subsequently reduces the magnitude differences between clusters located at different depths. Reduction in magnitude differences between clusters suggests that some attenuation-related biases could be effectively mitigated with relative magnitude measurements. The maximum likelihood method is applied to understand the magnitude frequency distributions and quantify the seismogenic index of the clusters. Statistical analyses with new magnitudes suggest that fractures that are more favourably oriented for shear failure have lower b-value and higher seismogenic index, suggesting higher potential for relatively larger earthquakes, rather than fractures subparallel to maximum horizontal principal stress orientation.

58 GEOSCIENCES

An investigation of the edge-sliding mode in fracture mechanics

A boundary collocation procedure has been applied to the Williams stress function to determine the elastic stress distribution for the crack tip region of a finite, edge-cracked plate subjected to mode II loading at the crack tips. The asymmetric specimen selected was particularly suitable for the determination of plane strain fracture toughness for mode II loading. Numerical solutions for stress intensity factors for the edge-sliding mode obtained by the boundary collocation method were in close agreement with values obtained from photoelastic experiments. Fracture tests of several compact shear specimens of 2024-T4 aluminum were conducted in order to experimentally investigate the behavior of the edge-sliding mode. In each case a brittle shear failure was observed and mode II fracture toughness values were obtained. The average value for K-IIc obtained from two tests was 39.5 ksi radical (in). No K-Ic data for 2024-T4 were available for comparison purposes; however, K-Ic values for a similar alloy, 2024-T351, have been reported as 34 ksi radical (in) which is only about 15 per cent below the corresponding K-IIc value.

Jones, D. L.

Graphite fiber reinforced thermoplastic resins

The results of a program designed to optimize the fabrication procedures for graphite thermoplastic composites are described. The properties of the composites as a function of temperature were measured and graphite thermoplastic fan exit guide vanes were fabricated and tested. Three thermoplastics were included in the investigation: polysulfone, polyethersulfone, and polyarylsulfone. Type HMS graphite was used as the reinforcement. Bending fatigue tests of HMS graphite/polyethersulfone demonstrated a gradual shear failure mode which resulted in a loss of stiffness in the specimens. Preliminary curves were generated to show the loss in stiffness as a function of stress and number of cycles. Fan exit guide vanes of HMS graphite polyethersulfone were satisfactorily fabricated in the final phase of the program. These were found to have stiffness and better fatigue behavior than graphite epoxy vanes which were formerly bill of material.

Navak, R. C.

Thermostructural design of a carbon-carbon heatshield for a Jovian entry

The thermostructural response of three candidate carbon-carbon composites for the Jovian entry probe heatshield was investigated. The analysis for the three materials, Sandia Felt, Carbitex 700, and SAI 4-D weave carbon-carbon was conducted using a dual finite element approach which involved heat conduction as well as the structural response. A receding boundary due to ablation and inertial loads encountered by the probe were included. Severe cracking, circumferential and radial, and interlaminar shear failure was observed during the radiative heating pulse for the Sandia Felt and Carbitex 700 materials, respectively. The 4-D weave material showed no failures over the entire entry.

White, M. J.

A study of the compatibility of an existing CFD package with a broader class of material constitutions

The flexibility of the PHOENICS computational fluid dynamics package was assessed along two general avenues; parallel modeling and analog modeling. In parallel modeling the dependent and independent variables retain their identity within some scaling factors, even though the boundary conditions and especially the constitutive relations do not correspond to any realistic fluid dynamic situation. PHOENICS was used to generate a CFD model that should exhibit the physical anomalies of a granular medium and permit reasonable similarity with boundary conditions typical to membrane or porous piston loading. A considerable portion of the study was spent prying into the existing code with a prejudice toward rate type and disarming any inherent fluid behavior. The final stages of the study were directed at the more specific problem of multiaxis loading of cylindrical geometry with a concern for the appearance of bulging, cross slab shear failure modes.

French, K. W., Jr.