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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 415 records · Page 23

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DOE OSTI2026

Effects of PLA/PHB Blend Ratio and Wood Flour Loading on the Melt Rheology and Thermomechanical Properties of Biobased Polymer Composites

The development of sustainable, biobased polymer composites is crucial for reducing supply chain dependence on fossil fuels. A major challenge lies in understanding and predicting the processability of these sustainable material alternatives, which directly impacts large-scale manufacturing. Here, this study systematically investigates the effect of poly(lactic acid) (PLA)/polyhydroxybutyrate (PHB) blend ratios and wood flour (WF) loadings on the thermal, rheological, and mechanical properties of the composites. Composites were prepared via melt compounding and characterized by using differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), oscillatory shear melt rheology, tensile testing, and scanning electron microscopy. Results showed that increasing the PHB content lowered the glass transition temperature, while higher PHB and WF loadings decreased thermal stability. Complex viscosity decreased with increasing PHB in 0 and 10% WF, whereas it increased in 20% and 30% WF for PHB-rich blends (80/20 and 70/30 PLA/PHB) due to stronger filler interactions with flexible PHB chains. At 30% WF, PHB-containing composites also showed elastic dominance with G′ higher than G″. This behavior was confirmed by van Gurp–Palmen plots, where the phase angle decreased with increasing PHB and WF loadings. WF addition also shifted Cole–Cole plots away from semicircular terminal relaxation, while time–temperature superposition validity was maintained, confirming that polymer chain dynamics continue to dominate melt behavior. Young’s modulus increased with WF loading, while tensile strength and toughness decreased due to weaker interfacial adhesion between the matrix and the filler. Interestingly, 10% WF systems containing PHB exhibited the highest toughness among all of the filled systems, indicating synergistic reinforcement from WF fillers and PHB-induced ductility. Overall, melt rheology effectively captured the internal structure and stiffness of the composites as the formulation changed, reinforcing the concept that the PLA/PHB ratio and WF content can be tuned to adjust melt elasticity and balance mechanical property trade-offs for targeted applications.

melt rheology↗

NASA NTRS1983

Graphite/Larc-160 technology demonstration segment test results

A structural test program was conducted on a Celion/LARC-160 graphite/polyimide technology demonstration segment (TDS) to verify the technology. The 137 x 152 cm (54 x 60 in.) TDS simulates a full-scale section of the orbiter composite body flap design incorporating three ribs and extending from the forward cove back to the rear spar. The TDS was successfully subjected to mechanical loads and thermal environments (-170 to 316 C) simulating 100 shuttle orbiter missions. Successful completion of the test program verified the design, analysis, and fabrication methodology for bonded Gr/PI honeycomb sandwich structure and demonstration that Gr/PI composite technology readiness is established.

Morita, W. H.↗

NASA NTRS2011

Edgewise Compression Testing of STIPS-0 (Structurally Integrated Thermal Protection System)

The Structurally Integrated Thermal Protection System (SITPS) task was initiated by the NASA Hypersonics Project under the Fundamental Aeronautics Program to develop a structural load-carrying thermal protection system for use in aerospace applications. The initial NASA concept for SITPS consists of high-temperature composite facesheets (outer and inner mold lines) with a light-weight insulated structural core. An edgewise compression test was performed on the SITPS-0 test article at room temperature using conventional instrumentation and methods in order to obtain panel-level mechanical properties and behavior of the panel. Three compression loadings (10, 20 and 37 kips) were applied to the SITPS-0 panel. The panel behavior was monitored using standard techniques and non-destructive evaluation methods such as photogrammetry and acoustic emission. The elastic modulus of the SITPS-0 panel was determined to be 1.146x106 psi with a proportional limit at 1039 psi. Barrel-shaped bending of the panel and partial delamination of the IML occurred under the final loading.

Brewer, Amy R.↗

NASA NTRS1981

Test methods and design allowables for fibrous composites; Proceedings of the Symposium, Dearborn, MI, October 2, 3, 1979

Papers are presented on special test methods for fibrous composites for quantifying design material properties. Studies are divided into four major areas: (1) new and special test methods, including those for transverse tensile strength, shear modulus, longitudinal compression, and impact resistance; (2) special test methods and analysis, including off-axes and angle-plied tension and compression, fracture and fatigue, and biaxial stress states; (3) design allowables, describing procedures for setting and selecting design allowables in general, and also for composite aircraft structures, graphite/polyimide bolted joints, cost-effective mechanical property characterization, statistical considerations, intraply hybrids, and compression and fatigue; (4) design allowables for special applications, describing procedures for buckling of cylindrical components, proof load of pressure vessels, strength of composite joints, and environmental effects and creep. The papers provide considerable information for test methods and for composite analysis of these methods, as well as tests and procedures for establishing design allowables.

Chamis, C. C.↗

NASA NTRS1979

Design fabrication and test of graphite/polyimide composite joints and attachments for advanced aerospace vehicles

Graphite/polyimide (Gr/PI) bolted and bonded joints were investigated. Possible failure modes and the design loads for the four generic joint types are discussed. Preliminary sizing of a type 1 joint, bonded and bolted configuration is described, including assumptions regarding material properties and sizing methodology. A general purpose finite element computer code is described that was formulated to analyze single and double lap joints, with and without tapered adherends, and with user-controlled variable element size arrangements. An initial order of Celion 6000/PMR-15 prepreg was received and characterized.

Source record↗

NASA NTRS1997

Application of Laser Based Ultrasound for NDE of Damage in Thick Stitched Composites

As design engineers implement new composite systems such as thick, load bearing composite structures, they must have certifiable confidence in structure s durability and worthiness. This confidence builds from understanding the structural response and failure characteristics of simple components loaded in testing machines to tests on full scale sections. Nondestructive evaluation is an important element which can provide quantitative information on the damage initiation, propagation, and final failure modes for the composite structural components. Although ultrasound is generally accepted as a test method, the use of conventional ultrasound for in-situ monitoring of damage during tests of large structures is not practical. The use of lasers to both generate and detect ultrasound extends the application of ultrasound to in- situ sensing of damage in a deformed structure remotely and in a non-contact manner. The goal of the present research is to utilize this technology to monitor damage progression during testing. The present paper describes the application of laser based ultrasound to quantify damage in thick stitched composite structural elements to demonstrate the method. This method involves using a Q-switched laser to generate a rapid, local linear thermal strain on the surface of the structure. This local strain causes the generation of ultrasonic waves into the material. A second laser used with a Fabry-Perot interferometer detects the surface deflections. The use of fiber optics provides for eye safety and a convenient method of delivering the laser over long distances to the specimens. The material for these structural elements is composed of several stacks of composite material assembled together by stitching through the laminate thickness that ranging from 0.5 to 0.8 inches. The specimens used for these nondestructive evaluation studies had either impact damage or skin/stiffener interlaminar failure. Although little or no visible surface damage existed, internal damage was detected by laser based ultrasound.

Anastasi, Robert F.↗

NASA NTRS1971

Effects of cyclical environments on high-performance multi-layer insulation materials.

Results of a test program designed to determine the effects of 100 temperature and compressive loading cycles on several multilayer insulation materials and composites. A total of four reflector materials, four separator materials, eight face-sheet systems, and one fastener material were subjected to 100 temperature cycles from -320 to 400 or 650 F. Generic types of materials studied included Mylar, Kapton, Dacron, Nomex, and Beta Glass. The temperature cycling was followed by visual inspection, metal adhesion tests on the reflectors, and tensile tests of the face sheets, fastener, and separators. A total of six composites were subjected to compressive cycles between zero and 0.15 psi, and density changes were measured. Application of the experimental results to the shuttle orbiter is discussed.

Krause, D. R.↗

NASA NTRS1989

The isothermal fatigue behavior of a unidirectional SiC/Ti composite and the Ti alloy matrix

The high temperature fatigue behavior of a metal matrix composite (MMC) consisting of Ti-15V-3Cr-3Al-3Sn (Ti-15-3) matrix reinforced by 33 vol percent of continuous unidirectional SiC fibers was experimentally and analytically evaluated. Isothermal MMC fatigue tests with constant amplitude loading parallel to the fiber direction were performed at 300 and 550 C. Comparative fatigue tests of the Ti-15-3 matrix alloy were also conducted. Composite fatigue behavior and the in-situ stress state of the fiber and matrix were analyzed with a micromechanical model, the Concentric Cylinder Model (CCM). The cyclic stress-strain response of the composite was stable at 300 C. However, an increase in cyclic mean strain foreshortened MMC fatigue life at high strain ranges at 550 C. Fatigue tests of the matrix alloy and CCM analyses indicated this response was associated with stress relaxation of the matrix in the composite.

Gayda, John, Jr.↗

NASA NTRS1981

Indentation law for composite laminates

Static indentation tests are described for glass/epoxy and graphite/epoxy composite laminates with steel balls as the indentor. Beam specimens clamped at various spans were used for the tests. Loading, unloading, and reloading data were obtained and fitted into power laws. Results show that: (1) contact behavior is not appreciably affected by the span; (2) loading and reloading curves seem to follow the 1.5 power law; and (3) unloading curves are described quite well by a 2.5 power law. In addition, values were determined for the critical indentation, alpha sub cr which can be used to predict permanent indentations in unloading. Since alpha sub cr only depends on composite material properties, only the loading and an unloading curve are needed to establish the complete loading-unloading-reloading behavior.

Yang, S. H.↗

NASA NTRS1982

Indentation law for composite laminates

Yang, S. H.↗

NASA NTRS1992

The Utilization of Advanced Composites in Military Aircraft

The purpose of this workshop was to identify the current state of the art in key issues related to compression loading and fluid effects in composite materials. In the area of compression loading, there was considerable concern over the different results obtained from various test methods. It was agreed that failure modes produced by the various test methods along with a better fundamental understanding of compression failure were key issues in the development of compression test methods. In the area of fluid effects, a lack of a comprehensive data base hampers identification of key mechanisms leading to fluid degradation. This is further complicated by the fact that interactions depend on the fluid and composite under consideration.

Advisory Group for Aerospace Research and Developm↗

DOE OSTI2025

Fused Deposition Modeling Additive Manufacturing of Carbonized Structures via Waste-Enhanced Filaments

This report details the development, characterization, and use of coal-enhanced composite materials in additive manufacturing applications. High coal loading formulations—containing up to 70 wt.% coal—were successfully extruded and processed using commercially available 3D printers. Extensive experimental testing was conducted to assess the mechanical, thermal, and microstructural properties of the composites. In parallel, multi-scale computational modeling was employed to elucidate atomistic interactions and evaluate the effects of printing-induced defects on structural performance. Large-scale printability trials demonstrated the feasibility of fabricating complex components for tooling and construction applications, including wind turbine blade molds and modular wall sections. Techno-economic analyses demonstrated the cost-effectiveness and scalability of coal-enhanced composites for large-scale additive manufacturing applications such as wind turbine blade tooling.

01 COAL, LIGNITE, AND PEAT↗

NASA NTRS1992

A review of crack propagation under unsteady loading

The theories and research current available on crack propagation under unsteady loadings, especially those of acoustic origin, are reviewed. Since the original theories on fatigue failure did not account for random loading conditions, modified theories which provide statistical methods for evaluating the random loading have emerged. The impact of acoustic fatigue in the aerospace industry, basic principles such as fatigue crack initiation and propagation and load interactions, and testing procedures are discussed. Attention is also given to metal and metal alloy structures, fiber-reinforced composites and nonmetallic structures, short crack growth, and the effects of temperature, moisture, and corrosion on structures. Suggestions for future research in this field are presented, namely, studies on the effect of 'snap-through' response and associated crack growth patterns, studies in microcrack and 'small crack'; propagation under unsteady loading conditions, and the development of an accurate analytical model to predict acceleration and retardation effects in fatigue crack growth under random loading conditions.

Bryan, H. H.↗

NASA NTRS2015

Experimental and Numerical Analysis of Triaxially Braided Composites Utilizing a Modified Subcell Modeling Approach

A combined experimental and analytical approach was performed for characterizing and modeling triaxially braided composites with a modified subcell modeling strategy. Tensile coupon tests were conducted on a [0deg/60deg/-60deg] braided composite at angles [0deg, 30deg, 45deg, 60deg and 90deg] relative to the axial tow of the braid. It was found that measured coupon strength varied significantly with the angle of the applied load and each coupon direction exhibited unique final failures. The subcell modeling approach implemented into the finite element software LS-DYNA was used to simulate the various tensile coupon test angles. The modeling approach was successful in predicting both the coupon strength and reported failure mode for the 0deg, 30deg and 60deg loading directions. The model over-predicted the strength in the 90deg direction; however, the experimental results show a strong influence of free edge effects on damage initiation and failure. In the absence of these local free edge effects, the subcell modeling approach showed promise as a viable and computationally efficient analysis tool for triaxially braided composite structures. Future work will focus on validation of the approach for predicting the impact response of the braided composite against flat panel impact tests.

Polymer Matrix Composites↗

NASA NTRS2002

Micro-Cracking Detection in Laminated Composites

Porosity and fatigue cracking are two critical factors that affect the performance and safety of cryogenic fuel tanks and feedlines made from unlined laminated or weaved carbon/epoxy materials. This paper presents the experiments to induce fatigue cracking of laminated composites through thermal cycling as well as the feasibility of using Thermography and Ultrasound Spectroscopy technology (UT) to detect and measure such micro-cracking. Carbon/epoxy laminated composite panels were built and cut into strips. These specimens were partially submerged in liquid nitrogen while subjected to various loads on a test machine. Edges of some specimens were polished and etched to determine the degree of micro-cracking. The rest of specimens were then examined with Thermography and Ultrasound Spectroscopy NDE systems to investigate the feasibility of finding such micro-cracking in the laminated composites. Thermography is utilized to determine changes in thermal diffusivity. The degree of cracking may reduce the apparent thermal diffusivity and therefore change the thermal response on the surface. Thermography testing was conducted on a group of specimens where it is desired to have some correlation between the predetermined stress and the thermography data. Ultrasound Spectroscopy was used to determine peak changes between the pre-stressed and stressed samples. Data from the inspections were analyzed and the results are presented in this paper.

Chu, Tsuchin↗

NASA NTRS1982

Small Fixture Strains Composites for Environmental Tests

Fixture for long-term strain tests of composites is based on inexpensive tool for repairing motorcycle chains. (In normal use tool forces rivet out of chain element.) As modified for composite testing, tool has precision screw and shim. Qualification tests for graphite/epoxy composites are made less expensive by simple test fixture. Used in quantity, fixtures apply precisely similar loads to many samples.

Tervet, F. W.↗

NASA NTRS1985

Thermal-mechanical fatigue test apparatus for metal matrix composites and joint attachments

Two thermal-mechanical fatigue (TMF) test facilities were designed and developed, one to test tungsten fiber reinforced metal matrix composite specimens at temperature up to 1430C (2600F) and another to test composite/metal attachment bond joints at temperatures up to 760C (1400 F). The TMF facility designed for testing tungsten fiber reinforced metal matrix composites permits test specimen temperature excursions from room temperature to 1430C (2600F) with controlled heating and loading rates. A strain-measuring device measures the strain in the test section of the specimen during each heating and cooling cycle with superimposed loads. Data is collected and recorded by a computer. The second facility is designed to test composite/metal attachment bond joints and to permit heating to a maximum temperature of 760C (1400F) within 10 min and cooling to 150C (300F) within 3 min. A computer controls specimen temperature and load cycling.

Westfall, L. J.↗

NASA NTRS1988

Thermal-mechanical fatigue test apparatus for metal matrix composites and joint attachments

Two thermal-mechanical fatigue (TMF) test facilities were designed and developed, one to test tungsten fiber reinforced metal matrix composite specimens at temperature up to 1430C (2600F) and another to test composite/metal attachment bond joints at temperatures up to 760F (1400F). The TMF facility designed for testing tungsten fiber reinforced metal matrix composites permits test specimen temperature excursions from room temperature to 1430C (2600F) with controlled heating and loading rates. A strain-measuring device measures the strain in the test section of the specimen during each heating and cooling cycle with superimposed loads. Data is collected and recorded by a computer. The second facility is designed to test composite/metal attachment bond joints and to permit heating to a maximum temperature of 760C (1400F) within 10 min and cooling to 150C (300F) within 3 min. A computer controls specimen temperature and load cycling.

Westfall, Leonard J.↗