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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 433 records · Page 24

Experimental studies of high-temperature thermal dissociation of iso-propanol

iso-Propanol is an important biofuel for transportation and industrial applications, as well as a canonical compound for understanding alcohol reaction chemistry. There are few studies of the thermal decomposition of iso-propanol, hence the objective of this work was to investigate the mechanism of iso-propanol pyrolysis at high-temperature conditions. Shock tube studies were used to investigate the thermal decomposition of iso-propanol and identify the dominant reaction pathways and the intermediate species present in the temperature range of 1395–2053 K and at pressures of 0.3–4 bar. Time-resolved mass spectra were obtained from pyrolysis experiments in shock tube/mass spectrometer apparatuses using electron impact ionization or synchrotron vacuum ultraviolet photoionization. The relative concentrations of the intermediate species were used to identify the dominant reaction channels. iso-Propanol dissociated by water loss to propene and by elimination of a methyl radical yielding a 1-hydroxyethyl radical at the conditions studied. The time-dependent mass spectra allowed secondary products to be identified along with the orders of appearance. Notably, peaks at m/z = 50 and 52 were observed providing insight into secondary reactions. These features have not been previously reported in propanol-pyrolysis literature.

Kim, John H. [Univ. of Michigan, Ann Arbor, MI (Un↗

Pop-up Langmuir probe diagnostic in the water cooled divertor of Wendelstein 7-X

The design, development, and successful implementation of pop-up Langmuir probes installed in the water-cooled divertor of W7-X are described. The probes are controlled by drive coils (actuators) installed behind the divertor plates. These drive coils make use of the magnetic field in W7-X to move the probe tips into and out of the plasma. The drive coils were installed in the vacuum vessel after extensively testing the durability of the coils and analyzing the criteria for safe operation. The probe design is carefully tailored for each of the 36 probe tips in order to be suitable for the different magnetic field configurations used in W7-X and ensure that the probes do not present leading edges to the magnetic flux tubes. An electronic bridge circuit is used for measurement to compensate for the effects of signal propagation time on the long cable lengths used. The diagnostic is integrated with the segment control of W7-X for automated operation and control of the diagnostic. The evaluation of the results from the plasma operation is presented after accounting for appropriate sheath expansion for negative bias voltage on the probes.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Design, Prototyping, Fabrication and Test of the Mu2e AC-Dipole Magnet

Fermilab Magnet Systems is building three High-frequency AC-Dipole Magnets for the Mu2e experiment at Fermilab. These magnets are composed of three single-loop one-meter-long ferrite loaded segments. The excitation consists of a copper tube, which is also used as a means for its cooling with the inherited challenges of Voltage and Frequency uncoupling. These magnets are designed to operate either at 300 kHz or 4.4 MHz via resonance tuning. Following the completion of the design, prototyping, and analysis phases, all ferrites and other components were procured, and the magnets were fabricated to meet vacuum compatibility requirements using strict procedures. Each magnet undergoes thorough baking and testing before being installed in the experiment. This paper discusses the magnets' role in proton background suppression as it represents a unique and essential device for the Mu2e experiment at Fermilab. We present the magnet design choices, modeling approach, and the challenges encountered during fabrication. Additionally, we outline the power supply driving mechanism, the testing that was performed, and our results.

Elementi, Luciano [Fermilab] (ORCID:00000002766372↗

Regolith-structure modeling

Early lunar missions have provided a basic understanding of the physical and strength properties of lunar regolith, which have been shown to differ from those of dry terrestrial granular soils. Lunar regolith is predominantly a fine sand of which nearly 40 percent can be characterized as silt with a particle size smaller than 100 micrometers. The top 10 to 20 cm of the regolith can be characterized as being in a loose to medium-loose state. The density of the regolith, however, rapidly increases below a depth of 20 cm. The highly irregular and angular shapes of the regolith particles tend to interlock and create relatively strong mechanical bonds that give the particulate mass substantial cohesive properties and smaller amounts of tensile strength properties. In addition, the friction angle of lunar regolith at medium to high densities is quite high and often exceeds 55 degrees. These known properties of lunar regolith have been matched in a terrestrially-manufactured analog known as Minnesota Lunar Simulant. A variety of experiments were conducted using this simulant to both verify existing information and generate new information on the physical and constitutive properties of lunar regolith. These experiments include maximum and minimum density determinations, specific mass of solids, grain-size distribution, conventional triaxial compression and extension, isotropic compression, one-dimensional compression, direct shear, and direct tension. Direct shear experiments were conducted under atmospheric and vacuum conditions. Results of the physical and strength experiments compare closely to results obtained from lunar missions. Results of simulant strength experiments performed in vacuum indicated no observable difference from results obtained in air. A test bed currently under study is one involving a regolith shield covering a first-generation human habitat module. It is understood that regolith in depths ranging from 3 to 5 meters is required for radiation shielding for habitation and workspace. The habitat module is treated as a rigid cylindrical tube with a smooth exterior. By making the cylinder rigid, a complex interaction problem is reduced to a situation where we can consider the support regolith and the shielding regolith as behaving independently of the structural properties of the cylindrical structure. Medium-dense lunar simulant was placed around a scaled model of the habitat module to provide a radiation shield. This embankment-type shield was constructed in relatively thin but fine layers by compacting, by mechanical vibratory means, layer upon layer of simulant placed adjacent to the horizontally-aligned cylinder. The slope angles were constructed at 55 degrees. The model described above was studied in a geotechnical centrifuge, which allows for the scaling of model dimensions to prototype dimensions by increasing the acceleration of gravity on the model. The deformation response can be scaled up to prototype dimensions to provide an assessment of the deformation patterns of the lunar structure. The actual process of local and/or global growth of instabilities or skip planes can also be observed.

Ko, Hon-Yim↗

Titanium-Water Thermosyphon Gamma Radiation Exposure and Results

Titanium-water thermosyphons are being considered for use in heat rejection systems for fission power systems. Their proximity to the nuclear reactor will result in some gamma irradiation. Noncondensable gas formation from radiation-induced breakdown of water over time may render portions of the thermosyphon condenser inoperable. A series of developmental thermosyphons were operated at nominal operating temperature under accelerated gamma irradiation, with exposures on the same order of magnitude as that expected in 8 years of heat rejection system operation. Temperature data were obtained during exposure at three locations on each thermosyphon: evaporator, condenser, and condenser end cap. Some noncondensable gas was evident; however, thermosyphon performance was not affected because the noncondensable gas was compressed into the fill tube region at the top of the thermosyphon, away from the heat rejecting fin. The trend appeared to be an increasing amount of noncondensable gas formation with increasing gamma irradiation dose. Hydrogen is thought to be the most likely candidate for the noncondensable gas and hydrogen is known to diffuse through grain boundaries. Post-exposure evaluation of one thermosyphon in a vacuum chamber and at temperature revealed that the noncondensable gas diffused out of the thermosyphon over a relatively short period of time. Further research shows a number of experimental and theoretical examples of radiolysis occurring through gamma radiation alone in pure water.

Sanzi, James, L.A↗

Heat pipe investigations

The OAO-C spacecraft has three circular heat pipes, each of a different internal design, located in the space between the spacecraft structural tube and the experiment tube, which are designed to isothermalize the structure. Two of the pipes are used to transport high heat loads, and the third is for low heat loads. The test problems deal with the charging of the pipes, modifications, the mobile tilt table, the position indicator, and the heat input mechanisms. The final results showed that the techniques used were adequate for thermal-vacuum testing of heat pipes.

Marshburn, J. P.↗

Calibration plan for ultraviolet spectrometer experiment S169

The calibration test equipment presented is employed to calibrate completely assembled and flight-ready Apollo Ultraviolet Spectrometers (UVS) consisting of a vacuum system in which the UVS can be installed. In it a premonochromator produces a monochromatic beam at any desired wavelength from a UV source. This beam can be focused by an adjustable transfer mirror to any point on the entrance slit of the UVS. The transfer mirror can also direct the beam to one or both of two absolutely calibrated reference photomultiplier tubes to determine the number of photons which enter the UVS. A movable mirror rhomb is also provided to intermittently monitor the number of photons in the beam when the beam is centered on the entrance slit.

Source record↗

Bioregenerative system components for microgravity

The goal of the class was to design, fabricate, and test prototype designs that were independent, yet applicable to a Closed Loop Life Support System. The three prototypes chosen were in the areas of agar plant growth, regnerative filtration, and microgravity food preparation. The plant growth group designed a prototype agar medium growth system that incorporates nutrient solution replenishment and post-harvest refurbishment. In addition, the unit emphasizes material containment and minimization of open interfaces. The second project was a filter used in microgravity that has the capability to clean itself. The filters are perforated plates which slide through a duct and are cleaned outside of the flow with a vacuum system. The air in the duct is prevented from flowing outside of the duct by a network of sliding seals. The food preparation group developed a device which dispenses and mixes ingredients and then cooks the mixture in microgravity. The dry ingredients are dispensed from a canister by a ratchet-operated piston. The wet ingredients are dispensed from plastic bags through tubing attached to a syringe. Once inside the mixing chamber, the ingredients are mixed using a collapsible whisk and then pushed into the cooking device.

Nevill, Gale E., Jr.↗

Portable Airflow Meter

Compact hand-held instrument measures airflow. Consists of hot-wire anemometer probe in flow-straightening tube that reduces swirling. Configuration developed empirically to reduce length of instrument to practical dimension for use and storage in confined space. Two versions of new straightener only 17 and 18 in. long. Weighs less than 8 lb. and readily stored on Space Shuttle, developed to measure airflow in waster-collection system during flight. Used on Earth to measure airflow in ventilation systems, vacuum cleaners, and the like.

Burgett, Frank A.↗

Penetrable Linear-Gap Pressure Seal

Pair of opposed inflatable rubber tubes allow object to be moved between them while maintaining pressure seal. Conceived for pressurized wind tunnel into which sensor probes inserted and positioned from outside. Probe moved along seal gap, pushed inward, and/or pulled outward while different pressures maintained inside and outside tunnel. Replaces bulky sealing unit. Adaptable to other situations in which objects must penetrate pressure walls and move along them. Works as well for vacuum chambers and for pressure vessels. Also applicable to dust seals not having to withstand differential pressures.

Trimarchi, Paul↗

A Heated Tube Facility for Rocket Coolant Channel Research

The capabilities of a heated tube facility used for testing rocket engine coolant channels at the NASA Lewis Research Center are presented. The facility uses high current, low voltage power supplies to resistively heat a test section to outer wall temperatures as high as 730 C (1350 F). Liquid or gaseous nitrogen, gaseous helium, or combustible liquids can be used as the test section coolant. The test section is enclosed in a vacuum chamber to minimize heat loss to the surrounding system. Test section geometry, size, and material; coolant properties; and heating levels can be varied to generate heat transfer and coolant performance data bases.

Green, James M.↗

Silicon Microleaks for Inlets of Mass Spectrometers

Microleaks for inlets of mass spectrometers used to analyze atmospheric gases can be fabricated in silicon wafers by means of photolithography, etching, and other techniques that are commonly used in the manufacture of integrated circuits and microelectromechanical systems. The microleaks serve to limit the flows of the gases into the mass-spectrometer vacuums to specified very small flow rates consistent with the capacities of the spectrometer vacuum pumps. There is a need to be able to precisely tailor the dimensions of each microleak so as to tailor its conductance to a precise low value. (As used here, "conductance" signifies the ratio between the rate of flow in the leak and the pressure drop from the upstream to the downstream end of the leak.) To date, microleaks have been made, variously, of crimped metal tubes, pulled glass tubes, or frits. Crimped-metal and pulled-glass-tube microleaks cannot readily be fabricated repeatably to precise dimensions and are susceptible to clogging with droplets or particles. Frits tend to be differentially chemically reactive with various gas constituents and, hence, to distort the gas mixtures to be analyzed. The present approach involving microfabrication in silicon largely overcomes the disadvantages of the prior approaches.

Harpold, Dan↗

Design and fabrication of the waveguide Iris couplers for the Spallation Neutron Source drift tube linac

The Spallation Neutron Source (SNS) employs six cavities in the Drift Tube Linac (DTL) section to accelerate the H- ion beam to 87MeV. Each cavity is energized by a 2.5MW peak power klystron at 402.5MHz using rapid tapered waveguide iris couplers. All six original iris couplers have been in operation without replacement for over two decades. The increased RF power demands of the Proton Power Upgrade (PPU) project and operational problems, including arcing, temperature excursions, and vacuum bursts, have prompted the development of new iris coupler spares. The original iris couplers were made of GlidCop material, which is known to be mechanically strong and thermally stable, but is porous, expensive, and difficult to use in fabrication. To overcome these problems, the new spare couplers use Oxygen-Free Copper (OFC) and stainless steel (SS). This paper will discuss the mechanical, thermal and RF design, as well as challenges in the final coupler fabrication.

Lee, Sung-Woo↗

Exploration Extravehicular Mobility Unit (xEMU) Lunar Boot Chamber B Thermal Vacuum Testing Results

NASA’s Exploration Extravehicular Mobility Unit (xEMU) is the government reference next-generation spacesuit design and is engineered to protect astronauts from extreme lunar environmental temperatures. To evaluate the xEMU hardware thermal requirements, the xEMU Testing Team invented, designed, and executed a dual-suit, uncrewed thermal vacuum (TVAC) test at Johnson Space Center’s (JSC) Chamber B. This paper details the test methodology, hardware setup, and results from the xEMU lunar boots. Eleven unique thermal profiles were tested including both cold and hot environmental cases over the course of five continuous days of testing. This paper will address only the cold environment testing results. The radiative thermal environment was controlled through exposure to liquid-nitrogen shrouds on the chamber walls and through a heater cage surrounding the boots. Notably, the xEMU boots also contacted the liquid-nitrogen chilled floor inside of Chamber B, which provided a conduction pathway to simulate the thermal effects of the lunar surface. Test hardware was developed to extend the water tubing from the Liquid Cooling Ventilation Garment (LCVG) into the boots to set the internal thermal boundary nominally provided by the astronaut’s foot. Thirty-three temperature sensors were used to collect data in critical locations in the xEMU boot assembly as well as for calorimetry to determine heat flux to and from the boots. This paper will document the testing results and provide a high-level interpretation of the testing results. To conclude, this paper will address possible forward work and knowledge gaps present in lunar boot thermal performance and testing.

xEMU↗

Titanium-Water Thermosyphon Gamma Radiation Effects and Results

Titanium-water thermosyphons are being considered for use in heat rejection systems for fission power systems. Their proximity to the nuclear reactor will result in some exposure to gamma irradiation. Non-condensable gas formation from radiation may breakdown water over time and render a portion of the thermosyphon condenser inoperable. A series of developmental thermosyphons were operated at nominal operating temperature with accelerated gamma irradiation exposures on the same order of magnitude that is expected in eight years of heat rejection system operation. Temperature data were obtained during exposure at three locations on each thermosyphon; evaporator, condenser, and condenser end cap. Some non-condensable gas was evident, however thermosyphon performance was not affected because the non-condensable gas was compressed into the fill tube region at the top of the thermosyphon, away from the heat rejecting fin. The trend appeared to be an increasing amount of non-condensable gas formation with increasing gamma irradiation dose. Hydrogen is thought to be the most likely candidate for the non-condensable gas and hydrogen is known to diffuse through grain boundaries. Post-exposure evaluation of selected thermosyphons at temperature and in a vacuum chamber revealed that the non-condensable gas likely diffused out of the thermosyphons over a relatively short period of time. Further research shows a number of experimental and theoretical examples of radiolysis occurring through gamma radiation alone in pure water.

Sanzi, James L.↗

Hydrogen-Helium shock Radiation tests for Saturn Entry Probes

This paper describes the measurement of shock layer radiation in Hydrogen/Helium mixtures representative of that encountered by probes entering the Saturn atmosphere. Normal shock waves are measured in Hydrogen-Helium mixtures (89:11% by volume) at freestream pressures between 13-66 Pa (0.1-0.5 Torr) and velocities from 20-30 km/s. Radiance is quantified from the Vacuum Ultraviolet through Near Infrared. An induction time of several centimeters is observed where electron density and radiance remain well below equilibrium. Radiance is observed in front of the shock layer, the characteristics of which match the expected diffusion length of Hydrogen.

Shock Tube↗

High voltage solar cell power generating system for regulated solar array development

A laboratory solar power system regulated by on-panel switches has been delivered for operating high power (3 kw), high voltage (15,000 volt) loads (communication tubes, ion thrusters). The modular system consists of 26 solar arrays, each with an integral light source and cooling system. A typical array contains 2560 series-connected cells. Each light source consists of twenty 500 watt tungsten iodide lamps providing plus or minus 5 per cent uniformity at one solar constant. An array temperature of less than 40 C is achieved using an infrared filter, a water cooled plate, a vacuum hold-down system, and air flushing.

Levy, E., Jr.↗

Hollow Fiber Flight Prototype Spacesuit Water Membrane Evaporator Design and Testing

The spacesuit water membrane evaporator (SWME) is being developed to perform thermal control for advanced spacesuits and to take advantage of recent advances in micropore membrane technology. This results in a robust heat-rejection device that is potentially less sensitive to contamination than is the sublimator. The Membrana Celgard X50-215 microporous hollow-fiber (HoFi) membrane was selected after recent extensive testing as the most suitable candidate among commercial alternatives for continued SWME prototype development. The current design was based on a previous design that grouped the fiber layers into stacks, which were separated by small spaces and packaged into a cylindrical shape. This was developed into a full-scale prototype consisting of 14,300 tube bundled into 30 stacks, each of which is formed into a chevron shape and separated by spacers and organized into three sectors of 10 nested stacks. The new design replaced metal components with plastic ones, and has a custom built flight like backpressure valve mounted on the side of the SWME housing to reduce backpressure when fully open. The spacers that provided separation of the chevron fiber stacks were eliminated. Vacuum chamber testing showed improved heat rejection as a function of inlet water temperature and water vapor backpressure compared with the previous design. Other tests pushed the limits of tolerance to freezing and showed suitability to reject heat in a Mars pressure environment with and without a sweep gas. Tolerance to contamination by constituents expected to be found in potable water produced by distillation processes was tested in a conventional way by allowing constituents to accumulate in the coolant as evaporation occurs. For this purpose, the SWME cartridge has endured an equivalent of 30 EVAs exposure and demonstrated minimal performance decline.

Bue, Grant↗