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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 73 records · Page 4

All sources NASA NTRS DOE OSTI

NASA NTRS2006

Electrostatic Properties of PE and PTFE Subjected to Atmospheric Pressure Plasma Treatment; Correlation of Experimental Results with Atomistic Modeling

The use of an atmospheric pressure glow discharge (APGD) plasma was used at KSC to increase the hydrophilicity of spaceport materials to enhance their surface charge dissipation and prevent possible ESD in spaceport operations. Significant decreases in charge decay times were observed after tribocharging the materials using the standard KSC tribocharging test. The polarity and amount of charge transferred was dependent upon the effective work function differences between the respective materials. In this study, polyethylene (PE) and polytetrafluoroethylene (PTFE) were exposed to a He+O2 APGD. The pre and post treatment surface chemistry was analyzed by X-ray photoelectron spectroscopy and contact angle measurements. Semi-empirical and ab initio calculations were performed to correlate the experimental results with some plausible molecular and electronic structure features of the oxidation process. For the PE, significant surface oxidation was observed, as indicated by XPS showing C-O, C=O, and O-C=O bonding, and a decrease in the surface contact angle from 98.9 deg to 61.2 deg. For the PTFE, no C-O bonding appeared and the surface contact angle increased indicating the APGD only succeeded in cleaning the PTFE surface without affecting the surface structure. The calculations using the PM3 and DFT methods were performed on single and multiple oligomers to simulate a wide variety of oxidation scenarios. Calculated work function results suggest that regardless of oxidation mechanism, e.g. -OH, =0 or a combination thereof, the experimentally observed levels of surface oxidation are unlikely to lead to a significant change in the electronic structure of PE and that its increased hydrophilic properties are the primary reason for the observed changes in its electrostatic behavior. The calculations for PTFE argue strongly against significant oxidation of that material, as confirmed by the XPS results.

Trigwell, Steve↗

DOE OSTI2013

Integrated Data Collection Analysis (IDCA) Program — Bullseye ® Smokeless Powder

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of Bullseye ® smokeless powder (Gunpowder). The participants found the Gunpowder: 1) to have a range of sensitivity to impact, from less than RDX to almost as sensitive as PETN, 2) to be moderately sensitive to BAM and ABL friction, 3) have a range for ESD, from insensitive to more sensitive than PETN, and 4) to have thermal sensitivity about the same as PETN and RDX.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2013

Integrated Data Collection Analysis (IDCA) Program - RDX Standard Data Set 2

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2022

Wallops Flight Facility Integration and Testing Customer Handbook

The Wallops Integration and Testing Handbook is a guide for planning operations at Wallops testing facilities. It provides a summary of the capabilities and technical specifications of available facilities. This handbook prescribes the information to be provided by the user that will enable the integration and testing team to effectively plan for and support the facility user’s project. Note that each facility plans for availability based on current workloads/ mission schedules. For example, sounding rockets may have between 20 and 35 missions in work at one time. Also note that special training, such as cleanroom certification, electrostatic discharge (ESD) or confined space training may be required for entrance to some facilities.

Adam Hammoudi↗

DOE OSTI2012

Integrated Data Analysis (IDCA) Program - PETN Class 4 Standard

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of PETN Class 4. The PETN was found to have: 1) an impact sensitivity (DH 50 ) range of 6 to 12 cm, 2) a BAM friction sensitivity (F 50 ) range 7 to 11 kg, TIL (0/10) of 3.7 to 7.2 kg, 3) a ABL friction sensitivity threshold of 5 or less psig at 8 fps, 4) an ABL ESD sensitivity threshold of 0.031 to 0.326 j/g, and 5) a thermal sensitivity of an endothermic feature with T min = ~ 141 °C, and a exothermic feature with a T max = ~205°C.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2015

Workmanship Training Industry

Special processes require special skills, knowledge and experienced application. For over 15 years, the NASA Johnson Space Center's Receiving, Inspection and Test Facility (RITF) has provided Workmanship Standards compliance training, issuing more than 500 to 800 training completion certificates annually. It is critical that technicians and inspectors are trained and that they maintain their proficiency to implement the applicable standards and specifications. Training services include 'hands-on' training to engineers, technicians, and inspectors in the areas of electrostatic discharge (ESD), soldering, fiber optics, lithium battery handling, torque and wire safety, and wire wrapping.

Patterson, Ashley↗

NASA NTRS2023

Space Environmental Effects on Additively Manufactured Materials – Results from MISSE-9 and MISSE-10

The NASA Marshall Space Flight Center (MSFC) Space Environmental Effects (SEE) and Contamination Control (CC) teams prepared and characterized MISSE-9 and MISSE-10’s additively manufactured (AM) materials samples to investigate the effect of ultraviolet (UV) radiation, thermal cycling, outgassing, and temperature and provide data on the durability of these samples. Materials studied were polyetherimide (Ultem 1010 and 9085), electrostatic dissipative polyetherketoneketone (ESD-PEKK), also known commercially as Antero 840CN03, polycarbonate biocompatible per ISO 10993 USP Class VI (PC-ISO), and Inconel 718. Some samples were manufactured at MSFC, while 3D printer manufacturers Stratasys and Made In Space, Inc. (MIS) (now Redwire) participated in this effort to compare different vendors and printing setups. Results from nondestructive analyses and tensile testing are presented.

additive manufacturing↗

NASA NTRS2015

Johnson Space Center: Workmanship Training

Special processes require special skills, knowledge and experienced application. For over 15 years, the NASA Johnson Space Center's Receiving, Inspection and Test Facility (RITF) has provided Agency-wide NASA Workmanship Standards compliance training, issuing more than 500 to 800 training completion certificates annually. It is critical that technicians and inspectors are trained and that they maintain their proficiency to implement the applicable standards and specifications. Training services include "hands-on" training to engineers, technicians, and inspectors in the areas of electrostatic discharge (ESD), soldering, surface mount technology (SMT), crimping, conformal coating, and fiber-optic terminations.

Patterson, Ashley↗

DOE OSTI2013

Integrated Data Collection Analysis (IDCA) Program — Ammonium Nitrate

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of ammonium nitrate (AN). AN was tested, in most cases, as both received from manufacturer and dried/sieved. The participants found the AN to be: 1) insensitive in Type 12A impact testing (although with a wide range of values), 2) completely insensitive in BAM friction testing, 3) less sensitive than the RDX standard in ABL friction testing, 4) less sensitive than RDX in ABL ESD testing, and 5) less sensitive than RDX and PETN in DSC thermal analyses.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2016

Electrostatic Discharge Testing of Carbon Composite Solar Array Panels for NASA's Planned Europa Mission to Jupiter

The next planned NASA mission to visit Jupiter is known as the Europa Mission. The objective of this mission concept is to enter orbit around Jupiter in order to conduct multiple close flybys of the icy moon Europa. After careful trade studies, the mission designers have selected solar arrays as the baseline power system for the proposed mission rather than more traditional radioisotope thermoelectric generators. In order to examine the risk of using solar arrays, a series of tests were devised to determine the response of a typical solar array coupon to energetic electrons. Test coupons were fabricated and exposed to electrons ranging from 10 keV to 100 keV, at 1 nA/cm2, while being held at both room and cryogenic temperatures and exposed to end of mission radiation levels. While under electron bombardment, electrical discharges were observed and recorded with the majority of discharges occurring with electron energies of 25 keV. The largest effects on discharge size and rate were the decrease in temperature and the reduction of dielectric material on the sample surface. These tests indicate that solar array panels could be used by the planned Europa Mission in the Jovian environment, but that electrostatic discharges could be expected on the carbon composite solar arrays.

carbon composite↗

DOE OSTI2013

Integrated Data Collection Analysis (IDCA) Program — RDX Standard Data Sets

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of the RDX Type II Class 5 standard, for a third and fourth time in the Proficiency Test and averaged with the analysis results from the first and second time. The results, from averaging all four sets (1, 2, 3 and 4) of data suggest a material to have slightly more impact sensitivity, more BAM friction sensitivity, less ABL friction sensitivity, similar ESD sensitivity, and same DSC sensitivity, compared to the results from Set 1, which was used previously as the values for the RDX standard in IDCA Analysis Reports.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2000

Asbestos Free Insulation Development for the Space Shuttle Solid Propellant Rocket Motor (RSRM)

Asbestos has been used for many years as an ablation inhibitor in insulating materials. It has been a constituent of the AS/NBR insulation used to protect the steel case of the RSRM (Reusable Solid Rocket Motor) since its inception. This paper discusses the development of a potential replacement RSRM insulation design, several of the numerous design issues that were worked and processing problems that were resolved. The earlier design demonstration on FSM-5 (Flight Support Motor) of the selected 7% and 11% Kevlar(registered) filled EPDM (KF/EPDM) candidate materials was expanded. Full-scale process simulation articles were built and FSM-8 was manufactured using multiple Asbestos Free (AF) components and materials. Two major problems had to be overcome in developing the AF design. First, bondline corrosion, which occurred in the double-cured region of the aft dome, had to be eliminated. Second, KF/EPDM creates high levels of electrostatic energy (ESE), which does not readily dissipate from the insulation surface. An uncontrolled electrostatic discharge (ESD) of this surface energy during many phases of production could create serious safety hazards. Numerous processing changes were implemented and a conductive paint was developed to prevent exposed external insulation surfaces from generating ESE/ESD. Additionally, special internal instrumentation was incorporated into FSM-8 to record real-time internal motor environment data. These data included inhibitor insulation erosion rates and internal thermal environments. The FSM-8 static test was successfully conducted in February 2000 and much valuable data were obtained to characterize the AF insulation design.

Allred, Larry D.↗

NASA NTRS2009

Effect of Electrostatic Discharge on Electrical Characteristics of Discrete Electronic Components

This article reports on preliminary results of a study conducted to examine how temporary electrical overstress seed fault conditions in discrete power electronic components that cannot be detected with reliability tests but impact longevity of the device. These defects do not result in formal parametric failures per datasheet specifications, but result in substantial change in the electrical characteristics when compared with pristine device parameters. Tests were carried out on commercially available 600V IGBT devices using transmission line pulse (TLP) and system level ESD stress. It was hypothesized that the ESD causes local damage during the ESD discharge which may greatly accelerate degradation mechanisms and thus reduce the life of the components. This hypothesis was explored in simulation studies where different types of damage were imposed to different parts of the device. Experimental results agree qualitatively with the simulation for a number of tests which will motivate more in-depth modeling of the damage.

Wysocki, Phil↗

DOE OSTI2013

Integrated Data Collection Analysis (IDCA) Program - NaClO 3 /Icing Sugar

The Integrated Data Collection Analysis (IDCA) program is conducting a proficiency study for Small- Scale Safety and Thermal (SSST) testing of homemade explosives (HMEs). Described here are the results for impact, friction, electrostatic discharge, and differential scanning calorimetry analysis of a mixture of NaClO 3 and icing sugar—NaClO 3 /icing sugar mixture. The mixture was found to: be more sensitive than RDX but less sensitive than PETN in impact testing (180-grit sandpaper); be more sensitive than RDX and about the same sensitivity as PETN in BAM fiction testing; be less sensitive than RDX and PETN except for one participant found the mixture more sensitive than PETN in ABL ESD testing; and to have one to three exothermic features with the lowest temperature event occurring at ~ 160°C always observed in thermal testing. Variations in testing parameters also affected the sensitivity.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2008

ESD Challenges for NASA Astronauts in Upcoming Missions

Electrostatic charging of insulators is well known to pose potential threats to electronic systems under terrestrial systems. We were asked to evaluate potential hazards associated with replacement of an electronics board in the vacuum of space during the upcoming Hubble Service Repair mission in September 2008. A device called a "tribot" was built to simulate triboelectric charging of several insulators that are capable of contact charging against astronaut's gloves and suit materials. Materials were evaluated as the extent of not only the magnitude of electric fields generated by the frictional action, but also any resulting discharge which would be a source of EMI. Experimental results are quite surprising and unexpected when compared with tests performed under ambient conditions under dry and humid air.

Buhler, Charles R.↗

NASA NTRS1986

Characteristics of electromagnetic interference generated by arc discharges

Electromagnetic interference (EMI) signatures resulting from arc discharges are characterized, and the effects of electrostatic discharges (ESDs) on the design of spacecraft systems are investigated. EMI characterization experiments were performed on Mylar, Teflon, Kapton, fused silica, and fiberglass in a vacuum chamber with acrylic walls; the experimental design and procedures are described. Discharge current pulses and RF spectra generated by the sample materials are examined. The relation between the magnitude of EMI generated during an ESD event and the material, environment, and geometry is studied. The solar-array/plasma interaction is analyzed; particular attention is given to the rate of discharge as a function of plasma density. The physical mechanisms of ESD-generated EMI are discussed. The data reveal that ESD parameters are dependent on the test environment.

Leung, Philip↗

DOE OSTI2020

LANL studies of ESD spark energy discharge through September 2019

Two concentric-sphere apparatuses were used to measure the energies deposited by electric sparks through air to calibrated loads. Both sets of spheres had clean, uninsulated metal surfaces. The 127-mm diameter pair of spheres had a gap of 10 mm and a capacitance of 52 pF. The maximum energy stored on these spheres was 12 mJ and the maximum energy delivered to the 50-mΩ load was 11 µJ, with or without inductance. This load energy amounted to 0.09% of the available input energy; the remainder of the input energy was expended in forming the spark. The second set of spheres was 330 mm in diameter with a gap of 14 mm and a capacitance of 240 pF. The maximum energy stored on these spheres was 71 mJ and the maximum energy delivered to the 50-mΩ load was 150 µJ without added inductance. This load energy was 0.27% of the input energy; again, the remainder of the input energy was expended in forming the spark. The inclusion of 250 nH and 500 nH inductances in the discharge path of the smaller spheres caused the current discharges to resonate, but had little effect on the maximum energies deposited in the loads. At the time of writing, inductances had not yet been added to the larger spheres. The magnitudes of the observed spark discharges were stochastic, so more than 1200 tests were required to develop the statistical bounds of the spark behavior, i.e., to estimate the worst case (highest likely) energy depositions in the loads. The action integrals of the current discharges $∫ i^2dt$ were found to be approximately independent of the load resistances for loads of less than ~1 Ω. Hence the energy deposition scaled with resistance as 207 µJ/Ω and 2.93 mJ/Ω for the two apparatuses.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗

DOE OSTI2012

An Analysis of Electrostatic Discharge Considerations in the Use of Sodium Bicarbonate Media for De-Potting Sensitive Electronic Assemblies

Sodium bicarbonate blast media offers superior performance in removing low-to-medium density polyurethane foam potting materials from electronic assemblies compared to conventional abrasive or other low-hardness blast media. This work identifies a class of processing equipment suitable for potting removal in electronic assemblies and provides a technical evaluation of appropriate process controls that significantly reduce the potential for Electrostatic Discharge (ESD) degradation or damage. Once appropriate process controls are added, the class of blast equipment demonstrated here, previously used only for non-ESD sensitive assemblies, can be safely used to provide new capabilities for component-level support. In many cases, assemblies that have been de-potted using sodium bicarbonate can be disassembled and rebuilt using normal production processes, enabling repair, reacceptance, and surveillance of assemblies that was previously impractical. This paper presents the results of a study that identifies significant process variables and their contribution to ESD generation. Data are presented to quantify process-related peak ESD voltages and mitigation methods. A discussion of how to implement practical ESD controls and de-potting process test methodologies is provided. The intent of this work is to document foundational experimental work that provides a technical basis for sodium bicarbonate as an ESD-safe material for use in de-potting processes when appropriate controls are implemented.

Kinzel, Robert L.↗