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At least 649 records · Page 36

Lithological maps of selected Apollo 14 Breccia samples

A booklet of mapped surfaces of some Apollo 14 samples was prepared as an intermediate step towards the preparation of a new Apollo 14 sample catalog. It contains recently obtained observations and pictures of some of the largest and less well documented Apollo breccia samples. Some of the samples (14303, 14305, 14306, and 14311) were chosen because they have large sawn surfaces. These were dusted and mapped using a binocular microscope through the window of the nitrogen cabinet.

Twedell, D. B.↗

A Ratio of Spore to Viable Organisms: A Case Study of the JPL-SAF Cleanroom

Spacecraft surfaces that are destined to land on potential life-harboring celestial bodies are required to be rigorously cleaned and continuously monitored for spore bioburden as a proxy for spacecraft cleanliness. The NASA standard assay (NSA), used for spacecraft bioburden estimates, specifically measures spores that are cultivable, aerobic, resistant to heat shock, and grow at 30 C in a nutrient-rich medium. Since the vast majority of microorganisms cannot be cultivated using the NSA, it is necessary to utilize state-of-the art molecular techniques to better understand the presence of all viable microorganisms, not just those measured with the NSA. In this study, the nutrient-deprived low biomass cleanrooms, where spacecraft are assembled, were used as a surrogate for spacecraft surfaces to measure the ratio of NSA spores in relation to the total viable microorganism population in order to make comparisons with the 2006 Space Studies Board (SSB) estimate of 1 spore per approximately 50,000 viable organisms. Ninety-eight surface wipe samples were collected from the Spacecraft Assembly Facility (SAF) cleanroom at the Jet Propulsion Laboratory (JPL) over a 6-month period. The samples were processed and analyzed using classical microbiology along with molecular methodology. Traditional microbiology plating methods were used to determine the cultivable bacterial, fungal, and spore populations. Molecular assays were used to determine the total organisms (TO, dead and live) and the viable organisms (VO, live). The TO was measured using adenosine triphosphate (ATP) and quantitative polymerase chain reaction (qPCR) assays. The VO was measured using internal ATP, propidium monoazide (PMA)-qPCR, and flow cytometry (after staining for viable microorganisms) assays. Based on the results, it was possible to establish a ratio between spore counts and VO for each viability assay. The ATP-based spore to VO ratio ranged from 149-746, and the bacterial PMA-qPCR assay-based ratio ranged from 314-1,491 VO, per spore. The most conservative estimate came from fluorescent-assisted cell sorting (FACS), which estimated the ratio to be 12,091 VO per 1 NSA spore. Since archaeal (less than 1%) and fungal (approximately 2%) populations were negligible, the spore to VO ratios were based on bacterial population estimates. The most conservative ratio from this study can be used as a replacement for the SSB estimate on nutrient-deprived (oligotrophic) desiccated spacecraft surfaces, to estimate the VO from NSA measurements without utilizing state-of-the art molecular methods that are costly and require more biomass than is typically found on spacecraft surfaces.

Hendrickson, Ryan↗

Overview of the Mars Sample Return Earth Entry Vehicle

NASA's Mars Sample Return (MSR) project will bring Mars surface and atmosphere samples back to Earth for detailed examination. Langley Research Center's MSR Earth Entry Vehicle (EEV) is a core part of the mission, protecting the sample container during atmospheric entry, descent, and landing. Planetary protection requirements demand a higher reliability from the EEV than for any previous planetary entry vehicle. An overview of the EEV design and preliminary analysis is presented, with a follow-on discussion of recommended future design trade studies to be performed over the next several years in support of an MSR launch in 2018 or 2020. Planned topics include vehicle size for impact protection of a range of sample container sizes, outer mold line changes to achieve surface sterilization during re-entry, micrometeoroid protection, aerodynamic stability, thermal protection, and structural materials selection.

Dillman, Robert↗

Electron spectroscopy analysis

The Surface Science Laboratories at the University of Alabama in Huntsville (UAH) are equipped with x-ray photoelectron spectroscopy (XPS or ESCA) and Auger electron spectroscopy (AES) facilities. These techniques provide information from the uppermost atomic layers of a sample, and are thus truly surface sensitive. XPS provides both elemental and chemical state information without restriction on the type of material that can be analyzed. The sample is placed into an ultra high vacuum (UHV) chamber and irradiated with x-rays which cause the ejection of photoelectrons from the sample surface. Since x-rays do not normally cause charging problems or beam damage, XPS is applicable to a wide range of samples including metals, polymers, catalysts, and fibers. AES uses a beam of high energy electrons as a surface probe. Following electronic rearrangements within excited atoms by this probe, Auger electrons characteristic of each element present are emitted from the sample. The main advantage of electron induced AES is that the electron beam can be focused down to a small diameter and localized analysis can be carried out. On the rastering of this beam synchronously with a video display using established scanning electron microscopy techniques, physical images and chemical distribution maps of the surface can be produced. Thus very small features, such as electronic circuit elements or corrosion pits in metals, can be investigated. Facilities are available on both XPS and AES instruments for depth-profiling of materials, using a beam of argon ions to sputter away consecutive layers of material to reveal sub-surface (and even semi-bulk) analyses.

Gregory, John C.↗

Surveyor III A preliminary report

Near the eastern shore of Oceanus Procellarum, 390 miles from Surveyor I, stands Surveyor III, now motionless and silent after a full lunar day's work during which the spacecraft transmitted to Earth 6315 photographs of its surroundings. A surface sampler, operated by command from the Earth and in view of Surveyor's television camera, conducted many tests of the character and structure of the lunar surface material, as well as digging four trenches. While Surveyor I put man's eyes on the Moon, Surveyor III added an arm and a hand with which to work. In this mission, Surveyor displayed remarkable adaptability and stability. Because the engines did not cut off before touchdown, the spacecraft in effect made three separate landings, giving information on surface bearing strength in several places. The spacecraft came to rest at an angle of about 14° from the vertical, well below the rim of a crater, making possible a detailed study of the floor and walls of a small lunar crater. The tilted position of the spacecraft also made it possible to obtain, for the first time from the surface of the Moon, photographs of a solar eclipse, and of the Earth in color. This report presents the preliminary findings from Surveyor III of the team of scientists and engineers of the Surveyor Program.

Surface property↗

A method of treating the non-grey error in total emittance measurements

In techniques for the rapid determination of total emittance, the sample is generally exposed to surroundings that are at a different temperature than the sample's surface. When the infrared spectral reflectance of the surface is spectrally selective, these techniques introduce an error into the total emittance values. Surfaces of aluminum overcoated with oxides of various thicknesses fall into this class. Because they are often used as temperature control coatings on satellites, their emittances must be accurately known. The magnitude of the error was calculated for Alzak and silicon oxide-coated aluminum and was shown to be dependent on the thickness of the oxide coating. The results demonstrate that, because the magnitude of the error is thickness-dependent, it is generally impossible or impractical to eliminate it by calibrating the measuring device.

Heaney, J. B.↗

Services provided in support of the planetary quarantine requirements

Results are presented of laboratory experiments conducted on the thermal resistance of naturally occurring airborne spores and microbiological examinations of space hardware using long-term slit samplers and rodac plate and swab-rinse methods of sampling environmental surfaces.

Favero, M. S.↗

Holographic nondestructive testing with impact excitation.

Review of some experimental results of bond flaw detection in composite materials by holographic recording of the surface of samples subjected to mechanical impact. The resulting deformation of the samples recorded in a sequence of double exposure holograms at increasingly longer time intervals after impact renders the presence of flaws observable. A proposed deformation enhancement technique increases detection sensitivity and is helpful in visualizing smaller flaws.

Chu, W. P.↗

Apollo soil mechanics experiment S-200

The physical and mechanical properties of the unconsolidated lunar surface material samples that were obtained during the Apollo missions were studied. Sources of data useful for deduction of soil information, and methods used to obtained the data are indicated. A model for lunar soil behavior is described which considers soil characteristics, density and porosity, strength, compressibility, and trafficability parameters. Lunar history and processes are considered, and a comparison is made of lunar and terrestrial soil behavior. The impact of the findings on future exploration and development of the moon are discussed, and publications resulting from lunar research by the soil mechanics team members are listed.

Mitchell, J. K.↗

Refinement in black chrome for use as a solar selective coating

Black chrome is significant as a solar selective coating because the current extensive use of black chrome in the electroplating industry as a durable decorative finish makes black chrome widely available on a commercial scale and potentially low in cost as a solar selective coating. Black-chrome deposits were modified by underplating with dull nickel or by being plated on rough surfaces. Both of these procedures increased the visible absorptance. There was no change in the infrared reflectance for the dull-nickel - black-chrome combination from that reported for the bright-nickel - black-chrome combination. However, the bright-nickel - black-chrome coating plated on rough surfaces indicated a slight decrease in infrared reflectance. As integrated over the solar spectrum for air mass 2, the reflectance of the dull-nickel - black-chrome coating was 0.077, of the bright-nickel - black-chrome coating plated on a 0.75-micron (30-microinch) surface was 0.070, of the bright-nickel - black-chrome coating plated on a 2.5 micron (100-microinch) surface was 0.064. The corresponding values for the bright-nickel - black-chrome coating on a 0.0125-micron (0.5-microinch) surface, two samples of black nickel, and two samples of Nextrel black paint were 0.132, 0.123, 0.133, and 0.033, respectively.

Mcdonald, G. E.↗

Examination of Apollo 17 surface fines for porphyrins and aromatic hydrocarbons

An Apollo 17 surface fines sample 75081,78, collected from Station 5, was extracted and examined fluorometrically. No porphyrins were found with fluorometric methods capable of detecting 2 times 10 to the minus 14th moles/g of Ni-mesoporphyrin IX in the sample. Also aromatic hydrocarbons were undetected.

Rho, J. H.↗

Lunar surface phenomena - Solar flare track gradients, microcraters, and accretionary particles

Data are presented concerning the energy spectra of solar flare particles and the distribution of particles producing submicron diameter craters. Processes which alter the albedo and possibly the chemistry of exposed lunar surfaces are also considered. Measurements are reported of solar flare track gradients in rock 64455 which is sufficiently young to have uneroded surfaces on its sides. Attention is also given to accretionary particles adhering to host surfaces, microcraters on soil particles, and microcraters on the oriented surfaces of sample 76015 from a boulder at Station 6 of the Apollo 17 site.

Blanford, G. E.↗