Interference and radiation blockage effects on surface temperatures of composite flight vehicles
Interference effects on aerodynamic heating and radiation blockage effects on surface temperature of space shuttle during boost
Thomas, A. C.↗
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Fabrication and surface characterization of composite refractory compounds suitable for thermionic converters
The techniques of fabricating and characterizing the surface properties of electrode materials were investigated. The basic surface properties of these materials were studied with respect to their utilization as thermionic energy converter electrodes. Emphasis was placed on those factors (e.g, cesium disorption kinetic and mechanisms of low work function production) which are of primary concern to thermionic converter performance.
Davis, P. R.↗
Remote Sensing of Icy Galilean Moon Surface and Atmospheric Composition Using Low Energy (1 eV-4 keV) Neutral Atom Imaging
We describe a low energy neutral atom imager suitable for composition measurements Europa and other icy Galilean moons in the Jovian magnetosphere. This instrument employs conversion surface technology and is sensitive to either neutrals converted to negative ions, neutrals converted to positive ions and the positive ions themselves depending on the power supply. On a mission such as the Jupiter Icy Moons Orbiter (JIMO), two back-to-back sensors would be flown with separate power supplies fitted to the neutral atom and iodneutral atom sides. This will allow both remote imaging of 1 eV < E < 4 keV neutrals from icy moon surfaces and atmospheres, and in situ measurements of ions at similar energies in the moon ionospheres and Jovian magnetospheric plasma. The instrument provides composition measurements of the neutrals and ions that enter the spectrometer with a mass resolution dependent on the time-of-flight subsystem and capable of resolving molecules. The lower energy neutrals, up to tens of eV, arise from atoms and molecules sputtered off the moon surfaces and out of the moon atmospheres by impacts of more energetic (keV to MeV) ions from the magnetosphere. Direct Simulation Monte Carlo (DSMC) models are used to convert measured neutral abundances to compositional distributions of primary and trace species in the sputtered surfaces and atmospheres. The escaping neutrals can also be detected as ions after photo- or plasma-ionization and pickup. Higher energy, keV neutrals come from charge exchange of magnetospheric ions in the moon atmospheres and provide information on atmospheric structure. At the jovicentric orbits of the icy moons the presence of toroidal gas clouds, as detected at Europa's orbit, provide M e r opportunities to analyze both the composition of neutrals and ions originating from the moon surfaces, and the characteristics of magnetospheric ions interacting with neutral cloud material. Charge exchange of low energy ions near the moons, and directional distributions of the resultant neutrals, allow indirect global mapping of magnetic field structures around the moons. Temporal variation of the magnetic structures can be linked to induced magnetic fields associated with subsurface oceans.
Collier, M. R.↗
Fracture surface characteristics of off-axis composites
The fracture surface characteristics of off-axis high-modulus graphite-fiber/epoxy composite specimens were studied using a scanning electron microscope (SEM). The specimens were subjected to tensile loading at various angles (0-90 deg) to the fiber direction. SEM photomicrographs of the fractured surfaces revealed three different load angle regions with distinct fracture characteristics. Based on these revelations, criteria were established which can be used to characterize fracture surfaces with respect to a predominant 'single-stress' fracture mode.
Sinclair, J. H.↗
Fracture surface characteristics of off-axis composites
The fracture surface characteristics of off-axis high-modulus graphite-fiber/epoxy composite specimens were studied, using a scanning electron microscope (SEM). The specimens were subjected to tensile loading at various angles (0 deg - 90 deg) to the fiber direction. SEM photomicrographs of the fractured surfaces revealed three different load angle regions with distinct fracture characteristics. Based on these revelations, criteria were established which can be used to characterize fracture surfaces with respect to a predominant single stress fracture mode.
Sinclair, J. H.↗
Fracture surface characteristics of notched angleplied graphite/epoxy composites
Composite fracture surface characteristics and related fracture modes have been investigated through extensive microscopic inspections of the fracture surfaces of notched angleplied graphite/epoxy laminates. The investigation involved 4 ply laminates of the configuration + or - theta (s) where theta = 0 deg, 3 deg, 5 deg, 10 deg, 15 deg, 30 deg, 45 deg, 60 deg, 75 deg, and 90 deg. Two-inch wide tensile specimens with 0.25 in. by 0.05 in. through-slits centered across the width were tested to fracture. The fractured surfaces were then removed and examined using a scanning electron microscope. Evaluation of the photomicrographs combined with analytical results obtained using the CODSTRAN computer code culminated in a unified set of fracture criteria for determining the mode of fracture in notched angleplied graphite/epoxy laminates.
Ginty, C. A.↗
Surface evolution of synthetic bilgewater emulsion
Bilgewater is oil-in-water emulsion emitted from shipboard and it is a source of pollution to the ocean. Wastewater treatment needs fundamental knowledge of the bilgewater surface changes; however, limited information is available. We have reported the first surface characterization of synthetic bilgewater emulsion using time-of-flight secondary ion mass spectrometry (ToF-SIMS) coupled with optical microscopy. A NAVY synthetic bilgewater emulsion consisting of three oils and a detergent mixture is used as the synthetic bilgewater model. Both fresh and aged emulsion samples are analyzed to determine their droplet size distributions (DSDs) and surface chemical compositions. Our results show that fresh emulsions are largely mono-modal with hydrocarbon fragments as the main surface composition. Aged emulsions are also monomodal with slightly larger size. Both SIMS spectral comparison and Principal Component Analysis (PCA) show that some surfactant components appear on the fresh emulsion surface immediately while larger molecular weight components appear at the aged bilge droplet surface. Our results indicate that the oil-water interface evolves after emulsion droplet forms. More importantly, surface evolution not only changes the bilgewater DSD but also surface chemical composition and reactivity.
bilgewater, droplet size distribution, ToF-SIMS, s↗
Ferromagnetic resonance and magnetic studies of cores 60009/60010 and 60003 - Compositional and surface-exposure stratigraphy
Ferromagnetic resonance and static magnetic measurements were made on 131 samples from core 60009/60010 and on 40 samples from section 60003 of the Apollo 16 deep drill core. These studies provided depth profiles for composition, in terms of the concentration of FeO, and relative surface exposure age (or maturity), in terms of the values of the specific FMR intensity normalized to the FeO content. For core 60009/60010, the concentration of FeO ranged from about 1.6 wt.% to 5.8 wt.% with a mean value of 4.6 wt.% and the maturity ranged from immature to mature with most of the soils being submature. A systematic decrease in maturity from the lunar surface to a depth of about 12.5 cm was observed in core section 60010. For core section 60003, the concentration of FeO ranged from about 5.2 wt.% to 7.5 wt.% with a mean value of 6.4 wt.% and the maturity ranged from submature to mature with most of the soils being mature.
Morris, R. V.↗
Fracture surface analysis in composite and titanium bonding
To understand the mechanical properties of fiber-reinforced composite materials, it is necessary to understand the mechanical properties of the matrix materials and of the reinforcing fibers. Another factor that can affect the mechanical properties of a composite material is the interaction between the fiber and the matrix. In general, composites with strong fiber matrix bonding will give higher modulus, lower toughness composites. Composites with weak bonding will have a lower modulus and more ductility. The situation becomes a bit more complex when all possibilities are examined. To be considered are the following: the properties of the surface layer on the fiber, the interactive forces between polymer and matrix, the surface roughness and porosity of the fiber, and the morphology of the matrix polymer at the fiber surface. In practice, the surface of the fibers is treated to enhance the mechanical properties of a composite. These treatments include anodization, acid etching, high temperature oxidation, and plasma oxidation, to name a few. The goal is to be able to predict the surface properties of carbon fibers treated in various ways, and then to relate surface properties to fiber matrix bonding.
Devilbiss, T. A.↗
Average chemical composition of the lunar surface
The available data on the chemical composition of the lunar surface at eleven sites (3 Surveyor, 5 Apollo and 3 Luna) are used to estimate the amounts of principal chemical elements (those present in more than about 0.5% by atom) in average lunar surface material. The terrae of the moon differ from the maria in having much less iron and titanium and appreciably more aluminum and calcium.
Turkevich, A. L.↗
The composition of Phobos - Evidence for carbonaceous chondrite surface from spectral analysis
In connection with a need for more definitive information concerning the composition of Phobos in a study of its origin, an ultraviolet-visible-infrared reflectance spectrum of the Martian satellite was compiled from the Mariner 9 ultraviolet spectrometer, Viking lander imaging, and ground-based photometric data. The probable surface composition of Phobos was deduced by comparing the obtained spectrum with the spectra of asteroids of known composition. The considered data show that the reflectivity of Phobos is flat from 1100 to 400 nm but decreases sharply in the ultraviolet to about 1 percent at 212 nm. The reflectance spectrum is similar to the spectra of asteroids Ceres and Pallas which were found to have surface compositions similar to that of carbonaceous chondrites. It is concluded that the surface composition of Phobos is also similar to that of carbonaceous chondrites. The results of the investigation point to different modes of origin for Mars and Phobos.
Pang, K. D.↗
A Real-Time MODIS Vegetation Composite for Land Surface Models and Short-Term Forecasting
The NASA Short-term Prediction Research and Transition (SPoRT) Center is producing real-time, 1- km resolution Normalized Difference Vegetation Index (NDVI) gridded composites over a Continental U.S. domain. These composites are updated daily based on swath data from the Moderate Resolution Imaging Spectroradiometer (MODIS) sensor aboard the polar orbiting NASA Aqua and Terra satellites, with a product time lag of about one day. A simple time-weighting algorithm is applied to the NDVI swath data that queries the previous 20 days of data to ensure a continuous grid of data populated at all pixels. The daily composites exhibited good continuity both spatially and temporally during June and July 2010. The composites also nicely depicted high greenness anomalies that resulted from significant rainfall over southwestern Texas, Mexico, and New Mexico during July due to early-season tropical cyclone activity. The SPoRT Center is in the process of computing greenness vegetation fraction (GVF) composites from the MODIS NDVI data at the same spatial and temporal resolution for use in the NASA Land Information System (LIS). The new daily GVF dataset would replace the monthly climatological GVF database (based on Advanced Very High Resolution Radiometer [AVHRR] observations from 1992-93) currently available to the Noah land surface model (LSM) in both LIS and the public version of the Weather Research and Forecasting (WRF) model. The much higher spatial resolution (1 km versus 0.15 degree) and daily updates based on real-time satellite observations have the capability to greatly improve the simulation of the surface energy budget in the Noah LSM within LIS and WRF. Once code is developed in LIS to incorporate the daily updated GVFs, the SPoRT Center will conduct simulation sensitivity experiments to quantify the impacts and improvements realized by the MODIS real-time GVF data. This presentation will describe the methodology used to develop the 1-km MODIS NDVI composites and show sample output from summer 2010, compare the MODIS GVF data to the AVHRR monthly climatology, and illustrate the sensitivity of the Noah LSM within LIS and/or the coupled LIS/WRF system to the new MODIS GVF dataset.
Case, Jonathan L.↗
Fabrication and surface characterization of composite refractory compounds suitable for thermionic converters
Procedures for fabricating high purity single crystals of LaB6 and SmB6 have been developed. Auger spectroscopy shows that a clean surface can be obtained by thermal heating at 1700 K; such a clean surface gives a value of B/La of 2.3 to 2.6 for the (100) face. The measured thermionic and FERP work functions of the (100) face of LaB6 are 2.47 and 2.28 eV, respectively. The electron reflection coefficient for LaB6(100) increases near zero primary energy to 0.5. Flash thermal desorption of an oxygen dosed surface showed that B2O3 is the desorption product at 1600 to 1700 K. A work function increase of 1.6 eV was observed on oxygen adsorption on LaB6(100). Thermal desorption of Co occurs at approximately 1300 K. A reduction of the work function to 1.39 eV was observed on adsorption of a partial monolayer of Cs on LaB6(100). The evaporation of LaB6 occurs as atomic La and B with a value of B/La of 6 to 3 in the temperature range 1700 to 2000 K. The activation energies of desorption for La and B are 6.3 + or - 0.3 and 6.8 + or - 0.3 eV, respectively.
Swanson, L. W.↗
PERCIVAL mission to Mars
With the downturn of the world economy, the priority of unmanned exploration of the solar system has been lowered. Instead of foregoing all missions to our neighbors in the solar system, a new philosophy of exploration mission design has evolved to insure the continued exploration of the solar system. The 'Discovery-class' design philosophy uses a low cost, limited mission, available technology spacecraft instead of the previous 'Voyager-class' design philosophy that uses a 'do-everything at any cost' spacecraft. The Percival Mission to Mars was proposed by Ares Industries as one of the new 'Discovery-class' of exploration missions. The spacecraft will be christened Percival in honor of American astronomer Percival Lowell who proposed the existence of life on Mars in the early twentieth century. The main purpose of the Percival mission to Mars is to collect and relay scientific data to Earth suitable for designing future manned and unmanned missions to Mars. The measurements and observations made by Percival will help future mission designers to choose among landing sites based on the feasibility and scientific interest of the sites. The primary measurements conducted by the Percival mission include gravity field determination, surface and atmospheric composition, sub-surface soil composition, sub-surface seismic activity, surface weather patterns, and surface imaging. These measurements will be taken from the orbiting Percival spacecraft and from surface penetrators deployed from Mars orbit. The design work for the Percival Mission to Mars was divided among four technical areas: Orbits and Propulsion System, Surface Penetrators, Gravity and Science Instruments, and Spacecraft Structure and Systems. The results for each of the technical areas is summarized and followed by a design cost analysis and recommendations for future analyses.
Reed, David W.↗
Laser ablation sampling system and method
A method and system for sampling a solid sample material can include the step of mounting the sample material on a support. A sample surface is coated with a surface treatment composition in a dry deposition process. A solvent supply conduit for supplying solvent to the sample surface and a solvent exhaust conduit for withdrawing solvent from the sample surface can be provided. Solvent is flowed from the solvent supply conduit to the surface treatment composition and the sample surface such that the solvent contacts the surface treatment composition. A laser beam is directed from a laser source to the sample and the surface treatment composition. The laser beam will ablate the sample and the surface treatment composition in portions intersected by the laser beam. Ablated sample material enters the solvent liquid and will be transported with the solvent away from the sample surface through the solvent exhaust conduit.
Kertesz, Vilmos↗
Laser ablation sampling system and method
A method and system for sampling a solid sample material can include the step of mounting the sample material on a support. A sample surface is coated with a surface treatment composition in a dry deposition process. A solvent supply conduit for supplying solvent to the sample surface and a solvent exhaust conduit for withdrawing solvent from the sample surface can be provided. Solvent is flowed from the solvent supply conduit to the surface treatment composition and the sample surface such that the solvent contacts the surface treatment composition. A laser beam is directed from a laser source to the sample and the surface treatment composition. The laser beam will ablate the sample and the surface treatment composition in portions intersected by the laser beam. Ablated sample material enters the solvent liquid and will be transported with the solvent away from the sample surface through the solvent exhaust conduit.
Kertesz, Vilmos↗
Temperature Dependence of Individual Absorptions Bands in Olivine: Implications for Inferring Compositions of Asteroid Surfaces from Spectra
The temperature variations of individual absorptions in olivine are modeled and found to narrow, move slightly in position, and change in relative strength as predicted by theory. These thermal changes may be confused with compositional differences.
Sunshine, J. M.↗
Electronic materials high-T(sub c) superconductivity polymers and composites structural materials surface science and catalysts industry participation
The fifth year of the Center for Advanced Materials was marked primarily by the significant scientific accomplishments of the research programs. The Electronics Materials program continued its work on the growth and characterization of gallium arsenide crystals, and the development of theories to understand the nature and distribution of defects in the crystals. The High Tc Superconductivity Program continued to make significant contributions to the field in theoretical and experimental work on both bulk materials and thin films and devices. The Ceramic Processing group developed a new technique for cladding YBCO superconductors for high current applications in work with the Electric Power Research Institute. The Polymers and Composites program published a number of important studies involving atomistic simulations of polymer surfaces with excellent correlations to experimental results. The new Enzymatic Synthesis of Materials project produced its first fluorinated polymers and successfully began engineering enzymes designed for materials synthesis. The structural Materials Program continued work on novel alloys, development of processing methods for advanced ceramics, and characterization of mechanical properties of these materials, including the newly documented characterization of cyclic fatigue crack propagation behavior in toughened ceramics. Finally, the Surface Science and Catalysis program made significant contributions to the understanding of microporous catalysts and the nature of surface structures and interface compounds.
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