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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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82 records · Page 5

Adapting Apollo-Era Instrumentation for Cold Sample Processing While Maintaining Curatorial Standard Practices

The goal of the Apollo Next Generation Sample Analysis (ANGSA) Program is to study “specially curated samples,” that is, unstudied Apollo samples that have been preserved under unique conditions. A subset of the funded ANGSA work includes the study of Apollo samples stored under cold conditions since their return from the Moon. Ongoing ANGSA processing and future returned samples require cold curation strategies to preserve the integrity of organic and other temperature-sensitive constituents within those samples. Standard Apollo curation processing hardware and procedures are designed for room temperature operations, not cold conditions. This abstract details the major modifications of a heritage lunar cabinet in preparation for the first cold curation processing at Johnson Space Center. Future publications will provide greater detail on the low temperature materials and operation procedures. This work not only supports Apollo but also future cold sample return missions.

Amick, Cecilia L.↗

In-Situ Detection of Process-Induced Porosity During Cure of Out-of-Autoclave Composites

Composite materials offer unique benefits in aerospace applications and are becoming increasingly used by industry manufacturers. Current manufacturing and processing methods can lead to defects in the composites, which are identified after fabrication using inspection methods.This study utilized a high-temperature ultrasonic inspection system to detect process-induced porosity in an out-of-autoclave (OOA) composite panel. An ultrasonic scanner was enclosed in a nitrogen-cooled insulating box that prevented thermal damage from the industrial oven to the temperature-sensitive electronics. Inspection of the composite part was performed through the bottom of the enclosure, which served as the tool plate for the part. In this study, a porosity gradient was introduced through a misfit of the part and caul plate. Using the data obtained from B-scans and amplitude C-scans throughout the cure cycle, the high and low porosity regions within the composite laminate were detected and localized. OOA tests aided the transition of this system to an autoclave, which is the primary method of curing aerospace-grade thermoset composites.

In-process, Defect Detection, Cure Monitoring, Por↗

Thermal design of the sample handling assembly in the sampling and caching subsystem on the Mars 2020 rover

The Mars 2020 Rover is scheduled to land on Mars on February 18, 2021. One of the primary mission objectives for the Mars 2020 Rover is to collect a set of Martian regolith samples for potential future return to Earth. Regolith and rock samples will be collected and placed into sample tubes using a coring drill, located at the end of a large Robotic Arm, on the outside of the rover. Filled sample tubes will be transferred from the outside of the Rover into the Adaptive Caching Assembly (ACA), located inside the Rover chassis, via the Bit Carousel. Once the filled sample tube is brought into the ACA, the Sample Handling Assembly (SHA) will transfer it to all of the internal processing stations of the ACA for volume assessment, sealing and finally drop-off on the Martian surface. The ACA is a volume within the rover chassis that is not temperature-controlled. Actuators inside the SHA and its End Effector (EE) must be warmed to above -55°C and -25°C, respectively, prior to use. This paper discusses the thermal design of the SHA that uses heaters and temperature sensors to warm up and maintain the temperature-sensitive arm components within temperature limits during operation. Thermal performance predictions for Mars surface operations are also presented.

Lee, Chern-Jiin↗

Cutting out the Middleman: Calibrating and Validating a Dynamic Vegetation Model (ED2-PROSPECT5) Using Remotely Sensed Surface Reflectance

Canopy radiative transfer is the primary mechanism by which models relate vegetation composition and state to the surface energy balance, which is important to light- and temperature-sensitive plant processes as well as understanding land–atmosphere feedbacks. In addition, certain parameters (e.g., specific leaf area, SLA) that have an outsized influence on vegetation model behavior can be constrained by observations of shortwave reflectance, thus reducing model predictive uncertainty. Importantly, calibrating against radiative transfer outputs allows models to directly use remote sensing reflectance products without relying on highly derived products (such as MODIS leaf area index) whose assumptions may be incompatible with the target vegetation model and whose uncertainties are usually not well quantified. Here, we created the EDR model by coupling the two-stream representation of canopy radiative transfer in the Ecosystem Demography model version 2 (ED2) with a leaf radiative transfer model (PROSPECT-5) and a simple soil reflectance model to predict full-range, high-spectral-resolution surface reflectance that is dependent on the underlying ED2 model state. We then calibrated this model against estimates of hemispherical reflectance (corrected for directional effects) from the NASA Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) and survey data from 54 temperate forest plots in the northeastern United States. The calibration significantly reduced uncertainty in model parameters related to leaf biochemistry and morphology and canopy structure for five plant functional types. Using a single common set of parameters across all sites, the calibrated model was able to accurately reproduce surface reflectance for sites with highly varied forest composition and structure. However, the calibrated model's predictions of leaf area index (LAI) were less robust, capturing only 46 % of the variability in the observations. Comparing the ED2 radiative transfer model with another two-stream soil–leaf–canopy radiative transfer model commonly used in remote sensing studies (PRO4SAIL) illustrated structural errors in the ED2 representation of direct radiation backscatter that resulted in systematic underestimation of reflectance. In addition, we also highlight that, to directly compare with a two-stream radiative transfer model like EDR, we had to perform an additional processing step to convert the directional reflectance estimates of AVIRIS to hemispherical reflectance (also known as “albedo”). In future work, we recommend that vegetation models add the capability to predict directional reflectance, to allow them to more directly assimilate a wide range of airborne and satellite reflectance products. We ultimately conclude that despite these challenges, using dynamic vegetation models to predict surface reflectance is a promising avenue for model calibration and validation using remote sensing data.

Alexey N Shiklomanov↗

Mars Climate Sounder Observations of Gravity Wave Activity throughout Mars’s Lower Atmosphere

Gravity waves are one way Mars’s lower atmospheric weather can affect the circulation and even composition of Mars’s middle and upper atmosphere. A recent study showed how on-planet observations near the center of the 15 micron CO2band by the A3 channel(635–665 cm−1)of the Mars Climate Sounder on board Mars Reconnaissance Orbiter (MRO-MCS) could sense horizontally short, vertically broad gravity waves at≈25 km above the surface by looking at small-scale radiance variability in temperature-sensitive channels. This approach is extended here to two additional channels closer to the wings of the 15 micron CO2band,A1 (595–615 cm−1) and A2 (615–645 cm−1), to sense gravity waves throughout the lower atmosphere. Using information from all three channels demonstrates that gravity wave activity in Mars’s lowermost atmosphere is dominated by orographic sources, particularly over the extremely rough terrain of Valles Marineris. Much of this orographic population is either trapped or filtered in the lowest two scale heights, such that variations in filtering and non-orographic sources shape the gravity wave population observed at 25 km above the surface. During global dust storms, however, gravity wave activity in the first scale height decreases by approximately a factor of two, yet trapping/filtering of what activity remains in the tropics substantially weakens. Exceptionally high radiance variability at night in the tropics during the less dusty part of the year is the result of observing mesospheric clouds rather than gravity waves.

Nicholas G Heavens↗

Temperature Sensing to Above 1500 °C Using Y 2 SiO 5 :Er Phosphor Thermometry

A transition from metallic to ceramic turbine components that can operate at higher turbine engine temperatures will push component surface temperatures from below 1200 °C into a 1300 to 1500 °C temperature range that is much more challenging for phosphor thermometry measurements. To address this challenge, Y 2 SiO 5 :Er was selected for its high temperature sensing performance by both luminescence lifetime and luminescence intensity ratio (LIR) methods as well as its thermochemical compatibility with the current generation of rare earth silicate environmental barrier coatings (EBCs) that are required to protect SiC/SiC ceramic composite components. Lifetime measurements that monitor the Er3+ 4S3/2→4I15/2 emission decay at 542 nm exhibited a slow decrease in decay time with temperature up to 1300° C, above which the decay decreased steeply to provide good temperature sensitivity in the 1300 to 1500 °C range (Fig. 1). LIR images were obtained where each pixel represented the ratio I488/I561 (I488 and I561 are the detected 488 nm 4F7/2→4I15/2 and the 561 nm 4S3/2→4I15/2 emission band intensities, respectively). Good temperature sensitivity (Fig. 2) and signal-to-background ratios were observed to above 1500 °C. Contrary to conventional guidance on selecting phosphors for high temperature sensing, the detected emission band intensities and decay times exhibited remarkably slow decreases with temperature up into the 1300 to 1500 °C range despite high phonon energies (>900 cm-1) that allow the energy gap between the 4S3/2 emitting reservoir level and the 4F9/2 level below it to be bridged by as few as three phonons. The benefits of utilizing a thermographic phosphor at very high temperatures that exhibits strong nonradiative multiphonon relaxation even at room temperature is explained by a competition between spontaneous and stimulated multiphonon emission, and the more temperature-sensitive decay time above 1300 °C is explained by a transition from high to low effective phonon energies.

temperature measurement↗

Transition Modeling Based on the Dual N-factor Method for the CRM-NLF Wind Tunnel Configuration

The dual N-factor method is used to model the boundary-layer transition over the common research model with natural laminar flow (CRM-NLF) aircraft configuration. The flow conditions match selected test conditions from a wind tunnel experiment in the National Transonic Facility at the NASA Langley Research Center. The paper presents a systematic methodology for transition prediction in the presence of a dual shock system and extends the prior capability for iteratively coupled computational fluid dynamics (CFD) predictions to incorporate three-dimensional, transonic wings. The method employs stability computations based on the linear parabolized stability equations (PSE), along with a dual N-factor criterion. The iterative process begins with the fully turbulent Reynolds-averaged-Navier-Stokes (RANS) mean flow solution. For the first iteration, a mean flow solution is calculated with an imposed transition front that aligns with the shock front from the fully turbulent solution. Subsequently, stability computations are performed along a set of streamlines across the wing to calculate the amplification of planar Tollmien-Schlichting (TS) and stationary crossflow (CF) modes. The transition criterion based on the dual N-factor method is used to infer the updated transition front and the process is successively repeated until convergence of the solution. Within three iterations, the predicted fronts for angles of attack of 1.45, 1.98, 2.46 and 2.94 degrees and a mean-aerodynamic-chord Reynolds number equal to 15 million, approach visual convergence in most regions of the studied cases, and the resulting predictions are in good agreement with the transition fronts deduced from measurements of temperature-sensitive paint. Even though surface pressure measurements based on fully-turbulent flow agree well with the measured pressure coefficient distributions, strong viscous-inviscid interaction effects cause significant shifts in the shock locations based on the imposed transition front, underscoring the intrusive nature of static pressure measurements using surface mounted ports on the CRM-NLF configuration.

Boundary Layer Transition↗

A Sub-THz CMOS Molecular Clock with 20 ppt Stability at 10,000 s Based on A Dual-Loop Spectroscopic Detection and Digital Frequency Error Integration

This paper presents a dual-loop chip-scale molecular clock (CSMC), which enhances the Allan Deviation performance by combining high signal-to-noise ratio of using fundamental mode and long-term stability of using higher order modes in derivative molecular absorption spectroscopy. In addition, digital frequency-error integration is adopted in the frequency-locked loop to provide an infinite open-loop DC gain, which fully suppresses any frequency drift caused by the temperature-sensitive crystal oscillator. This new generation CSMC is implemented in 65-nm CMOS, and achieves 20 ppt (part-per-trillion) Allan Deviation at 10,000 s averaging time with 71-mW power consumption.

Han, Ruonan↗

Sun-as-a-Star Spectral Line Variability in the 300–2390 nm Wavelength Range

Combining the near-daily Ozone Monitoring Instrument (OMI) and Tropospheric Monitoring Instrument (TROPOMI) measurements of solar spectra, we construct line indices (line-core to line-flanks ratios) for various transitions (mainly Fe I) in the 300–2390 nm spectral domain. The indices are supplemented by the wavelength-binned fluxes from OMI and Total and Spectral Solar Irradiance Sensor (TSIS-1). To study the short-term (solar-rotational) patterns, we normalize the indices and fluxes to the minimum-activity epoch, then de-trend them with 81 day running means. Comparisons of the de-trended TSIS-1 and OMI fluxes with the NASA-NOAA-LASP SSI (NNLSSI1) model show excellent agreement, to (0.5–2.2) × 10 -4 in the normalized and de-trended data. The data are subjected to a multiregression analysis against quantities representing the facular brightening and the sunspot darkening. The de-trended line indices and average fluxes show different sensitivities to these two solar magnetic-activity manifestations, with the fluxes being far more susceptible to the sunspot component. The de-trended line indices experience a rapid drop of activity levels towards longer wavelengths, albeit with a large rebound in the short-wave infrared (SWIR) domain that is caused by the ubiquitous, temperature-sensitive CO transitions. The wavelength-dependent activity also falls, however much slower, in the de-trended average fluxes. Qualitatively similar behavior is captured by semiempirical models.

Solar spectral Irradiance↗

Adaptive Curation at NASA Johnson Space Center: Preparing for Artemis Samples by Leveraging Proven Practices and Innovative Solution

The proper curation of returned astromaterial samples is essential to ensure that high-quality scientific investigations can be conducted for decades, enabling future generations to address evolving research questions. The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (hereafter JSC Curation) is responsible for curating all of NASA’s extraterrestrial samples. Under the governing document, NASA Procedural Requirement (NPR) 7100.5 “Curation of Extraterrestrial Materials”, JSC Curation is charged with “The curation of all extraterrestrial material under NASA control, including future NASA missions.” The Directive goes on to define Curation as including “...documentation, preservation, preparation, and distribution of samples for research, education, and public outreach.” JSC Curation has a long-standing legacy of curating extraterrestrial materials, including but not limited to Apollo and Luna lunar samples, Genesis solar wind samples, Stardust comet samples, asteroid samples (Hayabusa1, Hayabusa2, and OSIRIS-REx), and Antarctic Meteorite samples from a variety of parent bodies. Building on this foundation, the Artemis program introduces new challenges and opportunities for sample curation, requiring both the application of proven practices and the development of innovative solutions. The Artemis Collection will be curated using established protocols refined through decades of experience with Apollo and subsequent sample collections, including but not limited to the utilization of cleanrooms, custom nitrogen gloveboxes, specialized storage containers and tools; all of which have strict material utilization and prohibition requirements. These practices provide a robust framework for contamination control, documentation, and long-term preservation. However, Artemis samples may present unique scientific and operational requirements, including enhanced contamination control measures (relative to Apollo) driven by evolving science objectives. To meet these needs, JSC Curation is actively developing new technologies and protocols that extend beyond traditional approaches, ensuring that the integrity of samples is maintained under increasingly stringent standards. One critical area of innovation is the development of cold sample curation capabilities. Certain Artemis samples, particularly those from Permanently Shadowed Regions (PSRs) and cold environments, are expected to contain ices and volatile components that require preservation and handling at sub-zero or even cryogenic temperatures. JSC Curation is leveraging best practices from the cold and cryogenic sample industries, as well as other government agencies and academic experts, to design facilities and handling procedures that maintain sample integrity while enabling scientific access. The goal is to develop capabilities to allow researchers to investigate volatiles and other temperature-sensitive materials while minimizing chemical and physical alterations from their returned state. In summary, adaptive curation at JSC combines the reliability of proven methodologies with forward-looking innovations to meet the scientific and operational demands of Artemis. Through enhanced contamination control, advanced cold curation capabilities, and an understanding of known and evolving future science priorities, NASA is preparing to maximize the scientific return from Artemis samples and preserve their value for generations of researchers.

Andrea D Harrington↗