Semi-transparent gold film as simultaneous surface heater and resistance thermometer for nucleate boiling studies
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Oker, E.↗
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Estimating surface temperature in forced convection nucleate boiling: A simplified method
During a test program to investigate low-cycle thermal fatigue, 21 of 22 cylindrical test sections of a cylindrical rocket thrust chamber were thermally cycled to failure. Cylinder liners were fabricated from OFHC copper, Amzirc, and NARloy-Z. The cylinders were fabricated by milling cooling channels into the liner and closing out the backside with electrodeposited copper. The tests were conducted at a chamber pressure of 4.14 MN/sq m (600 psia) and an oxidant-fuel ratio of 6.0 using hydrogen-oxygen as propellants. The average throat heat flux was 54 MW/sq m (33 Btu/sq in./sec). All of the failures were characterized by a thinning of the cooling channel wall and eventual failure by tensile rupture. The 1/2-hard Amzirc material showed little improvement in cyclic life when compared with OFHC copper; while the NARloy-Z and aged Amzirc materials had the best cyclic life characteristics. One OFHC copper cylinder was thermall cycled 2044 times at a steady-state hot-gas-side wall temperature of 514 K (925 R) without failing.
Hendricks, R. C.↗
Estimating surface temperature in forced convection nucleate boiling - A simplified method
A simplified expression to estimate surface temperatures in forced convection boiling was developed using a liquid nitrogen data base. Using the principal of corresponding states and the Kutateladze relation for maximum pool boiling heat flux, the expression was normalized for use with other fluids. The expression was applied also to neon and water. For the neon data base, the agreement was acceptable with the exclusion of one set suspected to be in the transition boiling regime. For the water data base at reduced pressure greater than 0.05 the agreement is generally good. At lower reduced pressures, the water data scatter and the calculated temperature becomes a function of flow rate.
Hendricks, R. C.↗
Molecular model of ice nucleation
Two complementary techniques, semi-empirical quantum mechanical calculations and empirical central field pair potential calculations were used in developing a model of the interaction of water with simple surfaces.
Plummer, P. L. M.↗
Nucleation, growth, and postdeposition thermally induced epitaxy of gold on sapphire
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Heinemann, K.↗
Comments on 'Rocket effluent - Its ice nucleation activity and related properties'
Parungo and Allee (1978) reported ice nucleus (IN) measurements made from an aircraft in stabilized ground clouds from Titan III launches at KSC. They concluded from the measurements that the SGC contained IN. After an examination of the data the present authors (Hindman and Lala) argue that the filter devices were unable to detect IN in the SGC. In a reply Parungo and Allee attempt to refute this conclusion.
Hindman, E. E., II↗
A molecular model for ice nucleation and growth, attachment 1
The quantum mechanical technique is used to study ionic, configurational, and impurity defects in the ice surface. In addition to static calculations of the energetics of the water monomer-ice surface interactions, molecular dynamics studies were initiated. The calculations of the monomer-ice surface interaction, molecular dynamics studies were initiated. The calculations of monomer-ice surface interactions indicate that many adsorption sites exist on the ice surfaces and that the barriers between bonding sites are relatively low. Bonding on the prism face of ice is preferentially above lattice sites.
Plummer, P. L. M.↗
A molecular model for ice nucleation and growth, attachment 2
The central field empirical pair potential model is applied to studying the effects of kinks, ledges, and vacancies on the absorption of water molecules from the vapor. Molecular dynamics simulations indicate that cluster and/or surface modes play a primary role in the absorption process, the flexibility of the hydrogen bond serves to decrease the energy required for structural interconversion, and the rapid distribution of added energy in a hydrogen bonded system lead to aggregate stability which greatly exceeds that predicted by static energy calculations.
Hale, B. N.↗
Experimental program on nucleation and structure in undercooled melts
Undercooling and structural refinements in droplets of molten metal levitated in an induction field and/or by dispersion in a fluid carrier were studied. Nickel base and lower melting point alloys levitated in molten carrier fluids are considered. The dispersion of molten alloy droplets in a high temperature fluid following the procedures developed by Perepezko and co-workers for lower melting point alloys; obtaining a similar dispersion by room temperature mechanical mixing of particles of the metal and solidified liquid carrier; and solidification of single relatively large droplets in a transparent fluid carrier, enabling high-speed temperature measurement of the recalescence and subsequent cooling behavior are described.
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Nucleation theory and its atmospheric applications
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Kiang, C. S.↗
Experimental studies of the vapor phase nucleation of refractory compounds. II - The condensation of an amorphous magnesium silicate
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Nuth, J. A.↗
Contact ice nucleation by submicron atmospheric aerosols
An apparatus designed to measure the concentrations of submicron contact ice nuclei is described. Here, natural forces transfer nuclei to supercooled sample drops suspended in an aerosol stream. Experimental measurements of the scavenging rate of the sample drops for several humidities and aerosol sizes are found to be in agreement with theory to within a factor of two. This fact, together with the statistical tests showing a difference between the data and control samples, is seen as indicating that a reliable measurement of the concentrations of submicron contact ice nuclei has been effected. A figure is included showing the ice nucleus concentrations as a function of temperature and assumed aerosol radius. For a 0.01 micron radius, the average is 1/liter at -15 C and 3/liter at -18 C. It is noted that the measurements are in fair agreement with ice crystal concentrations in stable winter clouds measured over Elk Mountain, WY (Vali et al., 1982).
Deshler, T.↗
A potential energy scaling Monte Carlo simulation of thin film nucleation and growth
The initial growth of thin Ge fims on the (100) surface of an Fe substrate is investigated theoretically by means of Monte Carlo simulations based on a potential-energy-scaling technique. The substrate is modeled as a 20 x 20-square array with periodic boundary conditions, as described by Heinbockel et al. (1983), and the movement of surface atoms under the influence of the substrate interaction potential and the lateral interaction of neighboring atoms is explored via continuous updating (on the time scale of single events) of the potential energy at each site in the array. Results for the clustering of nine dispersed atoms over 1.0 s at 600 K and for deposition at 5 x 10 to the -14th/sq cm s over 2.0 s at 500 K are presented graphically.
Outlaw, R. A.↗
Stability of surface nucleation
The growth and decomposition rates of nuclei on a surface are expressed in microscopic terms. A stability factor is defined and employed for the derivation of a criterion for nucleus stability. Simulation results indicate that the stability factor can be used as a measure of the system stability.
Salik, J.↗
On the theory of the conversion of metallic mixed phases. 5: Fluctuations and nucleation in sub-cooled phases
A comparison is made between fluctuation-theoretical calculations and empirical results. Concentration fluctuations and the resulting separation, and the distribution function of the reversible fluctuations are approximately calculated. The relation of this distribution to the concentration-dependence of the free energy is discussed. Possible effects of fluctuations are discussed, and other attempts to explain the sub-cooling are described.
Borelius, G.↗
Nucleate pool boiling: High gravity to reduced gravity; liquid metals to cryogens
Requirements for the proper functioning of equipment and personnel in reduced gravity associated with space platforms and future space station modules introduce unique problems in temperature control; power generation; energy dissipation; the storage, transfer, control and conditioning of fluids; and liquid-vapor separation. The phase change of boiling is significant in all of these. Although both pool and flow boiling would be involved, research results to date include only pool boiling because buoyancy effects are maximized for this case. The effective application of forced convection boiling heat transfer in the microgravity of space will require a well grounded and cogent understanding of the mechanisms involved. Experimental results are presented for pool boiling from a single geometrical configuration, a flat surface, covering a wide range of body forces from a/g = 20 to 1 to a/g = 0 to -1 for a cryogenic liquid, and from a/g = 20 to 1 for water and a liquid metal. Similarities in behavior are noted for these three fluids at the higher gravity levels, and may reasonably be expected to continue at reduced gravity levels.
Merte, Herman, Jr.↗
Grain boundary oxidation and an analysis of the effects of oxidation on fatigue crack nucleation life
The effects of preoxidation on subsequent fatigue life were studied. Surface oxidation and grain boundary oxidation of a nickel-base superalloy (TAZ-8A) were studied at 600 to 1000 C for 10 to 1000 hours in air. Surface oxides were identified and the kinetics of surface oxidation was discussed. Grain boundary oxide penetration and morphology were studied. Pancake type grain boundary oxide penetrates deeper and its size is larger, therefore, it is more detrimental to fatigue life than cone-type grain boundary oxide. Oxide penetration depth, a (sub m), is related to oxidation temperature, T, and exposure time, t, by an empirical relation of the Arrhenius type. Effects of T and t on statistical variation of a (sub m) were analyzed according to the Weibull distribution function. Once the oxide is cracked, it serves as a fatigue crack nucleus. Statistical variation of the remaining fatigue life, after the formation of an oxide crack of a critical length, is related directly to the statistical variation of grain boundary oxide penetration depth.
Oshida, Y.↗
Protein crystal nucleation kinetics using relative light-scattering techniques: Center director's discretionary fund
Light-scattering intensity measurements are a sensitive method for following changes in the hydrodynamic radius of particles in solution. The approach used in this report utilizes the light-scattering intensity ratios of a polydisperse to a monodisperse system. By numerically modeling the process, and fitting the model curves to the data, estimates have been obtained for the dimerization equilibrium constant, the dimer + dimer yields tetramer equilibrium constant, and the association rate constant for the dimerization process.
Pusey, Marc Lee↗