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DOE OSTI2024

Hear It? – New Physics Calls For a Healthy Target!

Nowadays, when the attention of the physics community is drawn to muon collider prospects and neutrino projects, a target as the primary source of such exotic particles is a key component of a particle physics experiment. The extreme conditions placed on the target, though, decrease its functionality and threaten the future of high-power targetry. Subject to superb magnetic fields, extreme temperatures, and radiation damage, the target is constantly at risk of unexpected failures. The Target Health Monitor (THM) aims to enable the continuous analysis of the target state throughout the experiment. Based on the optical concept of Brewster s angle and the reflectivity variation with the compositional changes in the target material, the THM will record and evaluate the radiation-caused transmutations in the target to foresee its malfunction before it affects the experimental results. The first steps in validating our THM concept have been made this summer. Continuing reflectivity measurements of the prospective target materials, we anticipate proving the THM potential to monitor target health effectively.

Havryshchuk, Kateryna↗

DOE OSTI2024

Multiphysics Simulations of Nanofibrous High Power Targets for the Inference of Failure Modes

Fermilab s High Power Targetry Research and Development (HPT R&D) group have been developing and studying an electrospun nanofiber target concept to support the need for robust targets in future fixed target facilities. These nanofiber mats have demonstrated resistance to radiation damage, and the free motion of the individual fibers is expected to mitigate the cyclic stresses induced by a pulsed, high-power beam. To evaluate the efficacy of this concept, nanofiber mat samples have been sent by the HPT R&D group to the HiRadMat facility at CERN for prototypic thermal shock testing; the outcomes of these experiments show that the survivability of a nanofiber target depends on its construction parameters, in particular the packing density of the fibers. Samples with higher packing densities have consistently been destroyed by exposure to the HiRadMat beam, with a hole at the beam center visible, and layers of nanofibers peeled away from the center hole, whereas samples with lower densities have survived with limited damage. The exact reason for the failure of the higher density targets was unclear at the time of the original experiments, but the results of our recent multiphysics simulations which recreate the experiments support the hypothesis that the expansion and pressurization of the air inside the target after being heated by the pulsed beam is the cause; in a high density nanofiber mat, the motion of air through the pores of the mat is much more restricted, and induces a larger pressure on the fibers, blowing the mat apart. In this talk, we ll share the results of these simulations and discuss how they support this hypothesis.

Asztalos, Will↗

DOE OSTI2025

Molten Salt Targets - Concept Development

Overview of recent conceptual work examining molten salts for use in accelerator targetry.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2025

RaDIATE Collaboration Thermal shock studies

As next-generation accelerator target facilities (High Energy Physics, Spallation Sources, ... ) become increasingly more powerful and intense, high power target systems face key technical challenges, such as radiation damage and thermal shock. Those ultimately degrade the performance and lifetime of targets and have been identified as the leading cross-cutting challenges of high-power target facilities. In order to operate reliable beam-intercepting devices in the framework of energy and intensity increase for next generation accelerators, the RaDIATE Collaboration (Radiation Damage In Accelerator Target Environment), established in 2012 and managed by Fermilab, brings together existing expertise in nuclear material and accelerator targets from 20 international institutions, including CERN, to execute a coordinated strategy for high power targetry R&D. In this context, several thermal shock studies were performed at CERN's HiRadMat (High-Radiation to Materials) facility, that took a key step towards improving our knowledge on target damage tolerance. The first experiment HRMT-24, supported by EURCARD2 and completed in 2015, successfully validated the Johnson-Cook strength model developed at SwRI on beryllium S200FH (used for beam window material), providing a better confidence in simulating the thermal shock response of current and future S200FH beryllium components. HRMT-43, supported by ARIES and completed in 2018, tested various materials (Be, C, SiC, Si, Ti and ceramic nanofiber). It was a first and unique test which included pre-irradiated specimens from high energy proton beam irradiation to identify thermal shock response differences between non-irradiated and previously irradiated materials. Real-time measurement of dynamic thermomechanical response of graphite helped to benchmark numerical simulations.

43 PARTICLE ACCELERATORS↗

DOE OSTI2021

IAEA Activities on 67Cu, 186Re, 47Sc Theranostic Radionuclides and Radiopharmaceuticals

Despite interesting properties, the use of 67 Cu, 186 Re and 47 Sc theranostic radionuclides inpreclinical studies and clinical trials is curtailed by their limited availability due to a lack of widelyestablished production methods. An IAEA Coordinated Research Project (CRP) was initiated toidentify important technical issues related to the production and quality control of these emergingradionuclides and related radiopharmaceuticals, based on the request from IAEA Member States.The international team worked on targetry, separation, quality control and radiopharmaceutical aspectsof the radionuclides obtained from research reactors and cyclotrons leading to preparation ofa standard recommendations for all Member States. The CRP was initiated in 2016 with fourteenparticipants from thirteen Member States from four continents. Extraordinary results on the production,quality control and preclinical evaluation of selected radionuclides were reported in this projectthat was finalized in 2020. The outcomes, outputs and results of this project achieved by participatingMember States are described in this minireview.

Pharmacology & Pharmacy↗

DOE OSTI2024

Achievement in Beam Power Records for the NOvA Target System

We began updating the NOvA target system for 1-Mega Watt (1-MW) beam operation in 2017. Major changes include maintaining the quality of neutrino beams with reliable instrumentation, reducing instantaneous beam heating on the target, increasing cooling power to handle the high power beam, and controlling tritium water production rate. We successfully achieved a onehour beam power report of 1.018 MW in Summer 2024. This achievement marks an important milestone for Fermilab, demonstrating the capability of the accelerator complex to handle highintensity proton beams at a fast repetition rate. We are now prepared to proceed with a new accelerator upgrade plan, known as the Accelerator Complex Evolution - Main Injector Ramp and Targetry R&D (ACE-MIRT) to support future operates at beam power exceeding 2 MW for the Long Baseline Neutrino Facility (LBNF) and Deep Underground Neutrino Experiment (DUNE). We present the improvement of the target system to exceed the beam power 1-MW.

Yonehara, Katsuya [Fermilab] (ORCID:00000002544041↗

DOE OSTI2021

Production, Purification, and Applications of a Potential Theranostic Pair: Cobalt-55 and Cobalt-58m

The emerging success of [68Ga/177Lu]Ga/Lu-DOTATATE as a theranostic pair has spurred interest in other isotopes as potential theranostic combinations. Here, we review cobalt-55 and cobalt-58m as a potential theranostic pair. Radionuclidically pure cobalt-55 and cobalt-58m have been produced on small cyclotrons with high molar activity. In vitro, DOTATOC labeled with cobalt has shown greater affinity for SSTR2 than DOTATOC labeled with gallium and yttrium. Similarly, [58mCo]Co-DOTATATE has shown improved cell-killing capabilities as compared to DOTATATE labeled with either indium-111 or lutetium-177. Finally, PET imaging with an isotope such as cobalt-55 allows for image acquisition at much later timepoints than gallium, allowing for an increased degree of biological clearance of non-bound radiotracer. We discuss the accelerator targetry and radiochemistry used to produce cobalt-55,58m, emphasizing the implications of these techniques to downstream radiotracers being developed for imaging and therapy.

60 APPLIED LIFE SCIENCES↗

NASA NTRS1972

A target design for irradiation of NaI at high beam current

A solution to the targetry problems encountered when the iodine nucleus is a target for cyclotron irradiation is given as a target design. A target based on this design was used in 30 microampere irradiations of 46 MeV alpha particles for one-half hour without significant damage. Such an irradiation produces 6 to 7 mCi of Cs-129. This target should also be considered for cyclotron production of the radioisotopes Cs-127, I-123, and Xe-127.

Blue, J. W.↗

NASA NTRS1972

A target design for irradiation of NaI at high beam current.

A solution to the targetry problems encountered when the iodine nucleus is a target for cyclotron irradiation is given as a new target design. A target based on this design has been used in 30 microampere irradiations of 46 MeV alpha particles for one-half hour without significant damage. Such an irradiation produces 6 to 7 mCi of Cs-129, an isotope useful in nuclear medicine. This target should also be considered for cyclotron production of the radioisotopes Cs-127, I-123, and Xe-127.

Blue, J. W.↗

DOE OSTI2023

Workshop on a future muon program at FNAL

The Snowmass report on rare processes and precision measurements recommended Mu2e-II and a next generation muon facility at Fermilab (Advanced Muon Facility) as priorities for the frontier. The Workshop on a future muon program at FNAL was held in March 2023 to discuss design studies for Mu2e-II, organizing efforts for the next generation muon facility, and identify synergies with other efforts (e.g., muon collider). Topics included high-power targetry, status of R&D for Mu2e-II, development of compressor rings, FFA and concepts for muon experiments (conversion, decays, muonium and other opportunities) at AMF. This document summarizes the workshop discussions with a focus on future R&D tasks needed to realize these concepts.

43 PARTICLE ACCELERATORS↗

DOE OSTI2025

Production Target Studies at the M4 Diagnostic Absorber

High power production targetry is becoming essential to the future of HEP, but our current physics simulations are lacking validation in the lower energy ranges that many proposed secondary beam experiments will use. We propose a study of target materials at the M4 diagnostic absorber to monitor target temperatures during irradiation by an 8 GeV proton beam and provide some experimental validation for our simulations at lower energies as well as potentially perform post-irradiation examination of samples to understand changes to material properties.

Bloomer, Madeleine [UC, Davis] (ORCID:000900080329↗

DOE OSTI2025

Production Target Studies at the M4 Diagnostic Absorber

Bloomer, Madeleine [UC, Davis] (ORCID:000900080329↗

DOE OSTI2019

Pu-240 Target Preparation on Thin Backing Foils for GRETINA Experiments using ATLAS

Recent measurements of the octupole strength to the highest spin states in Pu-240 were performed using sub-barrier Coulomb excitation in order to unambiguously and convincingly demonstrate the existence of the rotational-aligned phonon condensation in this nucleus. The Pu-240 targets were prepared at the Center for Accelerator Target Science by molecular plating onto thin backing foils of C and Al. The required plutonium oxide dissolution, molecular plating methodology, plating results, and in-beam target performance will be discussed.

Actinides↗

DOE OSTI2024

Radiation damage study of POCO ZXF-5Q graphite for neutrino production targets using 4.5 MeV helium ions

To address the challenges of increased beam power and target survivability associated with next-generation particle production beam lines, high dose, high-energy proton beam conditions are simulated using irradiation from low-energy ion beams. A low-energy ion irradiation study of POCO ZXF-5Q graphite under conditions similar to those of the NuMI NT-02 neutrino production target at the Fermi National Accelerator Laboratory is reported. Helium ion irradiation was performed at 100 ∘ C to a maximum damage level of 0.9 displacements per atom (DPA). Irradiation induced hardening, swelling of the irradiated region, inter-plane lattice expansion, and intraplane lattice contraction with increasing ion fluence was observed using micromechanical (nanoindentation, atomic force microscopy) and electron microscopy (high-resolution imaging, selected area diffraction) characterization. Similar changes were also observed in post irradiation examination of the NT-02 target indicating that ion irradiation can be a valuable tool for estimating radiation damage in proton beam targets. Caution must be exercised though, because the hardening, lattice alteration, and swelling occur to different magnitudes for a given damage level. The observed hardening and embrittlement were greater for ion irradiated graphite. For He ion irradiated samples the lattice spacing changes were smaller at low damage levels (78% less expansion and 71% less contraction at 0.1 DPA) and larger at high damage levels (38% more expansion and 5% more contraction at 0.9 DPA) relative to that observed in the NT-02 target. The magnitude of swelling was 8.5× greater under ion irradiation which is influenced by the differing damage gradients and inclusion of implanted He ions in the region of interest.

43 PARTICLE ACCELERATORS↗

DOE OSTI2026

Combustion-assisted ink-jet printing of nuclear targets

Advances in target fabrication are critical to high-precision measurements in nuclear physics. This work details the preparation of patterned CeO 2 and ThO 2 architectures and thin-film targets via ink-jet deposition of combustible solutions. The produced targets were characterized by scanning electron microscopy (SEM), and by alpha-particle spectroscopy for radioactive targets to determine densities. Ink jet printing of the targets, used both ethanol and 2-methoxyethanol as solvents, with cerium or thorium nitrate as the oxidizer and acetylacetone as the fuel. Additionally, we found that the distance between each droplet dispersion (step size) played the most significant role in determining the final pattern uniformity and thickness. A 50 μm step size leads to relatively thick targets with a density of 350 μg/cm 2 . Significant overlap in droplet sizes leads to a heterogeneous target with an undesirable cracked surface structure. In contrast, 150 μm spacing yields thinner (20 μg/cm 2 ) patterned structures with excellent surface coverage. This method of Ink-jet printing provides a straightforward, scalable, and high-efficiency pathway to prepare custom made, high-quality targets for nuclear physics experiments.

CeO2↗

DOE OSTI2026

Irradiation Driven Restructuring of Nanocrystalline ThO 2 and Th 1–x U x O 2 Thin Films

Irradiation induced structural changes of actinide oxide materials is a key consideration in their development and use as nuclear fuels. This study reported on the synthesis of ThO 2 and Th 1–x U x O 2 (x = 0.15, 0.50) thin films, fabricated using electrospray-assisted solution combustion synthesis, and their responses to ion irradiation. Krypton ion irradiations, up to a fluence of 1 × 10 16 ions/cm 2 , were carried out to simulate radiation damage induced by fission products in a reactor environment. Structural and chemical changes induced by irradiation were analyzed using high-resolution scanning transmission electron microscopy (STEM), energy-dispersive X-ray spectroscopy (EDS), and electron energy-loss spectroscopy (EELS). It was determined that the extent and nature of irradiation-induced damage are strongly correlated with the uranium content. ThO 2 films were most susceptible to radiation-induced damage, with significant cavity formation and delamination from the substrate at high fluence. Of the compositions studied, Th 0.85 U 0.15 O 2 films showed the highest stability, characterized by moderate grain growth and the absence of voids or severe defect structures. In contrast, Th 0.5 U 0.5 O 2 films accumulated extensive damage, including the formation of a nanocrystalline central region. EELS analysis indicated that oxygen displacement is the primary driver of structural degradation in Th 0.5 U 0.5 O 2 films. α-particle spectroscopy confirmed minimal actinide loss across all compositions, underscoring the mechanical robustness of the films. These findings provide insight into the irradiation-induced damage mechanisms in Th O2 and Th 1–x U x O 2 systems, supporting their development as potential materials for nuclear fuels and irradiation-tolerant thin film targets in nuclear physics measurements.

Th1−xUxO2↗