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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 433 records · Page 24

Large deflection behavior of quasi-isotropic laminates under low-velocity impact type point loading

Eight-ply quasi-isotropic circular composite plates of Thornel 300 graphite in Narmco 5208 epoxy resin (T300/5208) were analyzed to obtain the large deformation behavior under low-velocity impact type point loads. A simple plate-membrane coupling model was developed. The impact type point loads were replaced by equivalent quasi-static point loads. The plate-membrane coupling model was used to obtain the large deformation shapes for the thin circular composite laminates. The analyses indicated that the large deformation shapes of the composite plates under point loads vary with the center point displacements, and hence are different for different load levels. Quasi-isotropic plates were analyzed by replacing anisotropic bending stiffness components with the equivalent flexural stiffness for the isotropic plates. The plate-membrane coupling model was verified by conducting a series of tests on clamped circular quasi-isotropic laminates. Deflected shapes for the thin composite plates were experimentally obtained. These shapes agreed well with the analytically predicted shapes.

Kelkar, A.↗

Novel ductile wellbore cementitious composite for geologic CO 2 storage

CO 2 leakage through damaged wellbore cement sheaths is a major risk of geologic CO 2 storage (GCS), as conventional wellbore cement is brittle and can be damaged due to acid attack and downhole stresses during CO 2 injection. Here we examine a novel fiber-reinforced engineered cementitious composite (ECC) proposed as a substitute to conventional wellbore cement due to its superior ductility and intrinsic crack width control. ECC and conventional wellbore cement coupons were exposed to water in equilibrium with CO 2 at 50 °C and 10 MPa. The samples were retrieved after several days and their mechanical performance was evaluated using a four-point bending test, microhardness, and compressive strength analyses. Optical microscopy and mercury intrusion porosimetry were used to characterize the progression of the carbonation front and pore structures of the specimens. Control experiments were conducted under the same temperature and pressure conditions but with a N 2 headspace to isolate the impact of CO 2 . It was found that carbonation increased the ultimate flexural strength of ECC but decreased its ductility. However, the ductility of carbonated ECC remained higher than that of conventional wellbore cements that exhibited brittle failure under all test conditions. Additionally, ECC exhibited minimal material loss and continued resistance to deformation in comparison to conventional wellbore cements. This suggests that while the exposure of ECC to CO 2 will alter its mechanical properties, altered ECC will continue to exhibit mechanical performance superior to conventional wellbore cement, and therefore shows promise as a highly durable wellbore cementing material for GCS applications.

58 GEOSCIENCES↗

Advanced Modeling of Micromirror Devices

The flexure-beam micromirror device (FBMD) is a phase only piston style spatial light modulator demonstrating properties which can be used for phase adaptive corrective optics. This paper presents a complete study of a square FBMD, from advanced model development through final device testing and model verification. The model relates the electrical and mechanical properties of the device by equating the electrostatic force of a parallel-plate capacitor with the counter-acting spring force of the device's support flexures. The capacitor solution is derived via the Schwartz-Christoffel transformation such that the final solution accounts for non-ideal electric fields. The complete model describes the behavior of any piston-style device, given its design geometry and material properties. It includes operational parameters such as drive frequency and temperature, as well as fringing effects, mirror surface deformations, and cross-talk from neighboring devices. The steps taken to develop this model can be applied to other micromirrors, such as the cantilever and torsion-beam designs, to produce an advanced model for any given device. The micromirror devices studied in this paper were commercially fabricated in a surface micromachining process. A microscope-based laser interferometer is used to test the device in which a beam reflected from the device modulates a fixed reference beam. The mirror displacement is determined from the relative phase which generates a continuous set of data for each selected position on the mirror surface. Plots of this data describe the localized deflection as a function of drive voltage.

Michalicek, M. Adrian↗

Infusible thermoplastic resin based sandwich structures for wind blade applications and the influence of scrim on facesheet to core interface debonding

Infusible thermoplastic Elium® family of resins from Arkema have garnered much attention in recent years as a possible replacement for thermoset resins in laminate and sandwich composite manufacturing for wind blade applications due to its ease of recyclability and the ability to utilize existing manufacturing processes without imposing complicated variations. However, physical and mechanical properties of the proposed Elium® based thermoplastic composites must be comparable to existing epoxy (thermoset) based composites using manufacturing processes relevant for large wind turbine blades. A 13-meter-long demonstration blade was manufactured for that purpose and sandwich samples were obtained from that project for a detailed study. This paper details three-point flexural properties of unidirectional E-glass fiber reinforced acrylic and epoxy based sandwich panels with identical balsa wood core materials. In addition, to evaluate the relative merit considering debond failure mode, the interfacial critical strain energy release rate, predominantly in mode-1, was compared via single cantilever beam testing. In sandwich composites constructed with balsa wood core material, resin uptake by the balsa core is traditionally impeded via the insertion of a scrim material at the facesheet to core interface. Results revealed that inclusion of scrim mesh layer at the facesheet to core interface reduced flexural properties and strain energy release rates in panels infused with acrylic resin but did not significantly reduce these properties in epoxy infused facesheets.

Engineering↗

Effect of Control Mode and Test Rate on Fracture Toughness of Advanced Ceramics

The effects of control mode and rate on the fracture toughness of ceramics were measured by using chevron-notched flexure specimen in accordance with ASTM C1421. The use of stroke control gave consistent results with about 2% variation in measured fracture toughness for a very wide range of rates (0.005 to 0.5 mm/min). Use of strain or CMOD control gave ~5% variation over a very wide range of rates, with the measurements being a function of rate. However, the effect was eliminated by use of dry nitrogen, implying a stress corrosion effect rather than a stability effect. With the use of nitrogen for strain control, fracture toughness values were within about 1% over a wide range of rates (1 to 80 /s). CMOD or strain control did allow stable crack extension well past maximum load, and thus is preferred for energy calculations. The effort is being used to confirm recommendations in ASTM International standard C1421 on fracture toughness measurement.

fracture toughness↗

Two-Stage Passive Vibration Isolator

The design and testing of a structural system were implemented to hold the optics of the planned Space Interferometry Mission (SIM) at positions and orientations characterized by vibrational translation and rotation errors of no more than a few nanometers or a few milliarcseconds, respectively. Much of the effort was devoted to a test bed for verifying the predicted behavior of a vibration- isolation structural subsystem working together with an active control system for positioning and orienting the SIM optics. There was considerable emphasis on the vibration-isolation subsystem, which was passive and comprised two stages. The main sources of vibration were six reaction wheels in an assembly denoted the "backpack." The first vibration-isolation stage consisted of hexapod isolator mounts - one for each reaction wheel - characterized by a natural vibration frequency of 10 Hz. The second stage was a set of three beams, disposed between the backpack and the structure that held the SIM optics, that were flexured such that they transmitted only bending loads, with a natural vibrational frequency and damping of about 5 Hz and 4 percent, respectively. Preliminary test results were presented and characterized as demonstrating the effectiveness of the two-stage vibration-isolation design.

Goullioud, Renaud↗

Analytical and experimental investigations of human spine flexure.

The authors report on experiments to measure the resistance of fresh human spines to flexion in the upper lumbar and lower thoracic regions and evaluate results by using a combination of strength of materials theory and effects of shear and comparing with data reported by other authors. The test results indicate that the thoraco-lumbar spine behaves approximately as a linear elastic beam, without relaxation effects. The authors formulate a simple continuum dynamic model of the spine simulating aircraft ejection and solve the resulting boundary value problem to illustrate the importance of the flexural mode. A constant cross-section, the selected model is a sinusoidally curved elastic beam with an end mass subjected to a Heaviside axial acceleration at the other end. The paper presents transient response results for the spinal model axial and bending displacements and axial force.-

Moffatt, C. A.↗

Analysis of three-point-bend test for materials with unequal tension and compression properties

An analysis capability is described for the three-point-bend test applicable to materials of linear but unequal tensile and compressive stress-strain relations. The capability consists of numerous equations of simple form and their graphical representation. Procedures are described to examine the local stress concentrations and failure modes initiation. Examples are given to illustrate the usefulness and ease of application of the capability. Comparisons are made with materials which have equal tensile and compressive properties. The results indicate possible underestimates for flexural modulus or strength ranging from 25 to 50 percent greater than values predicted when accounting for unequal properties. The capability can also be used to reduce test data from three-point-bending tests, extract material properties useful in design from these test data, select test specimen dimensions, and size structural members.

Chamis, C. C.↗

Detailed Analysis of RUS Insertion Experiment and Scoping Studies for Performing Next Experiment using an Enriched Fuel Sample

Microstructure evolution due to irradiation in a nuclear reactor can have a dramatic effect on material properties. A better understanding of this evolution is necessary for developing improved nuclear fuels and materials. The ability to measure such changes in real time is extremely challenging due to high temperatures, high radiation fields, and limited access of the reactor environment. Through carefully designed experiments, measurement of elastic properties can be tied directly to microstructure. We present an instrument that has been developed to monitor in-pile changes in grain microstructure. The measurement approach involves optically exciting and detecting flexural waves in a thin cantilever beam. An instrument capsule based on this technique was fabricated and underwent an irradiation test in the TREAT reactor in May 2019. Analyses of the test results are presented in this report. Scoping studies on the expected impact of radiation on similar tests are also presented.

36 MATERIALS SCIENCE↗

An Investigation on the Accuracy of Delamination Analysis Predictions for Unidirectional Laminate Configurations

The state-of-the-art methodologies for predicting delamination growth in composite laminates make use of the concept of mixed-mode fracture mechanics. In mixed-mode fracture approaches the individual Mode I, Mode II and Mode III components of the strain energy release rate (SERR) need to be determined under general loading conditions. Through the use of mixed-mode fracture, the individual components are used in combination with the critical strain energy release rates (interlaminar fracture toughnesses) for each fracture mode in a mixed mode criterion in order to predict delamination extension. These interlaminar fracture toughnesses are traditionally obtained by testing of unidirectional laminate coupons. This work presents an investigation on the accuracy of Double Cantilever Beam (DCB), End Notch Flexure (ENF) and Mixed-Mode Bending (MMB) delamination analysis predictions by comparing measured total strain-energy release rates obtained experimentally to results for structural analysis from closed-form expressions, shell finite element analysis, and continuum two-dimensional (2D) and three-dimensional (3D) (solid) finite element analysis.

Patrick Enjuto↗

Mechanical and Thermophysical Properties of 3D-Printed SiC-FY20

In the Transformational Challenge Reactor (TCR), the fuel blocks consist of an additively-manufactured silicon carbide (SiC) matrix and uranium nitride tristructural isotropic (UN TRISO) fuel particles, which are stacked to form fuel columns. The SiC matrix is manufactured using binderjet 3D printing followed by loading the TRISO fuel particles and the chemical vapor infiltration (CVI) process. Because the fuel matrix is a primary component of the TCR core and its response to mechanical and thermal loads during operation is one of the most influential factors on the integrity of TCR core, testing and evaluation have focused on producing mechanical and thermophysical properties data for the binderjet/CVI SiC. Mechanical and thermophysical properties were measured from various types of specimens printed for two or three orientations, which included equibiaxial flexural failure strength, elastic constants, thermal diffusivity and conductivity, density, and the coefficient of thermal expansion. Flexural failure strength datasets showed similar Weibull distributions regardless of sample variants including different orientations. The mean failure strengths of the 3D-printed SiC variants were in the range of 286–306 MPa, which are 22–27% lower than that of the CVD SiC. Thermophysical test results showed that specific heat and thermal expansion are not sensitive to the build directions of SiC samples, while thermal diffusivity is highly dependent on the build direction and can be correlated to the anisotropic character of the 3D-printed SiC. This report also includes discussions on the uniaxial tensile properties of the as-printed SiC before CVI and on ongoing efforts for irradiation effects studies.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Mechanical and Thermophysical Properties of 3D-Printed SiC before and after Neutron Irradiation – FY21

This report presents the mechanical and thermophysical properties of 3D-printed SiC before and after neutron irradiation that have been evaluated to assess the fuel matrix material for the Transformational Challenge Reactor (TCR). The TCR fuel form consists of an additively-manufactured silicon carbide (SiC) matrix and uranium nitride tristructural isotropic (UN TRISO) fuel particles, which is manufactured through a newly developed processing route combining binderjet 3D printing, TRISO fuel particle loading, and chemical vapor infiltration (CVI). Because the fuel matrix is a primary component of the TCR core and its response to mechanical and thermal loads during operation is one of the most influential factors on the integrity of TCR core, testing and evaluation have focused on producing mechanical and thermophysical properties data for the binderjet/CVI SiC. Baseline mechanical and thermophysical properties were measured from the disk specimens printed for different and sizes orientations, which included equibiaxial flexural failure strength, elastic constants, thermal diffusivity and conductivity, density, and the coefficient of thermal expansion. Flexural failure strength datasets showed similar Weibull distributions regardless of sample variants including different orientations. The mean failure strengths of the 3D-printed SiC variants were in the range of 280–310 MPa, which are slightly lower than that of the chemical vapor deposition (CVD) SiC. Thermophysical test results showed that specific heat and thermal expansion are not sensitive to the build direction of SiC samples, while thermal conductivity is highly dependent on the build direction and can be correlated to the anisotropic character of the 3D-printed SiC. Neutron irradiation tests were carried out on the 3D-printed 6-mm diameter SiC disk specimens. Irradiation was carried to 2.3 dpa over a temperature range of 360–880°C. No significant degradation in strength was observed in SiC after irradiations in various conditions and with different orientations. Anisotropy that had been observed in the thermal conductivity of 3D-printed SiC prior to irradiation vanished after irradiation as the irradiation defect thermal resistivity accumulated in the material. Electron microscopy of the microstructure after neutron irradiation showed distinct defect morphologies in the heterogenous material, but no evidence for irradiation-induced cracking or degradation in the microstructure was observed.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Flaw detection by mechanical resonant measurement

Testing technique is based on analysis of varying frequency scan applied to measured samples. Any changes in resonant-frequency harmonics detected in samples are used to indicate size of fault. Testing apparatus uses drive mechanism to apply vibrating force to sample. Force is applied longitudinally along axis to eliminate directionality on flexural vibrations.

Buck, O.↗

Effects of vibration and shock on the performance of gas-bearing space-power Brayton cycle turbomachinery. Part 4: Suppression of rotor-bearing system vibrations through flexible bearing support damping

A bearing damper, operating on the support flexure of a pivoted pad in a tilting-pad type gas-lubricated journal bearing, has been designed, built, and tested under externally-applied random vibrations. The NASA Brayton Rotating Unit (BRU), a 36,000 rpm, 10-Kwe turbogenerator had previously been subjected in the MTI Vibration Test Laboratory to external random vibrations, and vibration response data had been recorded and analyzed for amplitude distribution and frequency content at a number of locations in the machine. Based on data from that evaluation, a piston-type damper was designed and developed for each of the two flexibly-supported journal bearing pads (one in each of the two three-pad bearings). A modified BRU, with dampers installed, has been re-tested under random vibration conditions. Root-mean-square vibration amplitudes were determined from the test data, and displacement power spectral density analyses have been performed. Results of these data reduction efforts have been compared with vibration tolerance limits. Results of the tests indicate significant reductions in vibration levels in the bearing gas-lubricant films, particularly in the rigidly-mounted pads. The utility of the gas-lubricated damper for limiting rotor-bearing system vibrations in high-speed turbomachinery has thus been demonstrated.

Tessarzik, J. M.↗

Feasibility study on the development of tough, moisture-resistant laminating resins

The potential of cyanate resins as replacement for epoxy resins in composites with graphite fiber reinforcement was investigated in an effort to provide improved moisture resistance and toughness in laminating systems at a projected cost, handleability, and processing requirements equivalent to 400 K (260 F) curing epoxies. Monomer synthesis, formulation, blending, resin preparation, catalysis studies, prepreg preparation, laminate fabrication, and testing are discussed. A graphite fiber reinforced laminate was developed with 95 percent retention of the original 363 K (180 F) flexural strength and 70 percent retention of the 363 K (180 F) short beam shear strength after 500 hour exposure to 95 + 7 relative humidity at 324 K (120 F).

Brand, R. A.↗

Phase-A COBE study

A scaled version of a conical apodizing horm similar to the one used in the Cosmic Background Explorer as the antenna for the far infrared absolute spectrometer (FIRAS) was tested to determine its diffraction patterns. The test transmitter used and results are described. Calculation of the tradeoff between noise and spectral resolution for the FIRAS are examined. Flexural transports, the optical properties of the Martin-Pupplet polarizing interferometer, and radiation absorption of thin bismuth films are also discussed.

Source record↗

Polyimide matrix composites - Polyimidesulfone/LARC-TPI (1:1) blend

Polyimide matrix composites were fabricated from unidirectional unsized AS-4 carbon fiber and a doped 1:1 blend of two polyimides: PISO2 and LARC-TPI. To enhance melt flow properties, the molecular weight of the PISO2 was controlled by end-capping with phthalic anhydride and addition of 5 percent by weight p-phenylenediamine-phthalic anhydride bisamic acid dopant. Prepreg was drum-wound using a diglyme slurry comprised of the soluble polyamideacid of PISO2, the soluble bisamideacid of the dopant, and the insoluble imidized LARC-TPI powder. Melt flow studies with a rotary rheometer and parallel plate plastometer on neat resin and prepreg helped develop an optimum cure cycle. Composite mechanical properties at room and elevated temperatures, dry and moisture-saturated, were evaluated, including short beam shear strength and flexure, tensile, shear, and compression properties. Two 18 x 24-inch skin-stringer panels were fabricated, one of which was tested in compression to failure.

Johnston, Norman J.↗

Radial basis function network learns ceramic processing and predicts related strength and density

Radial basis function (RBF) neural networks were trained using the data from 273 Si3N4 modulus of rupture (MOR) bars which were tested at room temperature and 135 MOR bars which were tested at 1370 C. Milling time, sintering time, and sintering gas pressure were the processing parameters used as the input features. Flexural strength and density were the outputs by which the RBF networks were assessed. The 'nodes-at-data-points' method was used to set the hidden layer centers and output layer training used the gradient descent method. The RBF network predicted strength with an average error of less than 12 percent and density with an average error of less than 2 percent. Further, the RBF network demonstrated a potential for optimizing and accelerating the development and processing of ceramic materials.

Cios, Krzysztof J.↗