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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 451 records · Page 25
All sourcesNASA NTRSDOE OSTI
NASA NTRS1980

Space fabrication demonstration system

The development effort on the composite beam cap fabricator was completed within cost and close to abbreviated goals. The design and analysis of flight weight primary and secondary beam builder structures proceeded satisfactorily but remains curtailed until further funding is made available to complete the work. The induction fastening effort remains within cost and schedule constraints. Tests of the LARC prototype induction welder is continuing in an instrumented test stand comprised of a Dumore drill press (air over oil feed for variable applied loads) and a dynamometer to measure actual welding loads. Continued testing shows that the interface screening must be well impregnated with resin to ensure proper flow when bonding graphite-acrylic lap shear samples. Specimens prepared from 0.030 inch thick graphite-polyethersulfone are also available for future induction fastening evaluation.

Source record↗
NASA NTRS1984

Structurally stable, thin silicon solar cells

A fabrication process for structurally stable thin solar cell wafers that produce good power output after irradiation is described. The fabrication process is as follows. A 6 mil, circular wafer is oxidized on both sides. One side is then patterned with a rectangular array of holes in the oxide that are nominally 75 mils square and separated by 2 mil spacings. Wells are then etched into the silicon with KOH to a depth of 4 mils, leaving a 2 mil, unetched thickness. Two areas on the surface are left unetched to provide pads for bonding or testing. All oxide is then removed and the rest of the processing is normal; the unetched face is used as the illuminated face. When all other processing is complete, a 2 X 2 cm cell is sawed from the starting wafer leaving a border that is approximately 10 mils wide. The effective thickness, determined by weighing an unmetallized sample, of such a cell is about 2.4 mil.

Arndt, R. A.↗
NASA NTRS1986

Determination of the optical thickness of clouds from reflected solar radiation measurements

A procedure is presented for inferring cloud optical thickness from reflected solar radiation measurements. Asymptotic expressions are defined for the reflection and transmission functions of optically thick atmospheres, noting that the reflection function sensitivity to cloud optical thickness is highest with minimal surface albedo. Attention is also given to the dependence of the optical thickness on the cloud asymmetry factor. Sample results are provided from several high altitude aircraft flights to determine the reflection function of clouds.

King, M. D.↗
NASA NTRS1988

Increased effective barrier heights in Schottky diodes by molecular-beam epitaxy of CoSi2 and Ga-doped Si on Si(111)

Increasing the effective Schottky-barrier height of epitaxial CoSi2/Si(111) diodes by the use of thin, highly doped Si layers in close proximity to the metal-semiconductor interface has been studied. Intrinsic Si, Si doped by coevaporation of Ga, and epitaxial CoSi2 layers have all been grown in the same molecular-beam epitaxy system. Current-voltage and photoresponse characterization yield barrier heights ranging from 0.61 eV for a sample with no p(+) layer to 0.89 eV for a sample with a 20-nm-thick p(+) layer. These results are compared to theoretical values based on a one-dimensional solution of Poisson's equation under the depletion approximation.

Fathauer, R. W.↗
NASA NTRS1994

Antarctic weathering of the CK chondrites EET90004, 90007, and 90022: Nickel and sulfur mobility

CK chondrites are a relatively new class of carbonaceous chondrite that have been described in the literature. Most meteorites that comprise the CK group are restricted to Antarctic finds; therefore terrestrial weathering processes can influence the geochemical records contained within these chondrites. The paired CK chondrites EET90004, 90007, and 90022 share not only a common heritage but similar weathering histories since all three meteorites were found on Antarctic ice covered with thick evaporative coatings. Additional material has grown on these samples during curation at the Antarctic Meteorite Lab at JSC, NASA. At present, efflorescence up to a millimeter thick coats the surface of EET90004 and 90022, with less material coating EET90007. The chemistry, mineralogy, and isotopic composition of efflorescence on EET90004 and 90022, described here, provide valuable information regarding the fate of meteoritic components in the Antarctic environment.

Romanek, C. S.↗
NASA NTRS2007

RF Performance of Membrane Aperture Shells

This paper provides an overview of recent results establishing the suitability of Membrane Aperture Shell Technology (MAST) for Radio Frequency (RF) applications. These single surface shells are capable of maintaining their figure with no preload or pressurization and minimal boundary support, yet can be compactly roll stowed and passively self deploy. As such, they are a promising technology for enabling a future generation of RF apertures. In this paper, we review recent experimental and numerical results quantifying suitable RF performance. It is shown that candidate materials possess metallic coatings with sufficiently low surface roughness and that these materials can be efficiently fabricated into RF relevant doubly curved shapes. A numerical justification for using a reflectivity metric, as opposed to the more standard RF designer metric of skin depth, is presented and the resulting ability to use relatively thin coating thickness is experimentally validated with material sample tests. The validity of these independent film sample measurements are then confirmed through experimental results measuring RF performance for reasonable sized doubly curved apertures. Currently available best results are 22 dBi gain at 3 GHz (S-Band) for a 0.5m aperture tested in prime focus mode, 28dBi gain for the same antenna in the C-Band (4 to 6 GHz), and 36.8dBi for a smaller 0.25m antenna tested at 32 GHz in the Ka-Band. RF range test results for a segmented aperture (one possible scaling approach) are shown as well. Measured antenna system actual efficiencies (relative to the unachievable) ideal for these on axis tests are generally quite good, typically ranging from 50 to 90%.

Flint, Eirc M.↗
NASA NTRS2011

An Efficient Monte Carlo Method for Modeling Radiative Transfer in Protoplanetary Disks

Monte Carlo methods have been shown to be effective and versatile in modeling radiative transfer processes to calculate model temperature profiles for protoplanetary disks. Temperatures profiles are important for connecting physical structure to observation and for understanding the conditions for planet formation and migration. However, certain areas of the disk such as the optically thick disk interior are under-sampled, or are of particular interest such as the snow line (where water vapor condenses into ice) and the area surrounding a protoplanet. To improve the sampling, photon packets can be preferentially scattered and reemitted toward the preferred locations at the cost of weighting packet energies to conserve the average energy flux. Here I report on the weighting schemes developed, how they can be applied to various models, and how they affect simulation mechanics and results. We find that improvements in sampling do not always imply similar improvements in temperature accuracies and calculation speeds.

radiative transfer↗
DOE OSTI2023

Hardware, methodology and applications of 2 + D backscatter Mössbauer spectroscopy with simultaneous x-ray and γ-ray detection

Abstract A unique method is presented for the acquisition and analysis of 57 Fe backscatter Mössbauer spectra with simultaneous detection of the resonant 14.4 keV γ -rays and the characteristic 6.4 keV x-rays, using a custom-built multi-parameter analyser constructed on the basis of commercial analogue to digital converters and high-speed digital latches. The system allows for the simultaneous registration of Doppler-modulation velocities and photon energies, with up to 4096 and 8192 digital channels respectively. This arrangement is in contrast to most related systems, which detect at a single narrow energy window per detector. Samples of arbitrary atomic structure, morphology and surface topography can be studied without altering the setup or the analysis procedure, provided that the samples are at least micrometre sized. The hardware and software that are used to acquire data with minimal dead time are described and the custom and self-contained methods for post-measurement energy discrimination, background correction and velocity-axis folding are discussed. The data are fit using a general Hamiltonian model for the nuclear energy levels of 57 Fe and a quantum mechanical description of the angular momentum coupling is utilised, with consideration of the crystalline and chemical disorder of the sample under examination. Three examples of distinct magnetic systems, with thicknesses ranging from 5 μ m to 6 mm, that were studied using this method are presented, these are: an amorphous CoFeB-based ribbon with ultra-soft coercivity for high-frequency applications, magnetically hard Nd-Fe-B thick films on Si substrates, examined in both as-deposited and annealed states, and a sample from the nickel-rich iron meteorite NWA 6259 that contains the atomically ordered, elevated coercivity, L 1 0 phase of FeNi, tetrataenite. The wide applicability and usefulness of this method is thus demonstrated on three distinct sample morphologies that required little to no surface preparation prior to examination.

Engineering↗
NASA NTRS1990

A sensitive 10-micron search for emission arising from circumstellar dust associated with solar-type pre-main-sequence stars

The presence and evolutionary timescales of circumstellar disks surrounding solar-type premain-sequence stars are studied using excess IR radiation above photospheric levels. The analysis is based on optical photometry, published near-IR fluxes, IRAS fluxes, and 10-micron flux measurements of 20 stars in Taurus-Auriga obtained with the NASA IR telescope facility. About half of the stars with ages less than 3 Myr show excess 2.2 and 10 micron emission, consistent with emission from optically thick disks extending inward to the stellar surface. At ages of about 10 Myr, less than 10 percent of the sample stars show evidence of dust emission from optically thick disks. It is concluded that the timescale over which disks survive as IR-luminous, optically thick structures is less than 10 Myr. Also, evidence for inner holes in premain-sequence stars surrounded by optically thick disks is discussed.

Skrutskie, M. F.↗
DOE OSTI2023

Experimental review of the performances of protective coatings for interconnects in solid oxide fuel cells

Ferritic stainless-steel interconnects are used in solid oxide fuel cells; however, coatings are required to improve their performance. Although several types of coatings have been proposed, they have been scarcely investigated under similar conditions. This study compares the characteristics of uncoated Crofer 22 APU and eight different coatings on Crofer 22 APU for up to 3,000 hours at 800°C. The coatings were deposited at various research laboratories around the world, and the experiments were performed at Chalmers University of Technology, Sweden. Cross-sections of the samples were analysed using scanning electron microscopy and energy-dispersive x-ray spectroscopy. The (Co,Mn)-based coated steels showed more than 50-fold lower chromium evaporation and at least 3 times thinner Cr 2 O 3 scale thickness compared to uncoated steel. The coated steel samples showed lower area-specific resistance (ASR) values than the uncoated steel after 3,000 hours of exposure, irrespective of the coating thickness, composition and deposition method.

25 ENERGY STORAGE↗
NASA NTRS2011

Handling Heavenly Jewels - 35 Years of Antarctic Meteorite Processing at Johnson Space Center

The ANSMET program began in 1976, and since that time more than 18,000 meteorites have been processed in the Meteorite Processing Lab at Johnson Space Center in Houston, TX[1]. The meteorites are collected and returned to JSC on a freezer truck and remain frozen until they are initially processed. Initial Processing of Meteorites: Initial processing involves drying the meteorites in a nitrogen glove box for 24 to 48 hours, photographing, measuring, weighing and writing a description of the interior and exterior. The meteorite is broken and a representative sample is sent to the Smithsonian Institution for classification. Newsletter & Requests: Once initial processing has been complete and the meteorites have been classified, the information is published in the Antarctic Meteorite Newsletter[2,3]. The newsletter is published twice yearly and is sent electronically to researchers around the world and is also available on line. Researchers are asked to fill out a request form and submit it to the Meteorite Working Group secretary. All sample requests will be reviewed by either the meteorite curator or the Meteorite Working Group de-pending on the type of meteorite and the research being conducted. Processing for Sample Requests: In the meteorite processing lab, meteorite samples are prepared several different ways. Most samples are prepared as chips obtained by use of stainless steel chisels in a chipping bowl or rock splitter. In special situations where a researcher needs a slab the meteorite samples can be bandsawed in a dry nitrogen glove box with a diamond blade, no liquids are ever introduced into the cabinet. The last type of sample preparation is thin/thick sections. The meteorite thin section lab at JSC can prepare standard 30-micron thin sections, thick sections of variable thickness (100 to 200 microns), or demountable sections using superglue. Information for researchers: It is important that re-searchers fill the sample request form completely, in order to make sure the meteorite is processed correctly[4]. Re-searchers should list any special requirements on the form, i.e. packaging of samples (poly vs. stainless), thick sections and thickness needed, superglue needed, interior chips, exterior chips, fusion crust, contamination issues, all concerns should be listed so processing can be done accurately and any concerns the researcher has can be addressed be-fore the meteorites are broken.

Satterwhite, C. E.↗
NASA NTRS2018

Magnetic Properties of Fe-49Co-2V Alloy and Pure Fe at Room and Elevated Temperatures

The National Aeronautics and Space Administration (NASA) has a need for soft magnetic materials for fission power and ion propulsion systems. In this work the magnetic properties of the soft magnetic materials Hiperco 50 (Fe-49wt%Cr-2V) and CMI-C (commercially pure magnetic iron) were examined at various temperatures up to 600 C. Toroidal Hiperco 50 samples were made from stacks of 0.35 mm thick sheet, toroidal CMI-C specimens were machined out of solid bar stock, and both were heat treated prior to testing. The magnetic properties of a Hiperco 50 sample were measured at various temperatures up to 600 C and then again after returning to room temperature; the magnetic properties of CMI-C were tested at temperatures up to 400 C. For Hiperco 50 coercivity decreased as temperature increased, and remained low upon returning to room temperature; maximum permeability improved (increased) with increasing temperature and was dramatically improved upon returning to room temperature; remanence was not significantly affected by temperature; flux density at H = 0.1 kA/m increased slightly with increasing temperature, and was about 20% higher upon returning to room temperature; flux density at H = 0.5 kA/m was insensitive to temperature. It appears that the properties of Hiperco 50 improved with increasing temperature due to grain growth. There was no significant magnetic property difference between annealed and aged CMI-C iron material; permeability tended to decrease with increasing temperature; the approximate decline in the permeability at 400 C compared to room temperature was 30%; saturation flux density, B(sub S), was approximately equal for all temperatures below 400 C; B(sub S) was lower at 400 C.

De Groh, Henry C., III↗
NASA NTRS2004

Miniature Blimps for Surveillance and Collection of Samples

Miniature blimps are under development as robots for use in exploring the thick, cold, nitrogen atmosphere of Saturn's moon, Titan. Similar blimps can also be used for surveillance and collection of biochemical samples in buildings, caves, subways, and other, similar structures on Earth. The widely perceived need for means to thwart attacks on buildings and to mitigate the effects of such attacks has prompted consideration of the use of robots. Relative to rover-type (wheeled) robots that have been considered for such uses, miniature blimps offer the advantage of ability to move through the air in any direction and, hence, to perform tasks that are difficult or impossible for wheeled robots, including climbing stairs and looking through windows. In addition, miniature blimps are expected to have greater range and to cost less, relative to wheeled robots.

Jones, Jack↗
NASA NTRS1994

Corrosion Detection in Airframes Using a New Flux-Focusing Eddy Current Probe

A new flux-focusing eddy current probe was recently developed at NASA Langley Research Center. The new probe is similar in design to a reflection type eddy current probe, but is unique in that it does not require the use of an impedance bridge for balancing. The device monitors the RMS output voltage of a pickup coil and, as a result, is easier to operate and interpret than traditional eddy current instruments. The unique design feature of the probe is a ferromagnetic cylinder, typically 1020 steel, which separates a concentrically positioned drive and pickup coil. The increased permeability of the steel causes the magnetic flux produced by the drive coil to be focused in a ring around the pickup coil. At high frequencies the eddy currents induced in both the sample and the cylinder allow little or no flux to link with the pickup coil. This results in a self-nulling condition which has been shown to be useful for the unambiguous detection of cracks in conducting materials. As the frequency is lowered the flux produced by the drive coil begins to link with the pickup coil causing an output which, among other things, is proportional to the thickness of the test specimen. This enables highly accurate measurements of the thickness of conducting materials and helps to facilitate the monitoring of thickness variations in a conducting structure such as an aircraft fuselage. Under ideal laboratory conditions the probe can sense thickness changes on the order of 1% as illustrated. However, this is highly dependent upon the thickness, and the geometric complexity of the sample being tested and for practical problems the sensitivity is usually much less. In this presentation we highlight some of the advantages and limitations in using the probe to inspect aircraft panels for corrosion and other types of material nonuniformities. In particular, we present preliminary results which illustrate the probes capabilities for detecting first and second layer corrosion in aircraft panels which may contain air gaps between the layers. Since the probe utilized eddy currents its corrosion detection capabilities are similar to convectional eddy current techniques, but the new probe is much easier to use.

Fulton, James P.↗
DOE OSTI2023

Quantifying Pore Morphology in Spray-Formed Tantalum Using X-ray Micro-computed Tomography

In order to establish quantitative process–structure–property relationships in thermal spray coatings, a robust framework for defining (micro)structural characteristics is needed. Here, we present a quantitative characterization of the three-dimensional morphology of porosity in spray-formed tantalum samples based on high-resolution X-ray micro-computed tomography. Using synchrotron facilities, we acquired dozens of high-resolution scans, enabling a statistically meaningful comparison across multiple samples, different regions within samples, and spray processes. We quantify the spatial distribution, size, and topology of porous inclusions, with a significant focus on variability across samples and different spray processes (plasma and cold sprayed), as well as sensitivity to image segmentation and resolution. Based on a typical segmentation, we report porosities ranging from 0.9 to 1.7 pct for all samples tested, with significant sensitivity due to image segmentation resulting in estimates as low as 0.6 pct and as high as 4.8 pct. For the complex pore space morphology observed in these materials, we argue that a conventional analysis based on identifying individual pores is not well suited, and propose an alternative approach based on morphological metrics with a rich history in porous media literature, such as spatial correlations, local pore thickness, and scale-dependent sub-sampling. Spatial correlations indicate anisotropic splat structures, but only mildly anisotropic pores. Various measures of pore size show a wide distribution of sizes, ranging from sub-micron to 10-micron length scales. Scale-dependent variations in porosity suggest that representative volumes of several hundred microns are required for convergence of morphological metrics, with larger volumes for cold-spray materials. This work provides a robust quantitative basis for describing three-dimensional pore structure in thermal spray coatings.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Hydrothermal corrosion of 2nd generation FeCrAl alloys for accident tolerant fuel cladding

As part of an effort to develop advanced fuel cladding for use in light water reactors, several FeCrAl alloys have been developed at Oak Ridge National Laboratory. A second generation of these alloys bearing additional alloying elements over the previously tested model alloys were tested in boiling water reactor (BWR) conditions to determine their resistance to hydrothermal corrosion. Coupons with alloy compositions Fe–10Cr–6Al–2Mo, Fe–13Cr–5Al–2Mo, Fe–13Cr–6Al–2Mo, Fe–13Cr–7Al–2Mo, and Fe–13Cr–5Al–2Mo–1Nb were tested in normal water chemistry (NWC) and hydrogen water chemistry (HWC) for 9 months in continuously refreshing autoclaves. Commercial FeCrAl alloy APMT and Zircaloy-2 were also tested for comparison. Among samples exposed to HWC, Fe–13Cr–7Al–2Mo performed worst with an average mass loss of 1.3 mg/cm2 over 9 months. This mass loss represents an estimated thickness loss of approximately 60 μm over 6 years. Samples exposed to NWC had very small mass losses of less than 0.15 mg/cm2 or mass gains up to 0.05 mg/cm2. Based on the results of this testing, the 2nd generation FeCrAl alloys tested exhibit low wall thickness loss and are suitable in terms of corrosion resistance for use as LWR cladding in BWR-HWC and BWR-NWC under normal operating conditions.

Raiman, Stephen↗
NASA NTRS1992

Superconductivity devices: Commercial use of space

High T sub C superconducting thick film were prepared by a screen printing process. Y-based (YBa2Cu3O(7-x) superconducting thick film were printed on 211/Al2O3, SNT/Al2O3, and YSZ substrates. Because of poor adhesion of the superconductor thick films to 211/Al2O3 and SNT/Al2O3 substrates, relatively low T sub C and J sub C values were obtained from the films printed on these substrates. Critical temperatures (T sub C) of YBa2Cu3O(7-x) thick films deposited on 211/Al2O3 and SNT/Al2O3 substrates were about 80 K. The critical current densities (J sub C) of these films were less than 2 A/sq cm. Higher T sub C and J sub C YBa2Cu3O(7-x) thick films were printed on YSZ substrates. A YBa2Cu3O(7-x) thick film with T sub C=86.4 and J sub C= 50.4 A/sq cm was prepared by printing the film on YSZ substrate and firing at 990 C for 10 minutes. Multiple-lead samples were also prepared on the YSZ substrates. The multiple-lead samples showed lower T sub C and/or J sub C values than those of the plain samples. The electrical properties of YBa2Cu3O(7-x) thick films were determined by the microstructures of the films. The YBa2Cu3O(7-x) thick films printed on the YSZ substrates, which had the best properties among the films printed on the three different kinds of substrates, had the highest density and the best particle interconnection. The YBa2Cu3O(7-x) thick films with preferred orientation in (001) direction were obtained on the YSZ substrates. Cracks, which retard the properties of the films, were found from the films deposited on the YSZ substrates. Currently, a MSZ (Magnesium Stabilized Zirconia) substrate, which had higher thermal expansion coefficient than the YSZ substrate, is used as substrate for the YBa2Cu3O(7-x) thick film in order to eliminate the cracks on the film. Bi-based superconductor thick films were printed on polycrystalline MgO and YSZ substrates. Interactions between BSCCO thick films and the YSZ substrates were observed. Various buffer layer materials were applied onto the substrates in order to avoid the interactions between the BSCCO thick films and the ZrO2-based substrates. So far, a BSCCO printed on MgO substrate with T Sub C=89K was obtained. The J sub C of the film was lower than 0.1 A/sq cm by reason of poor interconnectivity of the BSCCO particles.

Haertling, Gene↗