Development of a prototype LH2 capacitance type mass flowmeter and readout Summary report
Capacitive mass flow meter with electronic readout for use with liquid hydrogen
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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Observation of the J = 2 to J = 1 transition of interstellar CO at 1.3 millimeters
The NRAO 36-foot antenna at Kitt Peak with a novel type of millimeter-wave superheterodyne receiver was used in observations of 1.3-mm line interstellar radiation due to J ? 2-1 transitions of C(12)0(16) and C(13)0(16). The liquid-helium-cooled hot-electron bolometer mixer of the superheterodyne receiver was used as the detecting element. The Orion Nebula CO system was found to be thermalized, showing a peak excitation temperature of about 76 K.
Phillips, T. G.↗
Thermoelectrically-cooled variable-temperature probe
Variable-temperature probe for electron spectroscopy requires no cryogenic liquids or resistance heating elements. Device consists of heat sink, probe tip, and nickel-plated copper body which resists oxidation and transfers heat efficiently between tip and heat sink.
Kelso, R. M.↗
Ordered pairing in liquid metallic hydrogen
We study two possible types of pairing involving the protons of a proposed low-temperature liquid phase metallic hydrogen. Electron-proton pairing, which can result in an insulating phase, is investigated by using an approximate solution of an Eliashberg-type equation for the anomalous self-energy. A very low estimate of the transition temperature is obtained by including proton correlations in the effective interaction. For proton-proton pairing, we derive a new proton pair potential based on the Abrikosov wave function. This potential includes the electron-proton interaction to all orders and has a much larger well depth than is obtained with linear screening methods. This suggests the possibility of either a superfluid paired phase analogous to that in He-3, or alternatively a phase with true molecular pairing.
Carlsson, A. E.↗
Characterization of production GaAs solar cells for space
The electrical performance of GaAs solar cells was characterized as a function of irradiation with protons and electrons with the underlying goal of producing solar cells suitable for use in space. Proton energies used varied between 50 keV and 10 MeV, and damage coefficients were derived for liquid phase epitaxy GaAs solar cells. Electron energies varied between 0.7 and 2.4 MeV. Cells from recent production runs were characterized as a function of electron and proton irradiation. These same cells were also characterized as a function of solar intensity and operating temperature, both before and after the electron irradiations. The long term stability of GaAs cells during photon exposure was examined. Some cells were found to degrade with photon exposure and some did not. Calibration standards were made for GaAs/Ge solar cells by flight on a high altitude balloon.
Anspaugh, B. E.↗
N/P InP homojunction solar cells with an In0.53Ga0.47As contacting layer grown by liquid phase epitaxy
N/P InP homojunction solar cells with an In sub 0.53 Ga sub 0.47 As contacting layer were fabricated by liquid phase epitaxy (LPE). Electron-Beam-Induced-Current (EBIC) measurements were performed on several selected samples. It was found that the background doping level in the base region sometimes results in a deep junction, which greatly affects the cell performance.
Shen, C. C.↗
First Experimental Demonstration of Full-Duplex Optical Communication on a Single Beam
The satellite industry is driven by the need to reduce costs. One way they have sought to do this is by reducing the size and weight of the satellite because of the extremely high cost per kilogram incurred launching a payload into orbit. The main difficulty in this approach is the lack of power capacity in a small satellite. One of the largest loads on a satellite's power system is the communications system. This has driven the need for a low-power communications system. This document examines a novel method of communicating optically with a low-Earth-orbit satellite from the ground without the need for a laser on the payload. The goal is to show the feasibility of such a system as a solution to the small satellite low-powered communication problem. Specially, that the system described herein: is capable of ground to low-Earth-orbit communications, has very little space-borne mass, and draws little power from the satellite. First, the system (hereafter referred to as LOWCAL "Lightweight Optical Wavelength Communication without A Laser in space") will be explained with details of the formats used and the link budgets. Discussions will be presented on the development of some of the system hardware (the laser diode driver, liquid crystal driver, and decision electronics for both the up and down links.) Finally, experimental test results of the entire system operating in a laboratory environment are presented and compared to theory. The results of the laboratory experiment support the original thesis: retro-modulated optical communications can meet the needs of the small satellite community. The system is capable of 10-kbps communication, has low space-borne mass, and draws little power from the satellite (less than 100-mW measured for the laboratory experiment, less than 1.5-W calculated for the Shuttle experiment).
Garrett, Christopher David↗
MEMS based pumped liquid cooling systems for micro/nano spacecraft thermal control
The electronic and other payload power densities in future micro/nano spacecraft are expected to exceed 25 Watts/cm(sup 2) and require advanced thermal control concepts and technologies to keep their payload within allowable temperature limits. This paper presents background on the need for pumped liquid cooling systems for future micro/nano spacecraft and results from this ongoing experimental investigation.
cooling system thermal control microspacecraft↗
Thermophysical properties of simple liquid metals: A brief review of theory
In this paper, we review the current theory of the thermophysical properties of simple liquid metals. The emphasis is on thermodynamic properties, but we also briefly discuss the nonequilibrium properties of liquid metals. We begin by defining a 'simple liquid metal' as one in which the valence electrons interact only weakly with the ionic cores, so that the interaction can be treated by perturbation theory. We then write down the equilibrium Hamiltonian of a liquid metal as a sum of five terms: the bare ion-ion interaction, the electron-electron interaction, the bare electron-ion interaction, and the kinetic energies of electrons and ions. Since the electron-ion interaction can be treated by perturbation, the electronic part contributes in two ways to the Helmholtz free energy: it gives a density-dependent term which is independent of the arrangement of ions, and it acts to screen the ion-ion interaction, giving rise to effective ion-ion pair potentials which are density-dependent, in general. After sketching the form of a typical pair potential, we briefly enumerate some methods for calculating the ionic distribution function and hence the Helmholtz free energy of the liquid: monte Carlo simulations, molecular dynamics simulations, and thermodynamic perturbation theory. The final result is a general expression for the Helmholtz free energy of the liquid metal. It can be used to calculate a wide range of thermodynamic properties of simple metal liquids, which we enumerate. They include not only a range of thermodynamic coefficients of both metals and alloys, but also many aspects of the phase diagram, including freezing curves of pure elements and phase diagrams of liquid alloys (including liquidus and solidus curves). We briefly mention some key discoveries resulting from previous applications of this method, and point out that the same methods work for other materials not normally considered to be liquid metals (such as colloidal suspensions, in which the suspended microspheres behave like ions screened by the salt solution in which they are suspended). We conclude with a brief discussion of some non-equilibrium (i.e., transport) properties which can be treated by an extension of these methods. These include electrical resistivity, thermal conductivity, viscosity, atomic self-diffusion coefficients, concentration diffusion coefficients in alloys, surface tension and thermal emissivity. Finally, we briefly mention two methods by which the theory might be extended to non-simple liquid metals: these are empirical techniques (i.e., empirical two- and three-body potentials), and numerical many-body approaches. Both may be potentially applicable to extremely complex systems, such as nonstoichiometric liquid semiconductor alloys.
Stroud, David↗
Melting of iron by significant structure theory
From Eyring's method of significant structures, a partition function is derived for liquid iron. The solid at high temperature is described in the Einstein approximation. Magnetic and electronic contributions to the thermodynamic properties of both the liquid and solid phases are considered. The model is compatible with properties (thermal expansion, compressibility, heat capacity, entropy of melting, and volume change on melting) at one atm. The melting temperature at high pressure is found by satisfying the requirement that the Gibbs free energies of the liquid and solid phases are equal at the melting temperature. Under conditions at the earth's core-mantle boundary, the melting temperature of iron is greater than approximately 5000 K, and under inner-outer core conditions the melting temperature is greater than approximately 7000 K. These estimates are consistent with the Lindemann melting law, but not with the Kraut-Kennedy melting law.
Leppaluoto, D. A.↗
Combustion Synthesis of Fullerenes and Fullerenic Nanostructures In Microgravity
The objectives of the proposed research were to determine the effects of gravity on fullerenes formation in flames and, based on the observed effects, to develop fundamental understanding of fullerenes formation and to identify engineering principles for fullerenes production. The research method consisted of the operation of laminar diffusion flames under normal- and reduced-gravity conditions, and the collection from the flames and subsequent analysis of condensables including any fullerenes present, using coupled high performance liquid chromatography/mass spectrometry and high resolution transmission electron microscopy. The focus included fullerene molecules C60 and C70 and fullerenic nanostructures including tubes, spherules and other shapes. The normal-gravity experiments were performed at MIT and complementary reduced-gravity experiments were to have been contributed by NASA. The independent variables of interest are gravity, fuel type, fuel/oxygen ratio, pressure, gas velocity at burner, diluent type and concentration. Given the large number of variables and the absence of data on either fullerene formation in diffusion flames or gravitational effects on fullerene formation in diffusion or premixed flames, the first part of the work was exploratory while the later part involved detailed study of the most interesting mechanisms. Samples of condensable material from laminar low pressure benzene/argon/oxygen diffusion flames were collected and analyzed by high-performance liquid chromatography to determine the yields of fullerenes, and by high-resolution transmission electron microscopy (HRTEM) to characterize the fullerenic material, i.e., curved-layer nanostructures, on and within the soot particles. The highest concentration of fullerenes was always detected just above the visible stoichiometric surface of a flame. The percentage of fullerenes in the condensable material increases with decreasing pressure. The overall highest amount of fullerenes was found for a surprisingly high dilution fuel with argon. The maximum flame temperature seems to be of minor importance in fullerene formation. The HRTEM analysis of the soot showed an increase of the curvature of the carbon layers, and hence increased fullerenic character. After this maximum, the curvature decreases. In addition to the soot, the samples included fullerenic nanostructures, such as tubes and spheroids including highly-ordered multilayered or onion-like structures. The soot itself shows highly ordered regions that appear to have been cells of ongoing fullerenic nanostructure formation.
Howard, Jack B.↗
Some topics in electrocatalysis
Liquid metal alloys surface composition and electronic structure roles in electrocatalysis evaluated by studying hydrogen-ion discharge reaction and electrical double layer
Butler, J. N.↗
Electron paramagnetic resonance study of alinement induced by magnetic fields in two smectic-A liquid crystals not exhibiting nematic phases
Using vanadyl acetylacetonate (VAAC) as a paramagnetic probe, the molecular ordering in two smectic-A liquid crystals that do not display nematic phases were studied. Reproducible alinement was attained by slow cooling throughout the isotropic smectic-A transition in dc magnetic fields of 1.1 and 2.15 teslas. The degree of order attained is small for a smectic-A liquid crystal. Measurements were made of the variation of the average hyperfine splitting of the alined samples as a function of orientation relative to the dc magnetic field of the spectrometer. This functional dependence is in agreement with the theoretical prediction except where the viscosity of the liquid crystal becomes large enough to slow the tumbling of the VAAC, as indicated by asymmetry in the end lines of the spectrum.
Fryburg, G. C.↗
Thermal alteration of young kerogen in relation to petroleum genesis
Kerogen, humic acid, and lipid material were separated from a young marine sediment and heated in sealed tubes in a nitrogen atmosphere at 150 and 410 C. Gaseous and liquid products generated during heating, and also the residual organic material, were characterized by gas-liquid chromatography, elemental analysis, infrared and electron spin resonance spectroscopy, and X-ray diffraction.
Ishiwatari, R.↗
Solidification processing superalloys in an electric field
The phase morphology of a given superalloy's microstructure is established during solidification. Solidification-processing in an applied electric field is a technique currently undergoing experimental characterization at NASA-Marshall. The method is predicated on the simplest model of a metallic solid, in which ions are arranged in basic space lattices that are permeated by an 'electron gas' whose valence electrons are free to move in the solid. When in a superheated liquid state, the metal is seen as a dense 'cold plasma' of electrons and ions. The application of an electric field during solidification establishes a steady, continuous current flow; the direction of propagation of the plasma waves coincides with the direction of the electric field. Such an alignment introduces an ordered arrangement of the electric vectors and introduces an additional degree of order in an already highly ordered alloy.
Ahmed, Shaffiq↗
Analysis of a Memory Device Failure
The recent failure of a vintage memory device presented a unique challenge to failure analysts. Normally device layouts, fabrication parameters and other technical information were available to assist the analyst in the analysis. However, this device was out of production for many years and the manufacturer was no longer in business, so the information was not available. To further complicate this analysis, the package leads were all but removed making additional electrical testing difficult. Under these conditions, new and innovative methods were used to analyze the failure. The external visual exam, radiography, PIND, and leak testing were performed with nominal results. Since electrical testing was precluded by the short lead lengths, the device was delidded to expose the internal structures for microscopic examination. No failure mechanism was identified. The available electrical data suggested an ESD or low level EOS type mechanism which left no visible surface damage. Due to parallel electrical paths, electrical probing on the chip failed to locate the failure site. Two non-destructive Scanning Electron Microscopy techniques, CIVA (Charge Induced Voltage Alteration) and EBIC (Electron Beam Induced Current), and a liquid crystal decoration technique which detects localized heating were employed to aid in the analysis. CIVA and EBIC isolated two faults in the input circuitry, and the liquid crystal technique further localized two hot spots in regions on two input gates. Removal of the glassivation and metallization revealed multiple failure sites located in the gate oxide of two input transistors suggesting machine (testing) induced damage.
Nicolas, David P.↗
Metal/Silicate Partitioning at High Pressures and Temperatures
The behavior of siderophile elements during metal-silicate segregation, and their resulting distributions provide insight into core formation processes. Determination of partition coefficients allows the calculation of element distributions that can be compared to established values of element abundances in the silicate (mantle) and metallic (core) portions of the Earth. Moderately siderophile elements, including W, are particularly useful in constraining core formation conditions because they are sensitive to variations in T, P, oxygen fugacity (fO2), and silicate composition. To constrain the effect of pressure on W metal/silicate partitioning, we performed experiments at high pressures and temperatures using a multi anvil press (MAP) at NASA Johnson Space Center and laser-heated diamond anvil cells (LHDAC) at the University of Maryland. Starting materials consisted of natural peridotite mixed with Fe and W metals. Pressure conditions in the MAP experiments ranged from 10 to 16 GPa at 2400 K. Pressures in the LHDAC experiments ranged from 26 to 58 GPa, and peak temperatures ranged up to 5000 K. LHDAC experimental run products were sectioned by focused ion beam (FIB) at NASA JSC. Run products were analyzed by electron microprobe using wavelength dispersive spectroscopy. Liquid metal/liquid silicate partition coefficients for W were calculated from element abundances determined by microprobe analyses, and corrected to a common fO2 condition of IW-2 assuming +4 valence for W. Within analytical uncertainties, W partitioning shows a flat trend with increasing pressure from 10 to 16 GPa. At higher pressures, W becomes more siderophile, with an increase in partition coefficient of approximately 0.5 log units.
Shofner, G.↗
(abstract) Mars Pathfinder Active Thermal Control System: Ground and Flight Performance of a Mechanically Pumped Cooling Loop
A key element of the Mars Pathfinder thermal control system is the Heat Rejection System (HRS). The HRS of Mars Pathfinder is designed to actively control the temperatures of the various parts of the spacecraft.This is achieved by mechanically circulating single-phase Freon 11 liquid through the lander and cruise electronics box heat exchangers and transferring the heat to an external radiator on the cruise stage. This is the first time in spacecraft history that a mechanically pumped cooling loop has been used on a long duration spacecraft mission. Many lessons have been learned during the testing and ground and flight operation of the HRS. This paper will present the performance of the mechanically pumped cooling loop during the ground and flight operations. Based on the lessons learned from this experience, recommendations on the design and operation of the pumped cooling loops for future space missions will be made.
Mars↗