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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 55 records · Page 3

Measurements of the Viscosity of the Undercooled Melts Under the Conditions of Microgravity and Supporting MHD Calculations

This report covers the work to support the measurement of the surface tension and viscosity of undercooled metals with the TEMPUS as a part of the IML-2 mission. This work consisted of two parts. First was the ground-based research program, whose purpose was to establish the feasibility of the flight program and to establish the knowledge base necessary to plan a successful flight program. Analytical calculations established a fundamental understanding of the problem, and then a more rigorous program of numerical calculations was employed in the development of the experimental program. The second part of the covered research was the actual flight program, developed in close collaboration with Prof. Egry. A metal sphere was levitated and melted, and then set oscillating by 'squeezing' it with the magnetic field. The droplet's oscillations were recorded on videotape and digital image analysis was employed in reduction of the data. The experiment was successful because surface tension measurements were obtained for the gold and gold-copper alloy samples. This data provides unique experimental evidence in support of theories about electromagnetic levitation on the ground. Because of unforeseen difficulties with stability of liquid samples in TEMPUS, the viscosity measurements were not possible, but the data collection and analysis techniques were well proven in this mission. Further research is being conducted regarding the measurement of viscosity by this technique.

Szekely, Julian↗

Custom Turnkey Time and Frequency Systems: A structured, expandable approach

Radiocode Clocks Ltd. have developed a Turnkey Time and Frequency Generation and Distribution, System strategy based upon a bus of three, 'core' signals from which any Time code, Pulse rate or Frequency can be produced. The heart of the system is a ruggedized 19 inch, 3U Single Eurocard chassis constructed from machined 10mm aluminum alloy plate and designed to meet stringent Military, Security and Telecommunications specifications. The chassis is fitted with an advanced multilayer backplane with separate ground planes for analog and digital signals ensuring no degradation of low noise frequency references in the proximity of high speed digital pulse transmissions. The system has been designed to be used in three possible configurations: 1) As a stand alone generation and distribution instrument; 2) As a primary distribution unit in a turnkey Time and Frequency system; and 3) As a secondary distribution unit at a remote location from the Turnkey Time and Frequency System providing regeneration of core signals and correction for transmission delays. When configured as a secondary distribution unit the system will continue to provide usable outputs when one, two or even all three of the 'core' signals are lost. The instrument's placement within a system as a possible single point of system failure has required the development of very high reliability translator, synthesizer, phase locked loop and distribution modules together with a comprehensive alarm and monitoring strategy.

Wright, David F.↗

A computer program for Moessbauer data processing

A computer program to analyze Mossbauer data is presented in detail. The least-squares curve fitting techniques described apply to single line spectra, single hyperfine spectra, or when the constituent spectra are separated well enough to let the individual absorption peaks stand alone. The present program is not adapted for complex spectra resulting from the existence of several local environments in the absorber iron alloy. Sample problems are presented to aid the user in setting up and running the program. The program is written in FORTRAN 4 language for the Control Data 6000 series digital computer with the SCOPE 3.0 operating system and requires approximately 115,000 octal locations of core storage. A typical case with one absorption peak runs in 20 seconds, and a typical problem with six absorption peaks requires 50 seconds.

Howser, L. M.↗

Test and Analysis of Sub-Components of Aluminum-Lithium Alloy Cylinders

Integrally machined blade-stiffened panels subjected to an axial compressive load were tested and analyzed to observe the buckling, crippling, and postcrippling response of the panels. The panels were fabricated from aluminum-lithium alloys 2195 and 2050, and both alloys have reduced material properties in the short transverse material direction. The tests were designed to capture a failure mode characterized by the stiffener separating from the panel in the postbuckling range. This failure mode is attributed to the reduced properties in the short transverse direction. Full-field measurements of displacements and strains using three-dimensional digital image correlation systems and local measurements using strain gages were used to capture the deformation of the panel leading up to the failure of the panel for specimens fabricated from 2195. High-speed cameras were used to capture the initiation of the failure. Finite element models were developed using an isotropic strain-hardening material model. Good agreement was observed between the measured and predicted responses for both alloys.

Haynie, Waddy T.↗

Surface roughness effects on bidirectional reflectance.

An experimental study of surface roughness effects on bidirectional reflectance of metallic surfaces is presented. Samples consisting of glass, aluminum alloy, and stainless steel materials were roughened using standard grinding techniques and coated with a radiatively opaque layer of pure aluminum. Surface roughness parameters, rms height and rms slope, were evaluated from digitized surface profile measurements and are less than 1.0 micron, and 0.28, respectively. Rough-surface specular, bidirectional, and directional reflectance measurements for selected values of polar angle and wavelength of incident energy within the range from 10 to 80 deg and from 1 to 14 microns, respectively, are reported. The influence of surface roughness is discussed in terms of rms height and rms slope.

Smith, T. F.↗

Uses of Computed Tomography in the NASA Materials Science Program

Computed Tomography (CT) has proved to be of inestimable use in providing a rapid evaluation of a variety of samples from Mechanics of Granular Materials (MGM) to electronic materials (Ge-Si alloys) to space grown materials such as meteorites. The system at Kennedy Space Center (KSC), because of its convenient geographical location, is ideal for examining samples immediately after returning to Earth. It also has the advantage of the choice of fluxes, and in particular the use of a radioactive cobalt source, which is basically monochromatic. This permits a reasonable measurement of density to be made from which chemical composition can be determined. Due to the current dearth of long duration space grown materials, the CT instrument has been used to characterize materials in preparation for flight, to determine thermal expansion values, and to examine long duration space grown materials, i.e. meteorites. The work will first describe the establishment of the protocol for obtaining the optimum density readings for any material. This will include both the effects of the hardware or instrumental parameters that can be controlled, and the techniques used to process the CT data. Examples will be given of the compositional variation along single crystals of germanium-silicon alloys. Density variation with temperature has been measured in preparation for future materials science experiments; this involved the fabrication and installation of a single zone furnace incorporating a heat pipe to ensure of high temperature uniformity. At the time of writing the thermal expansion of lead has been measured from room temperature to 900 C. Three methods are available. Digital radiography enable length changes to be determined. Prior to melting the sample is small than the container and the diameter change can be measured. Most critical, however, is the density change in solid, through the melting region, and in the liquid state. These data are needed for engineering purposes to aid in the design of containment cartridges, and for enabling fluid flow calculations. A second sample, with the lead alloyed with antimony is ready for scanning. This corresponds to the planned composition of Dr. Poirier's flight experiment. Finally, three-dimensional results will be shown of the structure of a two-phase metallic meteorite of metal and sulfide, in which the iron-nickel phase has coarsened during slow cooling over hundreds of millions of years.

Engel, H. Peter↗

Uses of Computed Tomography for Characterizing Materials Grown Terrestrially and in Microgravity

Tomography (CT) has proved to be of inestimable use in providing a rapid evaluation of a variety of samples from Mechanics of Granular Materials (MGM) to electronic materials (Ge-Si alloys) to space grown materials such as meteorites. The system at Kennedy Space Center (KSC), because of its convenient geographical location, is ideal for examining samples before launch and immediately after returning to Earth. It also has the advantage of the choice of fluxes, and in particular the use of a radioactive cobalt source, which is basically monochromatic. This permits a reasonable measurement of density to be made from which chemical composition can be determined. Due to the current dearth of long duration space grown materials, the CT instrument has been used: (1) to characterize materials in preparation for flight, (2) to determine thermal expansion values, and (3) to examine long duration space grown materials, i.e. meteorites. This work will first describe the establishment of the protocol for obtaining the optimum density readings for any material. Included will be the effects of the hardware or instrumental parameters that can be controlled, and the techniques used to process the CT data. Examples will be given of the compositional variation along a single crystal of Ge-Si alloy. Density variation with temperature has been measured in preparation for future materials science experiments; this involved the fabrication at MSFC and installation of a single zone furnace at KSC incorporating a heat pipe to ensure high temperature uniformity. At the time of writing the thermal expansion of lead (Pb) has been measured from room temperature to 900 C. Three methods are available. Digital radiography enables length changes to be determined. Prior to melting the sample is smaller than the container and the diameter change can be measured. Most critical, however, is the density change in solid, through the melting region, and in the liquid state. These data are needed for engineering purposes to aid in the design of containment cartridges, and for enabling fluid flow calculations. A second sample, with the Pb alloyed with Sb is ready for scanning. This corresponds to the planned composition of Dr. Poirier s flight experiment. Other materials pertinent to NASA programs such as Al-Cu (Trivedi), CdTe (Banish), HgCdTe (Lehoczky) will be examined below and above the melting point. Finally, three-dimensional results will be shown of the structure of a two-phase metallic meteorite of metal and sulfide, in which the Fe-Ni phase has coarsened during slow cooling over hundreds of millions of years.

Source record↗

Design, Optimization, and Evaluation of A1-2139 Compression Panel with Integral T-Stiffeners

A T-stiffened panel was designed and optimized for minimum mass subjected to constraints on buckling load, yielding, and crippling or local stiffener failure using a new analysis and design tool named EBF3PanelOpt. The panel was designed for a compression loading configuration, a realistic load case for a typical aircraft skin-stiffened panel. The panel was integrally machined from 2139 aluminum alloy plate and was tested in compression. The panel was loaded beyond buckling and strains and out-of-plane displacements were extracted from 36 strain gages and one linear variable displacement transducer. A digital photogrammetric system was used to obtain full field displacements and strains on the smooth (unstiffened) side of the panel. The experimental data were compared with the strains and out-of-plane deflections from a high-fidelity nonlinear finite element analysis.

Mulani, Sameer B.↗

Utilizing Strain Rate Jump Testing to Predict Flow Formability of Al Alloys Sensitive to Portevin-Le Chatelier Instabilities

Predicting the flow formability of Al alloys is challenging due to the incremental deformation, complex loading path, and wide range of strain rates characteristic of the process. State-of-the-art research efforts have primarily focused on formability metrics derived from ambient temperature, constant strain rate uniaxial tensile testing. However, Al alloys in formable tempers tend to exhibit serrated Portevin-Le Chatelier (PLC) flow. The appearance of PLC instabilities implies a negative strain rate sensitivity, loss of tensile area reduction capacity, and decreased formability. Elevated temperature and interrupted strain rate tensile tests of relevant Al alloys were conducted to investigate the effects of rapid changes in strain rate (analogous to a forming increment by a passing roller) on common formability metrics. Emphasis was placed on the character/extent of PLC instabilities using digital image correlation strain measurements. The outcome of this work highlights the possibility of predicting flow formability using strain rate jump testing.

flow forming↗

Surface roughness effects on bidirectional reflectance

An experimental study of surface roughness effects on bidirectional reflectance of metallic surfaces is presented. A facility capable of irradiating a sample from normal to grazing incidence and recording plane of incidence bidirectional reflectance measurements was developed. Samples consisting of glass, aluminum alloy, and stainless steel materials were selected for examination. Samples were roughened using standard grinding techniques and coated with a radiatively opaque layer of pure aluminum. Mechanical surface roughness parameters, rms heights and rms slopes, evaluated from digitized surface profile measurements are less than 1.0 micrometers and 0.28, respectively. Rough surface specular, bidirectional, and directional reflectance measurements for selected values of polar angle of incidence and wavelength of incident energy within the spectral range of 1 to 14 micrometers are reported. The Beckmann bidirectional reflectance model is compared with reflectance measurements to establish its usefulness in describing the magnitude and spatial distribution of energy reflected from rough surfaces.

Smith, T. F.↗

Thermophysical property sensitivity effects in steel solidification

The simulation of advanced solidification processes via digital computer techniques has gained widespread acceptance during the last decade or so. Models today can predict transient temperature fields, fluid flow fields, important microstructural parameters, and potential defects in castings. However, the lack of accurate thermophysical property data on important industrial alloys threatens to limit the ability of manufacturers to fully capitalize on the technology's benefits. A study of the sensitivity of one such numerical model of a steel plate casting to imposed variations in the data utilized for the thermal conductivity, specific heat, density, and heat of fusion is described. The sensitivity of the data's variability is characterized by its effects on the net solidification time of various points along the centerline of the plate casting. Recommendations for property measurements are given and the implications of data uncertainty for modelers are discussed.

Overfelt, Tony↗

Crack-tip-opening angle measurements and crack tunneling under stable tearing in thin sheet 2024-T3 aluminum alloy

The stable tearing behavior of thin sheets 2024-T3 aluminum alloy was studied for middle crack tension specimens having initial cracks that were: flat cracks (low fatigue stress) and 45 degrees through-thickness slant cracks (high fatigue stress). The critical crack-tip-opening angle (CTOA) values during stable tearing were measured by two independent methods, optical microscopy and digital image correlation. Results from the two methods agreed well. The CTOA measurements and observations of the fracture surfaces showed that the initial stable tearing behavior of low and high fatigue stress tests is significantly different. The cracks in the low fatigue stress tests underwent a transition from flat-to-slant crack growth, during which the CTOA values were high and significant crack tunneling occurred. After crack growth equal to about the thickness, CTOA reached a constant value of 6 deg and after crack growth equal to about twice the thickness, crack tunneling stabilized. The initial high CTOA values, in the low fatigue crack tests, coincided with large three-dimensional crack front shape changes due to a variation in the through-thickness crack tip constraint. The cracks in the high fatigue stress tests reach the same constant CTOA value after crack growth equal to about the thickness, but produced only a slightly higher CTOA value during initial crack growth. For crack growth on the 45 degree slant, the crack front and local field variables are still highly three-dimensional. However, the constant CTOA values and stable crack front shape may allow the process to be approximated with two-dimensional models.

Dawicke, D. S.↗

Project Explorer's unique experiments: Get Away Special #007

The Project Explorer payload represents the first attempt at broadcasting digitized voice signals via a Space Shuttle flight on amateur radio frequencies. These amateur ham-radio frequencies will be transmitting real time data while the experiments are operating. Experiments 1, 2, and 3 represent the work of students ranging from materials processing to the science of biology. Experiment 1 will study the solidification of two hypereutectic alloys, lead-antimony and aluminum-copper. Experiment 2 will investigate the examination and growth of radish seeds in space. Experiment 3 will examine the electrochemical growth process of potassium tetrocyonoplatinate hydrate crystals and Experiment 4 involves amateur radio transmissions, monitoring and support of the entire Get Away Special (GAS) 007 payload.

Arthur J. Henderson, Jr.↗

Automated Registration of Multi-Mode Nondestructive Evaluation Data

Registration techniques play a central role in applications of image processing to computer vision, medical imaging, and automatic target tracking. Feature-based techniques such as scale-invariant feature transform (SIFT) and speeded up robust features (SURF) are commonly used to register images derived from a single modality. However, SIFT and SURF struggle to register images from different modalities because the features tend to manifest rather differently and at sometimes very different length-scales. The most successful methods that have been developed to register multi-modal data use information-theoretic approaches. These methods play a key part in nondestructive evaluation scenarios where data that is collected by sensors of different modalities must be registered to be fused. In this paper, automated registration based on normalized mutual information is applied to align data derived from ultrasonic and radiographic inspections of (i) additively manufactured titanium alloy test coupons, and (ii) thin, lithium metal pouch-cell batteries. The quality of the registration is quantified in terms of computational resources and spatial accuracy. In the first case the X-ray computed tomography (XCT) data is captured on a region corresponding to a small subset of the ultrasonic data, while in the case of the lithium batteries the digital radiography (DR) captures a larger region of interest than the ultrasonic data. In both cases the radiographic data resolution is much higher than for ultrasound, but interestingly, in both cases the accuracy of the registration is approximately equal to two-to-three-pixel lengths in the ultrasonic images.

Nondestructive Evaluation↗

NASA Tech Briefs, October 2013

Topics include: A Short-Range Distance Sensor with Exceptional Linearity; Miniature Trace Gas Detector Based on Microfabricated Optical Resonators; Commercial Non-Dispersive Infrared Spectroscopy Sensors for Sub-Ambient Carbon Dioxide Detection; Fast, Large-Area, Wide-Bandgap UV Photodetector for Cherenkov Light Detection; Mission Data System Java Edition Version 7; Adaptive Distributed Environment for Procedure Training (ADEPT); LEGEND, a LEO-to-GEO Environment Debris Model; Electronics/Computers; Millimeter-Wave Localizers for Aircraft-to-Aircraft Approach Navigation; Impedance Discontinuity Reduction Between High-Speed Differential Connectors and PCB Interfaces; SpaceCube Version 1.5; High-Pressure Lightweight Thrusters; Non-Magnetic, Tough, Corrosion- and Wear-Resistant Knives From Bulk Metallic Glasses and Composites; Ambient Dried Aerogels; Applications for Gradient Metal Alloys Fabricated Using Additive Manufacturing; Passivation of Flexible YBCO Superconducting Current Lead With Amorphous SiO2 Layer; Propellant-Flow-Actuated Rocket Engine Igniter; Lightweight Liquid Helium Dewar for High-Altitude Balloon Payloads; Method to Increase Performance of Foil Bearings Through Passive Thermal Management; Unibody Composite Pressurized Structure; JWST Integrated Science Instrument Module Alignment Optimization Tool; Radar Range Sidelobe Reduction Using Adaptive Pulse Compression Technique; Digitally Calibrated TR Modules Enabling Real-Time Beamforming SweepSAR Architectures; Electro-Optic Time-to-Space Converter for Optical Detector Jitter Mitigation; Partially Transparent Petaled Mask/Occulter for Visible-Range Spectrum; Educational NASA Computational and Scientific Studies (enCOMPASS); Coarse-Grain Bandwidth Estimation Scheme for Large-Scale Network; Detection of Moving Targets Using Soliton Resonance Effect; High-Efficiency Nested Hall Thrusters for Robotic Solar System Exploration; High-Voltage Clock Driver for Photon-Counting CCD Characterization; Development of the Code RITRACKS; and Enabling Microliquid Chromatography by Microbead Packing of Microchannels.

Source record↗

Crystal growth of ZnSe and related ternary compound semiconductors by physical vapor transport

The materials to be investigated are ZnSe and related ternary semiconducting alloys (e.g., ZnS(x)Se(1-x), ZnTe(x)Se(1-x), and Zn(1-x)Cd(x)Se). These materials are useful for opto-electronic applications such as high efficient light emitting diodes and low power threshold and high temperature lasers in the blue-green region of the visible spectrum. The recent demonstration of its optical bistable properties also makes ZnSe a possible candidate material for digital optical computers. The investigation consists of an extensive ground-based study followed by flight experimentation, and involves both experimental and theoretical work. The objectives of the ground-based work are to establish the characteristics of the crystals grown on Earth as a basis for subsequent comparative evaluations of the crystals grown in a low gravity environment and to obtain the experimental data and perform the analyses required to define the optimum parameters for the flight experiments. During the six months of the Preliminary Definition Phase, the research efforts were concentrated on the binary compound ZnSe - the purification of starting materials of Se by zone refining, the synthesis of ZnSe starting materials, the heat treatments of the starting materials, the vapor transport rate measurements, the vapor partial pressure measurements of ZnSe, the crystal growth of ZnSe by physical vapor transport, and various characterization on the grown ZnSe crystals.

Su, Ching-Hua↗

A Multi-Mode Blade Damping Control using Shunted Piezoelectric Transducers with Active Feedback Structure

The Structural Dynamics and. Mechanics branch (RXS) is developing smart adaptive structures to improve fan blade damping at resonances using piezoelectric (PE) transducers. In this presentation, only one shunted PE transducer was used to demonstrate active control of multi-mode blade resonance damping on a titanium alloy (Ti-6A1-4V) flat plate model, regardless of bending, torsion, and 2-stripe modes. This work would have a significant impact on the conventional passive shunt damping world because the standard feedback control design tools can now be used to design and implement electric shunt for vibration control. In other words, the passive shunt circuit components using massive inductors and. resistors for multi-mode resonance control can be replaced with digital codes. Furthermore, this active approach with multi patches can simultaneously control several modes in the engine operating range. Dr. Benjamin Choi presented the analytical and experimental results from this work at the Propulsion-Safety and. Affordable Readiness (P-SAR) Conference in March, 2009.

Choi, Benjamin↗