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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 973 records · Page 54
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

First Measurements of Differential Cross Sections In Kinematic Imbalance Variables With The MicroBooNE Detector

Making high-precision measurements of neutrino oscillation parameters requires an unprecedented understanding of neutrino-nucleus scattering. In this presentation, we present the first muon neutrino charged current double-differential cross sections in kinematic imbalance variables. These variables characterize the imbalance in the plane transverse to an incoming neutrino. We use events with a single muon above 100 MeV/c, a single final state proton above 300 MeV/c, and no recorded final state pions. Thus, these variables act as a direct probe of nuclear effects such as final state interactions, Fermi motion, and multi-nucleon processes. We also present a complementary ongoing analysis using electron neutrinos. This channel is of the utmost importance for the extraction of neutrino oscillation parameters by making high-precision measurements. Our measurements allow us to constrain systematic uncertainties associated with neutrino oscillation results performed by near-future experiments of the Short Baseline Neutrino (SBN) program, as well as by future large-scale experiments like DUNE.

43 PARTICLE ACCELERATORS↗
DOE OSTI2022

Solution combustion synthesis of iron-based alumina nanocomposites for clean production of hydrogen from fossil fuels

Iron-based alumina nanocomposites are promising materials for microwave-assisted thermocatalytic dehydrogenation of fossil fuels, which has been proposed for the production of hydrogen with no CO2 emissions. Solution combustion synthesis (SCS) is an attractive technique for the fabrication of these materials because it has been used for synthesis of many nanoscale oxides. However, SCS can be carried out using different organic fuels and different heating equipment, and it is important to determine which fuel and heating mode generate materials with the best properties for dehydrogenation, such as maximized specific surface area. In the present work, the iron-based alumina nanocomposites were obtained by SCS using two different fuels (citric acid and glycine) and two different heating modes (a hotplate and a muffle furnace). The precursors/oxidizers were iron nitrate and aluminum nitrate. They were mixed with the fuel according to stoichiometry and dissolved in water. Heating the solution resulted in combustion synthesis. The products were characterized by X-ray diffraction analysis, Brunauer-Emmett-Teller surface area analysis, laser diffraction particle size analysis, scanning electron microscopy, and energy dispersive X-ray spectroscopy. The experiments have shown that the specific surface area of the iron-based alumina nanocomposites obtained by SCS can be dramatically increased by using citric acid instead of glycine, and additionally by using a muffle furnace instead of a hotplate.

Solution combustion synthesis, Nanoscale metal oxi↗
DOE OSTI2025

LDRD conclusion poster - Synthesizing Heterometallic Uranium Single Crystals to Understand the Influence of the Secondary Metals on Uranyl Axial Bond Strength

Understanding how transition metals influenced the chemistry of lanthanide and actinide (f-element) materials is critical for advancing separation technologies, materials design, and coordination chemistry. This project examined how incorporating first-row transition metals affected the structural and spectroscopic properties of f-element coordination polymers. In uranium(VI)-based systems synthesized with 2,6-pyridinedicarboxylic acid (PDC) ligands, single-crystal X-ray diffraction and Raman spectroscopy revealed that the presence of transition metals shortened the uranyl axial bond and induced a blue shift in its symmetric stretching vibration—evidence of increased bond strength. Electronic structure analysis, including Density of States (DOS) calculations using density functional theory (DFT), revealed altered orbital overlaps and highlighted the role of transition metal d-orbitals in modulating bonding. Raman modes were modeled using truncated structural fragments in collaboration with the University of Notre Dame, and although the predicted frequencies were lower than experimental values, they remained within expected ranges. In parallel, similar experiments with cerium (Ce) in the presence of cobalt (Co) and PDC demonstrated multi-step single-crystal-to-single-crystal transformations—behavior not observed in the uranium systems. Initial products included light yellow, orange, and polycrystalline materials. Single-crystal X-ray diffraction studies, conducted in collaboration with the Colorado School of Mines, identified the yellow phase as monometallic Ce(PDC)2(H2O)2·4H2O and the orange phase as heterometallic Ce2Co(PDC)4(H2O)6. After standing in solution for one week, both phases fully transformed into a dark yellow crystalline phase, [Ce3(PDC)5(H2O)8].6(H2O). Remarkably, this transformation was reversible—disturbing the equilibrium by removing some crystals caused reversion to the initial Ce(PDC)2(H2O)2·4H2O phase, highlighting dynamic behavior. All three structures were previously unreported. Solid-state UV-visible and Raman spectroscopy further distinguished these phases, revealing ligand-to-metal charge transfer involving Ce and characteristic d–d transitions from Co(II). The precise mechanism driving these transformations remained unclear; however, pH-dependent experiments confirmed that the transformation did not occur when the pH decreased. Overall, the project demonstrated that transition metals could be employed to tune bonding interactions, structural dimensionality, and optical properties in f-element materials, establishing new pathways for designing functional heterometallic systems. The work resulted in several novel structural discoveries and fostered productive collaborations with the University of Notre Dame and the Colorado School of Mines.

37 - INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL C↗
DOE OSTI2026

Irradiation Testing of Additively Manufactured Materials for LWR Applications: Alloy 718 and 316L Stainless Steel

The objective of this NSUF Project is to assess the changes in irradiated additively manufactured (AM) material properties as compared to non-irradiated material. Type 316L stainless steel and Alloy 718 samples were produced using Direct Metal Laser Melting (DMLM) fabrication. Materials produced from this fabrication method have several potential applications within the nuclear industry as reactor internal repair parts, fuel debris resistant filters, or fuel spacers within existing light water reactors (LWRs). AM materials have been shown to achieve equivalent mechanical behavior in simulated reactor environments as compared to wrought materials, but have significantly more flexibility when it comes to unique design features. The increased component design flexibility makes these AM materials an attractive choice for both current LWR applications as well as for small modular reactor (SMR) designs. Prior to use of these materials in reactor fleet operation, the industry as a whole must evaluate the effects of irradiation on their material properties. Standard 0.4 inch thick Compact Tension specimens and SSJ3 type tensile bars were neutron irradiated at the Advanced Test Reactor to ~1 dpa for the purpose of performing a variety of mechanical tests in a range of simulated environments applicable to LWRs. For the ductile austenitic Type 316L stainless steel, the irradiated data will be used to confirm that the AM process produces materials with properties that are equivalent to wrought materials under testing conditions applicable to LWR operation. Transmission electron microscopy analysis was also performed in order to understand microstructural and microchemical changes induced in each material in response to neutron irradiation. If possible, data collected from these AM 316L samples will be used to remove fluence limits from specifications of ASME code cases for this alloy, which will give vendors much more flexibility in building future components.

36 - MATERIALS SCIENCE↗
DOE OSTI2020

Aluminum Spent Fuel Performance in Dry Storage Task 4 Aluminum Oxide Sampling of ATR Dry Stored Fuel

Milestone report on sampling of long-term dry-stored ATR spent fuel elements. It describes tooling, sample acquisition methods and analysis of the aluminum oxide samples by scanning electron microscopy, thermogravimetric analysis, X-ray diffraction and transmission electron microscopy. The observations provide input to projections on controls necessary for maintaining the integrity of the fuel during extended interim storage.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2019

Deep-inelastic and quasielastic electron scattering from A = 3 nuclei

We perform a combined analysis of inclusive electron scattering data from $A=3$ nuclei in the deep-inelastic and quasielastic scattering regions, using Monte Carlo analysis methods and the nuclear weak binding approximation to establish the range over which the data can be described within the same theoretical framework. Comparison with quasielastic $^3$He cross sections from SLAC and Jefferson Lab suggests that most features of the $x \gtrsim 1$ data can be reasonably well described in the impulse approximation with finite-$Q^2$ nuclear smearing functions for momentum transfers $Q^2 \gtrsim 1$~GeV$^2$. For the DIS region, we analyze the recent $^3$He to deuterium cross section ratio from the Jefferson Lab E03-103 experiment to explore the possible isospin dependence of the nuclear effects. We discuss the implications of this for the MARATHON experiment, and outline how a Bayesian analysis of $^3$He, $^3$H and deuterium data can robustly determine the free neutron structure function.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
NASA NTRS2004

Soot Nanostructure: Using Fringe Analysis Software on High Resolution Transmission Electron Microscopy of Carbon Soot

Using high resolution transmission electron images of carbon nanotubes and carbon particles, we are able to use image analysis program to determine several carbon fringe properties, including length, separation, curvature and orientation. Results are shown in the form of histograms for each of those quantities. The combination of those measurements can give a better indication of the graphic structure within nanotubes and particles of carbon and can distinguish carbons based upon fringe properties. Carbon with longer, straighter and closer spaced fringes are considered graphite, while amorphous carbon contain shorter, less structured fringes.

King, James D.↗
NASA NTRS2011

Component-Level Electronic-Assembly Repair (CLEAR) Spacecraft Circuit Diagnostics by Analog and Complex Signature Analysis

The Component-Level Electronic-Assembly Repair (CLEAR) project at the NASA Glenn Research Center is aimed at developing technologies that will enable space-flight crews to perform in situ component-level repair of electronics on Moon and Mars outposts, where there is no existing infrastructure for logistics spares. These technologies must provide effective repair capabilities yet meet the payload and operational constraints of space facilities. Effective repair depends on a diagnostic capability that is versatile but easy to use by crew members that have limited training in electronics. CLEAR studied two techniques that involve extensive precharacterization of "known good" circuits to produce graphical signatures that provide an easy-to-use comparison method to quickly identify faulty components. Analog Signature Analysis (ASA) allows relatively rapid diagnostics of complex electronics by technicians with limited experience. Because of frequency limits and the growing dependence on broadband technologies, ASA must be augmented with other capabilities. To meet this challenge while preserving ease of use, CLEAR proposed an alternative called Complex Signature Analysis (CSA). Tests of ASA and CSA were used to compare capabilities and to determine if the techniques provided an overlapping or complementary capability. The results showed that the methods are complementary.

Oeftering, Richard C.↗
DOE OSTI2017

Fulfillment of Similarity Principles for Pulsed Discharges in a Highly Inhomogeneous Field at High Pressures Under Conditions of Runaway Electron Generation

An analysis of the fulfillment of the similarity law pτ = f(E/p) under conditions of a pulsed discharge triggered in a gas diode with a highly inhomogeneous field at the voltage in the incident wave >100 kV is performed. It is shown that in this case within the pressure range 1–12 atm the deviations from the similarity principles E/p(pτ) and U{sub br}(pd) are due to the nonconservation of proportions in the gas-filled diode geometry. Using a collector, the beam of runaway electrons is for the first time registered behind the anode foil in nitrogen at the pressure from 5 to 12 atm.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2020

Electron Energy Partition across Interplanetary Shocks. III. Analysis

An analysis of model fit results of 15,210 electron velocity distribution functions (VDFs), observed within ±2 hr of 52 interplanetary (IP) shocks by the Wind spacecraft near 1 au, is presented as the third and final part on electron VDFs near IP shocks. The core electrons and protons dominate in the magnitude and change in the partialto-total thermal pressure ratio, with the core electrons often gaining as much or more than the protons. Only a moderate positive correlation is observed between the electron temperature and the kinetic energy change across the shock, while weaker, if any, correlations were found with any other macroscopic shock parameter. No VDF parameter correlated with the shock normal angle. The electron VDF evolves from a narrowly peaked core with flaring suprathermal tails in the upstream to either a slightly hotter core with steeper tails or much hotter flattop core with even steeper tails downstream of the weaker and strongest shocks, respectively. Both quasi-static and fluctuating fields are examined as possible mechanisms modifying the VDF, but neither is sufficient alone. For instance, flattop VDFs can be generated by nonlinear ion acoustic wave stochastic acceleration (i.e., inelastic collisions), while other work suggested they result from the combination of quasi-static and fluctuating fields. This three-part study shows that not only are these systems not thermodynamic in nature; even kinetic models may require modification to include things like inelastic collision operators to properly model electron VDF evolution across shocks or in the solar wind.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS2020

Electron Energy Partition Across Interplanetary Shocks. III. Analysis

An analysis of model fit results of 15,210 electron velocity distribution functions (VDFs), observed within ±2 hr of 52 interplanetary (IP) shocks by the Wind spacecraft near 1 au, is presented as the third and final part on electron VDFs near IP shocks. The core electrons and protons dominate in the magnitude and change in the partialto-total thermal pressure ratio, with the core electrons often gaining as much or more than the protons. Only a moderate positive correlation is observed between the electron temperature and the kinetic energy change across the shock, while weaker, if any, correlations were found with any other macroscopic shock parameter. No VDF parameter correlated with the shock normal angle. The electron VDF evolves from a narrowly peaked core with flaring suprathermal tails in the upstream to either a slightly hotter core with steeper tails or much hotter flattop core with even steeper tails downstream of the weaker and strongest shocks, respectively. Both quasi-static and fluctuating fields are examined as possible mechanisms modifying the VDF, but neither is sufficient alone. For instance, flattop VDFs can be generated by nonlinear ion acoustic wave stochastic acceleration (i.e., inelastic collisions), while other work suggested they result from the combination of quasi-static and fluctuating fields. This three-part study shows that not only are these systems not thermodynamic in nature; even kinetic models may require modification to include things like inelastic collision operators to properly model electron VDF evolution across shocks or in the solar wind.

Solar wind↗
NASA NTRS1994

Measuring track densities in lunar grains using image analysis

We have used digitized scanning electron micrographs and computer image analysis programs to measure track densities in lunar soil grains. Tracks were formed by highly ionizing solar energetic particles and cosmic rays. Back-scattered electron images produced suitable high contrast images for analysis. We used computer counting and measurement of area to obtain track densities. We found an excellent correlation with manual measurements for track densities below 1x10(exp 8) cm(exp -2). For track densities between 1x10(exp 8) to 1x10(exp 9) cm(exp -2) we found that a regression formula using the percentage area covered by tracks gave good agreement with manual measurements. Measurement of tract densities in lunar samples has been a very rewarding technique for measuring exposure ages and soil maturation processes. We have shown that we can reliably measure track densities in lunar grains using image analysis techniques. Automating track counting may allow application of this technique to important problems in regolith dynamics including the ratio of radiation exposure to reworking in various surface and core samples and in regolith breccias.

Blanford, G. E.↗
NASA NTRS1983

Development of a miniature scanning electron microscope for in-flight analysis of comet dust

A description is presented of an instrument which was developed with the original goal of being flown on the International Comet Mission, scheduled for a 1985 launch. The Scanning Electron Microscope and Particle Analyzer (SEMPA) electron miniprobe is a miniaturized electrostatically focused electron microscope and energy dispersive X-ray analyzer for in-flight analysis of comet dust particles. It was designed to be flown on board a comet rendezvous spacecraft. Other potential applications are related to asteroid rendezvous and planetary lander missions. According to the development objectives, SEMPA miniprobe is to have the capability for imaging and elemental analysis of particles in the size range of 0.25 microns and larger.

Conley, J. M.↗
DOE OSTI2024

Insights into Prismatic Loop Formation in Irradiated Fe–Cr Alloys from Hypothesis-Driven Active Learning and Causal Analysis

Neutron and electron irradiation experimental studies conducted on body-centered cubic Fe and Fe–Cr alloys have established two prismatic dislocation loop populations, which have Burgers vectors of either a/2$\langle$111$\rangle$ or a$\langle$100$\rangle$. Here, the loop formation depends on factors such as dose (D), dose rate (D rt ), temperature (T), chromium content (Cr%), and other alloying elements. Hence, it is important to understand how irradiation-induced dislocation loops evolve conditional upon the loop characteristics, such as loop density (DD), average loop size d̅, and irradiation parameters (D, D rt , T, and irradiation type), which is still an active area of research. To understand these complex structure–property relationships, machine learning (ML) is employed in a three-step approach. This includes imputing missing data with a k-nearest neighbor, generating functionalized features, and assessing feature importance with random forest classification and regression. Physics-based features are incorporated in a hypothesis-driven active learning scheme to overcome data unavailability challenges. Insights obtained from ML models (i) to categorize dislocation loop types, show the highest correlation with d̅; (ii) Log(DD), obtained through mathematical formulations involving D, Cr%, d̅, and T (e.g., Log(DD) ~ D + exp(-Cr%) + 1/d̅ and log(DD) ~ D + exp(-Cr%) + 1/T). Hypothesis-driven active learning is able to predict Log(DD) in which the experimental date is not known. Causal models verify cause–effect relationships for dislocation loop classification and irradiation factors in FeCr alloys.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2019

An electrochemical investigation of interfacial electron uptake by the sulfur oxidizing bacterium Thioclava electrotropha ElOx9

Extracellular electron transfer (EET) allows microbes to acquire energy from solid state electron acceptors and donors, such as environmental minerals. Here, this process can also be harnessed at electrode interfaces in bioelectrochemical technologies including microbial fuel cells, microbial electrosynthesis, bioremediation, and wastewater treatment. Improving the performance of these technologies will benefit from a better fundamental understanding of EET in diverse microbial systems. While the mechanisms of outward (i.e. microbe-to-anode) EET is relatively well characterized, specifically in a few metal-reducing bacteria, the reverse process of inward EET from redox-active minerals or cathodes to bacteria remains poorly understood. This knowledge gap stems, at least partly, from the lack of well-established model organisms and general difficulties associated with laboratory studies in existing model systems. Recently, a sulfur oxidizing marine microbe, Thioclava electrotropha ElOx9, was demonstrated to perform electron uptake from cathodes. However, a detailed analysis of the electron uptake pathways has yet to be established, and electrochemical characterization has been limited to aerobic conditions. Here, we report a detailed amperometric and voltammetric characterization of ElOx9 cells coupling cathodic electron uptake to reduction of nitrate as the sole electron acceptor, even in the absence of any added inorganic carbon source. By comparing this cellular activity to spent media controls and using medium exchange experiments, we demonstrate that one of the pathways by which ElOx9 facilitates inward EET is by a direct-contact mechanism through a redox center with a formal potential of -94 mV vs SHE, rather than soluble intermediate electron carriers. In addition to the implications for understanding microbial sulfur oxidation in marine environments, this study highlights the potential for ElOx9 to serve as a convenient and readily culturable model organism for understanding the molecular mechanisms of inward EET.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Titanium-deposition assisted brazing of SiC ceramics using inactive AgCu filler

Highlights: • Reliable joint of SiC ceramics was achieved via Titanium-deposition assisted brazing using inactive AgCu filler metal. • Microstructure characteristic of deposited-SiC brazed joint was investigated in detail. • Ti-deposition assisted brazing inhibited the formation of numerous intermetallic compounds. - Abstract: In this study, active titanium element film was designed to deposit on SiC ceramics directly to enhance the brazability of inactive AgCu brazing alloy on ceramics. The result showed the reliable joint was successfully obtained and the deposition of titanium film on SiC directly inhibited the formation of amounts of intermetallic compounds effectively in the brazing seam. Detailed interfacial microstructure of joint investigated by scanning electron microscope equipped with energy dispersive spectrum analysis and transmission electron microscope revealed that the interfacial reactions were based on deposited Ti film. The typical joint was SiC/TiCu + Ti{sub 2}Cu/TiC/Ti{sub 5}Si{sub 3} containing TiC particles/Ag(s,s) + Cu(s,s)/Ti{sub 5}Si{sub 3} containing TiC particles/TiC/TiCu + Ti{sub 2}Cu/SiC.

36 MATERIALS SCIENCE↗