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All sourcesNASA NTRSDOE OSTI
DOE OSTI2019

Dust Polarization Maps from TIGRESS: E/B Power Asymmetry and TE Correlation

We present the first large set of all-sky synthetic dust polarization maps derived directly from a self-consistent magnetohydrodynamics simulation using the TIGRESS framework. Turbulence in this simulation is predominantly driven by supernova explosions, with rates that are self-consistently regulated by feedback loops. The simulation covers both the outer scale and inertial range of turbulence with uniformly high resolution. The shearing-box utilized in the simulation, in concert with resolved supernova-driven turbulence, enables the capturing of generation, growth, and saturation of both turbulent and mean magnetic fields. We construct polarization maps at 353 GHz, as seen by observers inside a model of the multiphase, turbulent, magnetized interstellar medium (ISM). To fully sample the simulated ISM state, we use 350 snapshots spanning over $\sim 350\,\mathrm{Myr}$ (more than six feedback loops) and nine representative observers. The synthetic skies show a prevalent E/B power asymmetry (${EE}\gt {BB}$) and positive TE correlation in broad agreement with observations by the Planck satellite. However, the ranges of ${EE}/{BB}\sim 1.4\mbox{-}1.7$ and ${TE}/{({TT}\cdot {EE})}^{1/2}\sim 0.2\mbox{-}0.3$ are generally lower than those measured by Planck. We find large fluctuations of E/B asymmetry and TE correlation depending on the observer's position and temporal fluctuations of ISM properties due to bursts of star formation. The synthetic maps are made publicly available to provide novel models of the microwave sky.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

The Electromagnetic Counterpart of the Binary Neutron Star Merger LIGO/Virgo GW170817. III. Optical and UV Spectra of a Blue Kilonova from Fast Polar Ejecta

We present optical and ultraviolet spectra of the first electromagnetic counterpart to a gravitational-wave (GW) source, the binary neutron star merger GW170817. Spectra were obtained nightly between 1.5 and 9.5 days post-merger, using the Southern Astrophysical Research and Magellan telescopes; the UV spectrum was obtained with the Hubble Space Telescope at 5.5 days. Our data reveal a rapidly fading blue component (T≈5500 K at 1.5 days) that quickly reddens; spectra later than ≳4.5 days peak beyond the optical regime. The spectra are mostly featureless, although we identify a possible weak emission line at ∼7900 Å at t≲4.5 days. The colors, rapid evolution, and featureless spectrum are consistent with a “blue” kilonova from polar ejecta comprised mainly of light r-process nuclei with atomic mass number A≲140. This indicates a sightline within θ{sub obs}≲45{sup ∘} of the orbital axis. Comparison to models suggests ∼0.03 M {sub ⊙} of blue ejecta, with a velocity of ∼0.3c. The required lanthanide fraction is ∼10{sup −4}, but this drops to <10{sup −5} in the outermost ejecta. The large velocities point to a dynamical origin, rather than a disk wind, for this blue component, suggesting that both binary constituents are neutron stars (as opposed to a binary consisting of a neutron star and a black hole). For dynamical ejecta, the high mass favors a small neutron star radius of ≲12 km. This mass also supports the idea that neutron star mergers are a major contributor to r-process nucleosynthesis.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

The Electromagnetic Counterpart of the Binary Neutron Star Merger LIGO/Virgo GW170817. V. Rising X-Ray Emission from an Off-axis Jet

Here, we report the discovery of rising X-ray emission from the binary neutron star merger event GW170817. This is the first detection of X-ray emission from a gravitational-wave (GW) source. Observations acquired with the Chandra X-ray Observatory ( CXO ) at $t\approx 2.3$ days post-merger reveal no significant emission, with ${L}_{x}\lesssim 3.2\times {10}^{38}\,\mathrm{erg}\,{{\rm{s}}}^{-1}$ (isotropic-equivalent). Continued monitoring revealed the presence of an X-ray source that brightened with time, reaching ${L}_{x}\approx 9\times {10}^{38}\,\mathrm{erg}\,{{\rm{s}}}^{-1}$ at $\approx 15.1$ days post-merger. We interpret these findings in the context of isotropic and collimated relativistic outflows (both on- and off-axis). We find that the broadband X-ray to radio observations are consistent with emission from a relativistic jet with kinetic energy ${E}_{k}\sim {10}^{49-50}\,\mathrm{erg}$, viewed off-axis with ${\theta }_{\mathrm{obs}}\sim 20^\circ \mbox{--}40^\circ $. Our models favor a circumbinary density $n\sim {10}^{-4}\mbox{--}{10}^{-2}\,{\mathrm{cm}}^{-3}$, depending on the value of the microphysical parameter ${\epsilon }_{B}={10}^{-4}\mbox{--}{10}^{-2}$. A central-engine origin of the X-ray emission is unlikely. Future X-ray observations at $t\gtrsim 100$ days, when the target will be observable again with the CXO , will provide additional constraints to solve the model degeneracies and test our predictions. Our inferences on ${\theta }_{\mathrm{obs}}$ are testable with GW information on GW170817 from advanced LIGO/Virgo on the binary inclination.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

The DESI Y1 RR Lyrae catalog I: Empirical modeling of the cyclic variation of spectroscopic properties and a chemodynamical analysis of the outer halo

We present the catalog of RR Lyrae stars observed in the first year of operations of the Dark Energy Spectroscopic Instrument (DESI) survey. This catalog contains 6,240 RR Lyrae stars out to $\sim100$ kpc from the Galactic center and over 12,000 individual epochs with homogeneously-derived stellar atmospheric parameters. We introduce a novel methodology to model the cyclical variation of the spectroscopic properties of RR Lyrae from single-epoch measurements. We employ this method to infer the radial velocity and effective temperature variation of fundamental mode and first-overtone RR Lyrae stars and to determine their systemic velocities and mean temperatures. For fundamental mode pulsators, we obtain radial velocity curves with amplitudes of $\sim$30--50 km s$^{-1}$ and effective temperature curves with 300--1,000 K variations, whereas for first-overtone pulsators these amplitudes are $\sim20$ km s$^{-1}$ and $\sim 600$ K, respectively. We use our sample to study the metallicity distribution of the halo and its dependence on Galactocentric distance ($R_{\rm GC}$). Using a radius-dependent mixture model, we split the data into chemodynamically distinct components and find that our inner halo sample ($R_{\rm GC}\lesssim50$ kpc) is predominantly composed of stars with [Fe/H] $\sim-1.5$ dex and largely radial orbits (with an anisotropy parameter $\beta\sim0.94$), that we associate with the Gaia-Sausage-Enceladus merger event. Stars in the outer halo field exhibit a broader and more metal-poor [Fe/H] distribution with more circular orbits ($\beta\sim0.39$). The metallicity gradient of the metal-rich and the metal-poor components is found to be $0.005$ and $0.010$ dex kpc$^{-1}$, respectively. Our catalog highlights DESI's tantalizing potential for studying the Milky Way and the pulsation properties of RR Lyrae stars in the era of large spectroscopic surveys.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

Constraints on Inflationary Gravitational Waves with Two Years of SPT-3G Data

We present a measurement of the $B$-mode polarization power spectrum of the cosmic microwave background anisotropies at 32 $\le$$\ell$$<$ 502 for three bands centered at 95, 150, and 220 GHz using data from the SPT-3G receiver on the South Pole Telescope. This work uses SPT-3G observations from the 2019 and 2020 winter observing seasons of a $\sim$1500 deg$^2$ patch of sky that directly overlaps with fields observed with the BICEP/Keck family of telescopes, and covers part of the proposed Simons Observatory and CMB-S4 deep fields. Employing new techniques for mitigating polarized atmospheric noise, the SPT-3G data demonstrates a white noise level of 9.3 (6.7) $\mu$K-arcmin at $\ell \sim 500$ for the 95 GHz (150 GHz) data, with a $1/\ell$ noise knee at $\ell$=128 (182). We fit the observed six auto- and cross-frequency $B$-mode power spectra to a model including lensed $\Lambda$CDM $B$-modes and a combination of Galactic and extragalactic foregrounds. This work characterizes foregrounds in the vicinity of the BICEP/Keck survey area, finding foreground power consistent with that reported by the BICEP/Keck collaboration within the same region, and a factor of $\sim$ 3 higher power over the full SPT-3G survey area. Using SPT-3G data over the BICEP/Keck survey area, we place a 95% upper limit on the tensor-to-scalar ratio of $r < 0.25$ and find the statistical uncertainty on $r$ to be $\sigma(r) = 0.067$.

Zebrowski, J. A. [Chicago U., KICP; Chicago U., As↗
DOE OSTI2025

Diffusion Codes: Self-Correction from Small(er)-Set Expansion with Tunable Non-locality

Optimal constructions of classical LDPC codes can be obtained by choosing the Tanner graph uniformly at random among biregular graphs. We introduce a class of codes that we call ``diffusion codes'', defined by placing each edge connecting bits and checks on some graph, and acting on that graph with a random SWAP network. By tuning the depth of the SWAP network, we can tune a tradeoff between the amount of randomness -- and hence the optimality of code parameters -- and locality with respect to the underlying graph. For diffusion codes defined on the cycle graph, if the SWAP network has depth $\sim Tn$ with $T> n^{2β}$ for arbitrary $β>0$, then we prove that almost surely the Tanner graph is a lossless ``smaller set'' vertex expander for small sets up size $δ\sim \sqrt T \sim n^β$, with bounded bit and check degree. At the same time, the geometric size of the largest stabilizer is bounded by $\sqrt T$ in graph distance. We argue, based on physical intuition, that this result should hold more generally on arbitrary graphs. By taking hypergraph products of these classical codes we obtain quantum LDPC codes defined on the torus with smaller-set boundary and co-boundary expansion and the same expansion/locality tradeoffs as for the classical codes. These codes are self-correcting and admit single-shot decoding, while having the geometric size of the stabilizer growing as an arbitrarily small power law. Our proof technique establishes mixing of a random SWAP network on small subsystems at times scaling with only the subsystem size, which may be of independent interest.

Combinatorics (math.CO)↗
DOE OSTI2018

A protocol for an intercomparison of biodiversity and ecosystem services models using harmonized land-use and climate scenarios

Abstract. To support the assessments of the Intergovernmental Science-Policy Platform on Biodiversity and Ecosystem Services (IPBES), the IPBES Expert Group on Scenarios and Models is carrying out an intercomparison of biodiversity and ecosystem services models using harmonized scenarios (BES-SIM). The goals of BES-SIM are (1) to project the global impacts of land-use and climate change on biodiversity and ecosystem services (i.e., nature's contributions to people) over the coming decades, compared to the 20th century, using a set of common metrics at multiple scales, and (2) to identify model uncertainties and research gaps through the comparisons of projected biodiversity and ecosystem services across models. BES-SIM uses three scenarios combining specific Shared Socio-economic Pathways (SSPs) and Representative Concentration Pathways (RCPs) – SSP1xRCP2.6, SSP3xRCP6.0, SSP5xRCP8.6 – to explore a wide range of land-use change and climate change futures. This paper describes the rationale for scenario selection, the process of harmonizing input data for land use, based on the second phase of the Land Use Harmonization Project (LUH2), and climate, the biodiversity and ecosystem services models used, the core simulations carried out, the harmonization of the model output metrics, and the treatment of uncertainty. The results of this collaborative modeling project will support the ongoing global assessment of IPBES, strengthen ties between IPBES and the Intergovernmental Panel on Climate Change (IPCC) scenarios and modeling processes, advise the Convention on Biological Diversity (CBD) on its development of a post-2020 strategic plans and conservation goals, and inform the development of a new generation of nature-centred scenarios.

58 GEOSCIENCES↗
NASA NTRS1976

Economic analysis of standard interface modules for use with the multi-mission spacecraft. Volume 2: Appendices and drawings

The cost savings that could be obtained by the use of SIM to perform certain sensor electrical interfacing functions that were historically an integral part of the sensor are evaluated. Reduction in both the nonrecurring and recurring costs of this sensor interface hardware could be achieved through the use of SIM, and the study concludes that the development and use of certain power conditioning and data handling SIM units are economically justified.

Greenberg, J. S.↗
NASA NTRS1978

Aircraft simulation data management - A prototype system

Piloted flight simulations are used throughout the aircraft development process to evaluate design concepts, handling qualities and operational procedures. Simulation project managers are often inundated with data but without a convenient and efficient way to make the correlations and analyses necessary to evaluate system performance. A computer-based Simulation Management System (SIMS) is under development. SIMS will permit simulation project engineers to quickly acquire, access, display, edit, analyze, and document the information necessary to more efficiently manage the research program. SIMS features interactive, associative access to simulation data. This paper describes SIMDEM, a prototype system designed to demonstrate these concepts and procedures in order to obtain feedback from simulator users to guide system design.

Crane, D. F.↗
NASA NTRS1992

Improvements In Processing And Aiming For Squint-Mode SAR

Improved technique for aiming antenna of synthetic-aperture radar (SAR) operating in squint imaging mode (SIM) complements improved algorithm for processing raw SIM SAR data. Developed to reduce deleterious effects of two unique characteristics of SIM SAR: large range walk and large variation of Doppler centroid as function of range.

Chang, Chi Y.↗
NASA NTRS1991

Supportability to 'Mars...and beyond'

The development of a 'front-end' Integrated Logistics Support (ILS) strategic concept and a Supportability Index Model (SIM) for incorporation into future SEI engineering efforts is discussed. The ILS objectives and support strategy are examined. The SIM mission phases, which evaluates those items determined to be the most crucial for each mission phase in terms of a measure of supportability effectiveness, are summarized and the SIM data development and initial model results are reviewed.

Thurman, Loren A.↗
NASA NTRS1993

Stormtime transport of ring current and radiation belt ions

This is an investigation of stormtime particle transport that leads to formation of the ring current. Our method is to trace the guiding-center motion of representative ions (having selected first adiabatic invariants mu) in response to model substorm-associated impulses in the convection electric field. We compare our simulation results qualitatively with existing analytically tractable idealizations of particle transport (direct convective access and radial diffusion) in order to assess the limits of validity of these approximations. For mu approximately less than 10 MeV/G (E approximately less than 10 keV at L equivalent to 3) the ion drift period on the final (ring-current) drift shell of interest (L equivalent to 3) exceeds the duration of the main phase of our model storm, and we find that the transport of ions to this drift shell is appropriately idealized as direct convective access, typically from open drift paths. Ion transport to a final closed drift path from an open (plasma-sheet) drift trajectory is possible for those portions of that drift path that lie outside the mean stormtime separatrix between closed and open drift trajectories, For mu approximately 10-25 MeV/G (110 keV approximately less than E approximately less than 280 keV at L equivalent to 3) the drift period at L equivalent to 3 is comparable to the postulated 3-hr duration of the storm, and the mode of transport is transitional between direct convective access and transport that resembles radial diffusion. (This particle population is transitional between the ring current and radiation belt). For mu approximately greater than 25 MeV/G (radiation-belt ions having E approximately greater than 280 keV at L equivalent to 3) the ion drift period is considerably shorter than the main phase of a typical storm, and ions gain access to the ring-current region essentially via radial diffusion. By computing the mean and mean-square cumulative changes in 1/L among (in this case) 12 representative ions equally spaced in drift time around the steady-state drift shell of interest (L equivalent to 3), we have estimated (from both our forward and our time-reversed simulations) the time-integrated radial-diffusion coefficients D(sup sim)(sub LL) for particles having selected values of mu approximately greater than 15 MeV/G. The results agree surprisingly well with the predictions (D(sup ql)(sub LL)) of quasilinear radial diffusion theory, despite the rather brief duration (approximately 3 hrs) of our model storm and despite the extreme variability (with frequency) of the spectral-density function that characterizes the applied electric field during our model storm. As expected, the values of D(sup sim)(sub LL) deduced (respectively) from our forward and time-reversed simulations agree even better with each other and with D(sup sim)(sub LL) when the impulse amplitudes which characterize the individual substorms of our model storm are systematically reduced.

Chen, Margaret W.↗
NASA NTRS1995

Effects of low earth orbit on the optical performance of multi-layer enhanced high reflectance mirrors

Two mirror designs developed for space applications were flown along with a standard mid-infrared design on the leading and trailing edges of the Long Duration Exposure Facility (LDEF). Preliminary observations of induced changes in optical performance of ZnS-coated mirrors and impact-related microstructural and microchemical effects are described in the proceedings of the First LDEF Post-Retrieval Symposium. In this paper, effects of the induced environment and meteoroid/debris impacts on mirror performance are described in more detail. Also, an analysis of reflectance spectra using the results of Auger and secondary ion mass spectroscopy (SIMS) profiling measurements are used to identify an optical-degradation mechanism for the ZnS-coated mirrors. Structural damage associated with a high-velocity impact on a (Si/Al2O3)-coated mirror was imaged optically and with scanning electron and atomic force microscopy (SEM and AFM). Scanning Auger and SIMS analysis provided chemical mapping of selected impact sites. The impact data suggest design and fabrication modifications for obtaining improved mechanical performance using a design variation identified in preflight laboratory simulations. Auger surface profile and SIMS imaging data verified the conclusion that secondary impacts are the source of contamination associated with the dendrites grown on the leading-edge ZnS-coated test samples. It was also found that dendrites can be grown in the laboratory by irradiating contaminated sites on a trailing-edge ZnS-coated sample with a rastered electron beam. These results suggest a mechanism for dendrite growth.

Donovan, Terence↗
NASA NTRS1995

Stormtime ring current and radiation belt ion transport: Simulations and interpretations

We use a dynamical guiding-center model to investigate the stormtime transport of ring current and radiation-belt ions. We trace the motion of representative ions' guiding centers in response to model substorm-associated impulses in the convection electric field for a range of ion energies. Our simple magnetospheric model allows us to compare our numerical results quantitatively with analytical descriptions of particle transport, (e.g., with the quasilinear theory of radial diffusion). We find that 10-145-keV ions gain access to L approximately 3, where they can form the stormtime ring current, mainly from outside the (trapping) region in which particles execute closed drift paths. Conversely, the transport of higher-energy ions (approximately greater than 145 keV at L approximately 3) turns out to resemble radial diffusion. The quasilinear diffusion coefficient calculated for our model storm does not vary smoothly with particle energy, since our impulses occur at specific (although randomly determined) times. Despite the spectral irregularity, quasilinear theory provides a surprisingly accurate description of the transport process for approximately greater than 145-keV ions, even for the case of an individual storm. For 4 different realizations of our model storm, the geometric mean discrepancies between diffusion coefficients D(sup sim, sub LL) obtained from the simulations and the quasilinear diffusion coefficient D(sup ql, sub LL) amount to factors of 2.3, 2.3, 1.5, and 3.0, respectively. We have found that these discrepancies between D(sup sim, sub LL) and D(sup ql, sub LL) can be reduced slightly by invoking drift-resonance broadening to smooth out the sharp minima and maxima in D(sup ql, sub LL). The mean of the remaining discrepancies between D(sup sim, sub LL) and D(sup ql, sub LL) for the 4 different storms then amount to factors of 1.9, 2.1, 1.5, and 2.7, respectively. We find even better agreement when we reduce the impulse amplitudes systematically in a given model storm (e.g., reduction of all the impulse amplitudes by half reduces the discrepancy factor by at least its square root) and also when we average our results over an ensemble of 20 model storms (agreement is within a factor of 1.2 without impulse-amplitude reduction). We use our simulation results also to map phase-space densities f in accordance with Liouville's theorem. We find that the stormtime transport of approximately greater than 145-keV ions produces little change in f-bar the drift-averaged phase-space density on any drift shell of interest. However, the stormtime transport produces a major enhancement from the pre-storm phase-space density at energies approximately 30-145 keV, which are representative of the stormtime ring current.

Lyons, Larry R.↗
NASA NTRS1996

Sputtering Erosion in Ion and Plasma Thrusters

Low energy sputtering of molybdenum, tantalum and boron nitride with xenon ions are being studied using secondary neutral and secondary ion mass spectrometry (SNMS/SIMS). An ultrahigh vacuum chamber was used to conduct the experiment at a base pressure of 1x10(exp -9) torr. The primary ion beam is generated by an ion gun which is capable of delivering ion currents in the range of 20 to 500 nA. The ion beam can be focused to a spot size of approximately 1 mm in diameter. The mass spectrometer is positioned 10 mm from the target and 90 deg to the primary ion beam direction. SNMS and SIMS spectra were collected at various incident angles and different ion energies. For boron nitride sputtering, the target was flooded with an electron beam to neutralize the charge buildup on the surface. In the SNMS mode, sputtering of Mo and Ta can be detected at an ion energy as low as 100 eV whereas in boron nitride the same was observed up to an energy of 300 eV. However, in the positive-SIMS mode, the sputtering of Mo was observed at 10 eV incident ion energy. The SIMS spectra obtained for boron nitride clearly identifies the two isotopes of boron as well as cluster ions such as B2(sup +) and molecular ions such as BN(sup +). From the angle versus yields measurements, it was found that the maximum SNMS yield shifts towards lower incident angles at low ion energies for all three samples.

Ray, Pradosh K.↗
NASA NTRS1995

Long Duration Exposure Facility

The Long Duration Exposure Facility (LDEF) materials were useful for testing technical concepts that needed to be validated for the Cosmic Dust Collector Facility (CDCF) - a large instrument that was under study for inclusion on the upcoming Space Station. As it turned out, CDCF, which was approved at one point as an external payload, was ultimately canceled due to the scaling back of the Space Station capabilities. However, the study of cosmic dust is still a field of great interest for NASA, being the crucial part of at least one experiment that is still being considered for a Discovery mission. The optimum analysis of hypervelocity impacts is thus a continuing NASA concern. Two experiments, AO187-1 and AO187-2 were explicitly designed to measure the flux and composition of dust particles impacting LDEF. The former consisted of flat targets of Au and Al while the second comprised a set of 237 "capture cells" using Ge target plates covered by thin (2.5 microns) metallized plastic foils. The spacecraft maintained a constant orientation with respect to its velocity vector thereby defining leading and trailing edges that faced respectively into and away from the direction of motion. Both AO187-1 and AO187-2 had detectors on both the leading and trailing edges of LDEF. It was expected that interplanetary dust particles would dominate impacts on the trailing edge while the leading edge would be exposed to both cosmic dust and particles of orbital manmade debris. In AO187-1, the compositions of the impactors was determined by SEM-EDS techniques; in AO187-2 a sensitive surface analysis technique - SIMS - was used to determine both elemental and (some) isotopic compositions. In the initial analysis of AO187-2, it was found that SIMS was more sensitive for the analysis of thin impact debris layers than SEM-EDS. The present grant was made to determine if SIMS analysis could also be applied to impacts recorded in the Au surfaces of AO187-1. Success would extend the analysis of AO187-1 and would also contribute important technical information for the design of future cosmic dust space missions. The results obtained with this grant are incorporated in the attached paper presented at the Third LDEF Symposium and are briefly summarized here. In addition, we comment on the potential implications of this work for future research.

Source record↗
NASA NTRS2000

Differences in Acceleration Training and Exercise Training on Resting Cardiovascular Variables

The relative effects of alternating exercise vs. acclamation training an mean blood pressure (BP, Finapres), cardiac output (CO, BoMed) and peripheral resistance (PR, calculated) were evaluated. Six healthy men (33$\pm$(SD)6 yr. 178$\pm$4 cm, 86$\pm$6 kg) underwent exercise training (ET, n=3): supine on a cycle ergometer (40 to 90\% Vo$_{2}$ max) during exposure to constant+1G$_{z}$ for $\sim$30 min/day for 14 days on NASA's 1.9m Human Powered Centrifuge (HPC). They also underwent oscillatory (between +1 G$ {z}$and$\sim$2.5G$_{z}$) acceleration training (AT, n=3) for $\sim$30 min/day for 14 days on the HPC. After four weeks of ambulatory deconditioning, training protocols were switched. AT increased resting CO by 9.MpmS(SE)3.2\% (p$less than$0.05) with no effect on BF, and ET decreased BP by 9.2$\pm$4.6\% (p$less than$0.08) as well as spectral power of PR by 41$\pm$9\% (p$less than$0.05). The major effect of acceleration training was to increase resting cardiac output while that of exercise mining was to decrease resting blood pressure.

Evans, J. M.↗
NASA NTRS2001

High Resolution Chemical Study of ALH84001

We have studied the chemistry of a sample of the SNC meteorite ALH84001 using an environmental scanning electron microscope (ESEM) with an energy dispersive chemical analytical detector and a focused ion beam secondary ion mass spectrometer (FIB-SIMS). Here we present the chemical data, both spectra and images, from two techniques that do not require sample preparation with a conductive coating, thus eliminating the possibility of preparation-induced textural artifacts. The FIB-SIMS instrument includes a column optimized for SEM with a quadrupole type mass spectrometer. Its spatial and spectral resolution are 20 nm and 0.4 AMU, respectively. The spatial resolution of the ESEM for chemical analysis is about 100 nm. Limits of detection for both instruments are mass dependent. Both the ESEM and the FIB-SIMS instrument revealed contrasting surficial features; crumbled, weathered appearance of the matrix in some regions as well as a rather ubiquitous presence of euhedral halite crystals, often associated with cracks or holes in the surface of the rock. Other halogen elements present in the vicinity of the NaCl crystals include K and Br. In this report, elemental inventories are shown as mass spectra and as X-ray maps.

Conrad, Pamela G.↗