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NASA NTRS2020

Contributions of Antarctic Meteorites in Understanding the Inner Solar System: The Interplay of Samples and Paradigms

Antarctic meteorites number nearly 50,000 in world collections, and have provided significant contributions to our understanding of the Solar System. Collections include samples from the Moon, Mars, asteroid 4 Vesta, as well as dozens or even hundreds of other bodies from the asteroid belt or near Earth objects. This 50th anniversary of the Japanese Antarctic finds from Yamato Mountains offers a chance to reflect on the contributions to planetary science. Antarctic meteorites have provided fundamental constraints on Solar System science in three major roles: A) unique samples of bodies (Mars and Vesta), B) complementary samples of bodies (Moon, together with Apollo and Luna), and C) foundational samples that have expanded the variety of known and documented materials in our sample collections. These have all contributed to the ideas and paradigms that have influenced the understanding of our Solar System.

Righter, K.↗
NASA NTRS2020

Applicability and Utility of the Astromaterials X-Ray Computed Tomography Laboratory at Johnson Space Center

The Astromaterials Acquisition and Curation Office at NASA’s Johnson Space Center is responsible for curating all of NASA’s astromaterial sample collections (i.e. Apollo samples, Luna Samples, Antarctic Meteorites, Cosmic Dust Particles, Microparticle Impact Collection, Genesis solar wind atoms, Stardust comet Wild-2 particles, Stardust interstellar particles, and Hayabusa asteroid Itokawa particles) [1-3]. To assist in sample curation and distribution, JSC Curation has recently installed an X-ray computed tomography (XCT) scanner to visualize and characterize samples in 3D. [3] describes the instrumental set-up and the utility of XCT to astromaterials curation. Here we describe some of the current and future projects and illustrate the usefulness of XCT in studying astromaterials.

Eckley, S. A.↗
NASA NTRS2018

A Novel Sensing Tether for Rovers

Luna has extended the length of its fiber optic shape sensing technology out to a continuous, high-fidelity measurement of a 100-meter sensor, creating a novel concept for a self-monitoring tether for robotic exploration. This tether is capable of measuring its own tension, curvature, and full 3-D shape along its entire length as it is deployed by a robotic rover. Using Optical Frequency Domain Reflectometry (OFDR) and the Rayleigh scatter signature to sense the state of a customized multicore optical fiber, the new technology is lightweight, compact, and immune to electromagnetic interference. Results are presented from tests with a 50-meter tether on the Axel Rover at JPL’s Mars Yard testing ground.

Kominsky, Daniel↗
NASA NTRSDate not supplied

Debris Avoidance and Phase Change Maneuvers in Near Rectilinear Halo Orbits

Over the course of its lifetime, Ga teway may execute excursions from itsba seline NRHO that include short-lead maneuvers to avoid other spacecraft or debris objects or long-lea d rephasing within the NRHO to support rendezvous or other mission objectives. The dynamical cha racteristics of the NRHO a re distinct from those of low Ea rth a nd low luna r orbits due to the simulta neous gra vitational influences of the Ea rth a nd Moon. Thus, new a pproaches for executing debris a voidance ma neuvers a nd repha sing ma neuversa re necessary. The current investiga tion proposesmethods for designing low-cost DAMs with short-lead pla nning time a s well a s rephasing maneuvers with many months of advance notice.

Diane C Davis↗
NASA NTRSDate not supplied

Lunar Exploration in the 21st Century

The Apollo and Luna missions to the Moon in the 1960s and 1970s unambiguously established that the Moon is useful, interesting, and attainable. Starting with the Clementine mission in 1994, Moon has been the focus of a new series of increasingly ambitious science and exploration missions from many nations. In 2025, it is expected that the Artemis III mission will be the first human landing on the Moon in the 21st Century, eventually leading to the establishment of a field station at the lunar south pole. In the United States, lunar missions have been guided by a series of community documents that established lunar science and exploration objectives. In this talk, I will summarize the long-established science goals of US lunar exploration missions as expressed in foundational community documents and the processes used to establish these science goals.

Samuel Lawrence↗
NASA NTRSDate not supplied

Mineralogical, Elemental, and Tomographic Reconnaissance Investigation for CLPS (METRIC): A Proposed Mission to the Lunar South Pole-Aitken Basin

The global Lunar Magma Ocean (LMO) hypothesis is based on analyses of ferroan anorthosites (FAN), magnesian plutonic rocks (Mg-suite), and KREEPy (Potassium - K; Rare Earth Elements - REE; Phosphorous - P) material present at the Apollo landing sites and the assumed global distribution of these lithologies. However, orbital spacecraft data over the last two decades have highlighted that the location of the Apollo missions within and near the Procellarum KREEP Terrane (PKT) is compositionally anomalous and not representative of the entire lunar surface and suggests that Apollo samples provide a biased view of the Moon. Further, meteorites, which originate from random areas on the lunar surface, including those not visited by Apollo, Luna, or Chang’E-5, provide complementary datasets that reveal a more complex lunar formation and evolution than the simple LMO onion skin model. While many recent investigations support and refine the LMO model, other recent studies have questioned whether this mechanism alone is responsible for the primordial differentiation of the Moon. Thus, relating the distinct and asymmetrically distributed geochemical terranes on the Moon, especially KREEP which is a predicted global LMO product, to lunar formation and differentiation remains a fundamental goal of lunar science. The South Pole-Aitken (SPA) impact carved a two-and-a-half thousand-kilometer basin into the Moon’s ancient crust, excavating material from as deep as the upper mantle. Orbital remote sensing of the basin indicates compositions with elevated thorium (Th) contents and unique mineralogies that provide a window into early lunar structure and LMO processes. We propose to land a powerful characterization laboratory at Birkeland crater on the far side of the Moon–where Th-rich SPA ejecta have been re-exposed near the surface–in order to address outstanding questions about the evolution of the Moon.

K M Cannon↗
NASA NTRSDate not supplied

Applicability of Micro X-Ray Fluorescence Spectroscopy to Astromaterials Curation and Research

Introduction: The Astromaterials Acquisition and Curation Office at NASA’s Johnson Space Center (JSC) curates NASA’s astromaterial sample collections which includes: Apollo samples, Luna samples, Ant-arctic meteorites, cosmic dust particles, microparticle impacts into space-flown materials, Genesis solar wind atoms, Stardust comet Wild-2 particles, Stardust inter-stellar particles, Hayabusa asteroid Itokawa particles, Hayabusa 2 asteroid Ryugu particles, and future OSIRIS-Rex asteroid Bennu particles (landing in Sep-tember, 2023) [1–3]. To enhance JSC’s advanced cu-ration capabilities, we have recently installed a high-performance micro-X-ray fluorescence (µXRF) spec-trometer to assist in sample characterization through rapid, non-destructive, in-situ elemental analyses that do not require the sample preparation protocols (i.e., polishing and carbon-coating) commonly needed for electron beam analyses. With this new instrument, we are capable of detecting all elements down to carbon in a variable-pressure or He-purged chamber for anal-ysis of a wide range of sample types. Here we describe the instrumental set-up, capabilities, and applicability of µXRF analysis to astromaterials curation and re-search. Instrumentation and Methodology: The X-ray fluorescence and computed tomography lab (X-FaCT) lab at JSC is now equipped with a Bruker M4 Tornado Plus µXRF (Fig. 1). This system is an energy-dispersive x-ray spectrometer equipped with two 60 mm2 silicon drift detectors (SDD) that are able to be used simulta-neously for output count rates ~500,000 cps. New light element windows allow detecting and analyzing the entire elemental range from carbon to americium. Two x-ray tubes (micro-focus Rh with polycapillary lenses and W with collimators of 0.5, 1.0, 2.0, and 4.5 mm) with max excitation parameters of 50 kV, 30 W and 50 kV, 40 W, respectively, allow for more flexibility of the analysis of high energy lines. The motorized X-Y-Z stage has a mapping range of 190 x 160 mm and can support samples up to 7 kg (~15.5 lbs) and a height of 120 mm [4]. Analytical modes include elemental analysis (down to ~20 µm spot size) via point, line, or area of bulk materials (rock surfaces, thin sections, thick sections, etc.) as well as coating analysis (determination of thickness and composition) of samples. This system has a variable vacuum chamber (1 mbar to 1 atm) that is also equipped with a He-purge system which accommodates vacuum sensitive samples while still allowing detection of light elements at atmospheric pressure. Utility and Applicability of µXRF in Astro-materials research and exploration science (ARES): Elemental analysis using µXRF is commonly em-ployed for both terrestrial and planetary geological science disciplines [5]. It is especially useful for analy-sis of astromaterials given the limited sample prepara-tion required, which is not feasible for certain materi-als. Here we show select applications of µXRF anal-yses of astromaterials that can, have, and will be done at JSC’s X-FaCT lab. Point analysis: In-situ spot analyses (~20 µm spot size) on a cut slab of Martian meteorite NWA 10922 allowed for the discovery, qualitative elemental analy-sis and determination of different feldspar minerals [6]. These point analyses served as an effective prelim-inary step for subsequent quantitative analyses. Ana-lytical standards can be employed for more accurate quantification of µXRF spot analyses. Area analysis: This analytical mode measures all detectable elements (from C to Am) at each pixel (>5 µm pixel size) in a user-defined area. The results are shown as elemental maps which can be extracted as 16-bit TIFF’s for further data processing. In Fig. 2. we show elemental distribution maps of the high-Ti basalt 73001,531 that have been processed using ImageJ software. From these maps you can accurately and quickly (this map took ~50 mins.) identify mineral components, such as pyroxene, plagioclase, oxides, and phosphates, compositional zoning, and mineral textures. Detection of high-Z phases: µXRF techniques are es-pecially effective at analyzing trace minerals with high-atomic-number (high-Z) elements because the high-energy characteristic X-rays used (relative to SEM EDS) allow for mapping of K lines in elements up to La (typically SEM maps use L X-ray lines for elements >Zn, and these can often have interferences). Thus, µXRF is especially suited for identifying minerals like zircon, baddeleyite, REE-rich phosphates, Fe-rich met-als, oxides, sulfides, and phosphides [4]. In Fig. 3 we show elemental distribution maps for 73001,530 where we are able to correlate the original video image with, Zr, Si, Y and Hf elemental maps together identi-fying the location of a zircon. In this location you would expect lower Si compared to surrounding mate-rial, as well as higher Zr, Y, and Hf content compared to surrounding material, all of which is confirmed by our XRF ele-mental distribution maps (Figure 2.) Conclusions: The new M4 Tornado Plus µXRF within the Astromaterials Acquisition and Curation office at NASA JSC allows for rapid and non-destructive elemental analysis of astromaterials with limited or no sample preparation. µXRF analyses pro-vide crucial compositional knowledge for the prelimi-nary examination and curation of astromaterials. This instrument enhances the advanced curation capabili-ties in the X-FaCT laboratory at JSC by allowing pro-ductive, cohesive, and non-destructive multi-modal x-ray analyses on astromaterial samples, which is neces-sary for the comprehensive curation and study of our current and future astromaterial collections. Addition-ally, µXRF can provide complimentary information to researchers for studies on astromaterials. References: [1] Allen, C. et al., (2011). Chemie De Erde Geochemistry, 71, 1-20. [2] McCubbin, F. M. et al., (2016) 47th LPSC, abstract #2668 [3] Zeigler, R. A. et al., (2017) 48th LPSC, abstract #2772 [4] Bruker User Manual [5] Young et al., (2016) Appl. Geochemistry, 72, 77-87 [6] Mor-ris, R. V. et al., (2023) 54th LPSC.

E W O'Neal↗
NASA NTRSDate not supplied

Investigating Pyroclastic Volcanism in the Taurus-Littrow Valley (TLV) Using the Station 3 Double Drive Tube 73001-73002

Well over 100 pyroclastic deposits have been identified on the Moon. Eruptive processes such as represented by these deposits transported endogenous volatiles from the Moon’s mantle to its surface. Debris from pyroclastic deposits has been identified in all Apollo and Luna samples. The high-Ti pyroclastic de- posit sampled at Shorty Crater by the Station 4 double drive tube (74001-74002) is our best sampling of these types of deposits. Samples 78500 and 78526, NAC images of fissures in the Sculptured Hills, ash identified in 70001-7, and other green volcanic glass indicate that very low-Ti basalt (VLT) erup- tions also occurred in TLV. The double drive tube core being investigated by the ANGSA initiative provides an- other view of TLV pyroclastic eruptions. The regolith in 73001-73002 and the regolith breccias therein have nu- merous pyroclastic beads. Some individual regolith brec- cia fragments have abundant pyroclastic beads (>50 in a polished surface). In this work, we address the following questions. Do these glass beads overlap in composition with those sampled elsewhere in the TLV or do they rec- ord another episode of pyroclastic eruption? Are the magmas associated with pyroclastic eruptions petroge- netically related to the crystalline mare basalts in the TLV? Finally, is the volatile record of the pyroclastic eruptions better preserved in the newly opened and spe- cially contained Station 3 double drive tube core?

C.K. Shearer↗
NASA NTRSDate not supplied

Space Transformation -- Localizing the Remote and Connecting the Isolated

In motivating the Space Transformation theme for this year’s 4S symposium, the organizers provided the following context, “Transformation of economies are driven by a change in values and accelerated by new technologies.” These words rang particularly true when I read them at the beginning of the holiday season. Like so many others, I was in the early phases of my Christmas shopping procrastination campaign, and I’d just been reflecting on how Amazon Prime was the transformational tool I’d been waiting for. Basic limiting principles of time and space, supply and demand, were all but erased by the Amazon Prime phenomenon. Coupled with emerging 3D printing and other adaptive manufacturing technologies, a transformation from deliberate planning to “think it … have it” had occurred, empowering me to procrastinate longer than I’d ever dreamed possible. The organizers went on to ponder, “Will space transformation also affect society?”, just as our team at the Air Force Research Lab’s (AFRL) Center for Rapid Innovation (CRI) were working alongside partners within our larger Integrated Capabilities Directorate, NASA’s Flight Opportunities and Small Spacecraft Technology programs, and DARPA’s Luna-10 program to develop technologies and execute demonstration missions that leverage the space domain to genuinely connect even the most remote and austere domains on the timeline of need. Picking apart the miracle that is Amazon prime, where does the model fail, and why? More relevantly to the theme of this year’s symposium, how can the space domain be used to overcome its limitations and minimize its weaknesses? Perhaps it is best assessed in the context of Use Cases. What are the Amazon delivery cost, schedule, and cargo limiters to the Amundsen-Scott South Pole Research Station, or the Lunar South Pole Research Station? This paper will explore enabling infrastructure that allows Amazon prime to thrive and assess the transformational enabling technologies that would be necessary to extend that miracle to the truly remote or the truly austere. Localizing the Remote • First, it will evaluate the ability of the on-going AFRL Rocket Cargo and Space Initiatives Ringside Seats systems, coupled with Astrobotic’s Xodiak and Xogdor capabilities, developed to support the NASA Flight Opportunities Program (FOP), to supply orbital/suborbital delivery to both improved and austere sites on the Earth and Moon. • Then, it will add the surface terminal distribution leg, with an examination of Lunar Outpost’s Mobile Autonomous Prospecting Platform (MAPP), equipped with Mobile Autonomous Robotic Swarm (MARS) software, and Intuitive Machine’s Hopper, developed with support of AFRL and NASA’s Commercial Lunar Payload Services (CLPS) program. Connecting the Isolated From there, it will focus on the destination, asking what implied destination services are required to support highly assured autonomous delivery. • Specifically, it will highlight Astrobotic’s Skymage mesh-networked publish and subscribe communication and navigation service, as well as AFRL’s on-going developments of radioisotope and reactor nuclear-sourced thermoelectric power generation and distribution systems under development under the Joint Emergent Technology Supplying On-orbit Nuclear Power (JETSON) program by Lockheed Martin, Westinghouse, Intuitive Machines, and Zeno Power, to provide the power service to locations well off the grid. • Finally, the paper will connect to the “human machine”. What connects the remote or in-situ human consumer to the remote domain? What connects the diverse international government and commercial services to each other? The former will focus on AFRL’s OraCloud feeding their Space Defense Control and Characterization System (SDCCS) and Lunar Station’s MoonHacker systems, while the latter will focus on the BlueHalo/Tensor LunX Technology Platform for the Cislunar Commodity Marketplace. In 1984, Krafft Ehricke famously remarked that, “If God wanted man to become a spacefaring species, He would have given man a Moon.” This paper is not about the Moon, but is about humans as a spacefaring species, shedding the pesky land/air limitations of the Amazon Prime model … so that we can all live a procrastinator’s “think it … have it” existence.

Charles Finley↗
NASA NTRS2024

Review of melt inclusions in lunar rocks: constraints on melt and mantle composition and magmatic processes

Mineral-hosted melt inclusions provide a window into magmatic processes and pre-eruptive liquid compositions. Because melt inclusions are small (typically < 100 µm), the study of lunar melt inclusions is enabled by advancements of microbeam instrumental techniques. In the 1970s immediately following the Apollo and Luna missions, major and minor oxide concentrations of lunar melt inclusions were measured using electron microprobes. The data were used to understand magma evolution, and they revealed the immiscibility of two silicate liquids in the late stage of lunar magma evolution. More recently, the development of secondary ion mass spectrometry as well as laser ablation–inductively coupled plasma–mass spectrometry has enabled the measurement of key volatile elements and other trace elements in lunar melt inclusions, down to about the 0.1 ppm level. The applications of these instruments have ushered in a new wave of lunar melt inclusion studies. Recent advances have gone hand in hand with improved understanding of post-entrapment loss of volatiles. These studies have provided deep insights into pre-eruptive volatiles in lunar basalts, the abundance of volatiles in the lunar mantle, the isotopic ratios of some volatile elements, and the partition of trace elements between host olivine and melt inclusions. The recent studies of lunar melt inclusions have played a critical role in establishing a new paradigm of a fairly wet Moon with about 100 ppm H2O in the bulk silicate Moon (rather than a “bone-dry” Moon) and have been instrumental in developing an improved understanding of the origin and evolution of the Moon.

Youxue Zhang↗
NASA NTRSDate not supplied

Lunar Laser Ranging in the Artemis Era

The retroreflector arrays placed on the lunar surface by the Apollo astronauts and the Soviet Luna missions continue to contribute to our understanding of gravitational physics, Earth and Moon geophysics, geodesy, and dynamics. The key science questions addressed by Lunar Laser Ranging remain very relevant today: What is the interior structure of the Moon? Is the Equivalence Principle exact? Does the strength of gravity vary with space and time? What is the nature of spacetime? Do extra dimensions or other new physics alter the inverse square law of gravity? The lunar retroreflectors are also an essential component of the realizations of the lunar reference frames. The half-century old lunar retroreflectors continue to provide excellent ranging targets but are showing signs of degradation and the measurement error associated with their physical size and varying tilt is becoming a limitation in the quest for more precise range measurements. In addition, the clustering of the arrays in the mid-latitudes of the Moon limits their geometrical strength and coverage. The south polar region planned for Artemis presents an ideal opportunity for improving the geometric distribution. Retroreflectors utilizing a large optical cross-section single cube corner do not have tilt error associated with the existing arrays making them good options for lunar deployment. Several new retroreflectors of this type are being prepared for upcoming Commercial Lunar Payload Services missions as well as Artemis. This presentation will discuss NASA’s plans for expanding the lunar laser ranging capabilities with a focus on the Artemis Lunar Laser Retroreflector.

Stephen Merkowitz↗
NASA NTRS2026

Adaptive Curation at NASA Johnson Space Center: Preparing for Artemis Samples by Leveraging Proven Practices and Innovative Solution

The proper curation of returned astromaterial samples is essential to ensure that high-quality scientific investigations can be conducted for decades, enabling future generations to address evolving research questions. The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (hereafter JSC Curation) is responsible for curating all of NASA’s extraterrestrial samples. Under the governing document, NASA Procedural Requirement (NPR) 7100.5 “Curation of Extraterrestrial Materials”, JSC Curation is charged with “The curation of all extraterrestrial material under NASA control, including future NASA missions.” The Directive goes on to define Curation as including “...documentation, preservation, preparation, and distribution of samples for research, education, and public outreach.” JSC Curation has a long-standing legacy of curating extraterrestrial materials, including but not limited to Apollo and Luna lunar samples, Genesis solar wind samples, Stardust comet samples, asteroid samples (Hayabusa1, Hayabusa2, and OSIRIS-REx), and Antarctic Meteorite samples from a variety of parent bodies. Building on this foundation, the Artemis program introduces new challenges and opportunities for sample curation, requiring both the application of proven practices and the development of innovative solutions. The Artemis Collection will be curated using established protocols refined through decades of experience with Apollo and subsequent sample collections, including but not limited to the utilization of cleanrooms, custom nitrogen gloveboxes, specialized storage containers and tools; all of which have strict material utilization and prohibition requirements. These practices provide a robust framework for contamination control, documentation, and long-term preservation. However, Artemis samples may present unique scientific and operational requirements, including enhanced contamination control measures (relative to Apollo) driven by evolving science objectives. To meet these needs, JSC Curation is actively developing new technologies and protocols that extend beyond traditional approaches, ensuring that the integrity of samples is maintained under increasingly stringent standards. One critical area of innovation is the development of cold sample curation capabilities. Certain Artemis samples, particularly those from Permanently Shadowed Regions (PSRs) and cold environments, are expected to contain ices and volatile components that require preservation and handling at sub-zero or even cryogenic temperatures. JSC Curation is leveraging best practices from the cold and cryogenic sample industries, as well as other government agencies and academic experts, to design facilities and handling procedures that maintain sample integrity while enabling scientific access. The goal is to develop capabilities to allow researchers to investigate volatiles and other temperature-sensitive materials while minimizing chemical and physical alterations from their returned state. In summary, adaptive curation at JSC combines the reliability of proven methodologies with forward-looking innovations to meet the scientific and operational demands of Artemis. Through enhanced contamination control, advanced cold curation capabilities, and an understanding of known and evolving future science priorities, NASA is preparing to maximize the scientific return from Artemis samples and preserve their value for generations of researchers.

Andrea D Harrington↗
NASA NTRS1985

Two-plane balance and slip-ring design

A 3.25 cm (1.28 in.) two plane balance and eight channel slip ring assembly has been designed to measure and transmit the thrust (667-N;150-lb) and torque (135-N-m;100-lb-ft) components produced by wind tunnel model turboprops and drive motors operating at 300 Hz.

Luna, P. M.↗
NASA NTRS1988

Experiments with metallic and ceramic porous media

Work in the area of mechano-caloric phenomena was initiated during 1988 with startup in the Summer 1988 period. The ideal system utilizing He-II super-phenomena is modeled readily, within the frame of thermodynamics energetics, using the concept of an ideal superleak. The real system however uses porous media of non-ideal pore-grain ingredients. The early phase of experimental and related modeling studies is outlined for the time period from Summer 1988 to the end of 1988.

Frederking, T. H. K.↗
NASA NTRS1989

Mechano-caloric cooling device

The mechano-caloric effect is potentially useful in the He II temperature range. Aside from demonstration work, little quantification effort appears to have been known since other refrigeration possibilities have been available for some time. Successful He II use-related system examples are as follows: in space, the utilization of the latent heat of vaporization has been quite successful in vapor-liquid phase separation (VLPS) in conjunction with thermomechanical force application in plugs. In magnet cooling systems, the possibility of using the mechano-caloric cooling effect in conjunction with thermo-mechanical circulation pump schemes, has been assessed (but not quantified yet to the extent desirable). A third example is quoted in conjunction with superfluid wind tunnel studies and liquid helium tow tank for surface vessels respectively. In all of these (partially future) R and D areas, the question of refrigerator effectiveness using the mechano-caloric effect appears to be relevant, possibly in conjunction with questions of reliability and simplicity. The present work is concerned with quantification of phenomena including simplified thermodynamic cycle calculations.

Frederking, T. H. K.↗
NASA NTRS1989

The Crop Growth Research Chamber - A ground-based facility for CELSS research

Crop Growth Research Chambers (CGRCs) are being developed as CELSS research facilities for the NASA/Ames Research Center. The history of the CGRC project is reviewed, noting the applications of CGRC research for the development of the Space Station. The CGRCs are designed for CELSS research and development, system control and integration, and flight hardware design and experimentation. The atmospheric and hydroponic environments of the CGRC system are described and the science requirements for CGRC environmental control are listed.

Bubenheim, David L.↗