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At least 109 records · Page 6

Preliminary Investigations of Joining Technologies for Attaching Refractory Metals to Ni-Based Superalloys

In this study, a range of joining technologies has been investigated for creating attachments between refractory metal and Ni-based superalloys. Refractory materials of interest include Mo-47%Re, T-111, and Ta-10%W. The Ni-based superalloys include Hastelloy X and MarM 247. During joining with conventional processes, these materials have potential for a range of solidification and intermetallic formation-related defects. For this study, three non-conventional joining technologies were evaluated. These included inertia welding, electro-spark deposition (ESD) welding, and magnetic pulse welding (MPW). The developed inertia welding practice closely paralleled that typically used for the refractory metals alloys. Metallographic investigations showed that forging during inertia welding occurred predominantly on the nickel base alloy side. It was also noted that at least some degree of forging on the refractory metal side of the joint was necessary to achieve consistent bonding. Both refractory metals were readily weldable to the Hastelloy X material. When bonding to the MarM 247, results were inconsistent. This was related to the higher forging temperatures of the MarM 247, and subsequent reduced deformation on that material during welding. ESD trials using a Hastelloy X filler were successful for all material combinations. ESD places down very thin (5- to 10- m) layers per pass, and interactions between the substrates and the fill were limited (at most) to that layer. For the refractory metals, the fill only appeared to wet the surface, with minimal dilution effects. Microstructures of the deposits showed high weld metal integrity with maximum porosity on the order of a few percent. Some limited success was also obtained with MPW. In these trials, only the T-111 tubes were used. Joints were possible for the T-111 tube to the Hastelloy X bar stock, but the stiffness of the tube (resisting collapse) necessitated the use of very high power levels. These power levels resulted in damage to the equipment (concentrator) during welding. It is of note that the joint made showed the typical wavy bond microstructure associated with magnetic pulse/explosion bond joints. Joints were not possible between the T-111 tube and the MarM 247 bar stock. In this case, the MarM 247 shattered before sufficient impact forces could be developed for bonding.

Gould, Jerry E.↗

Effect of Electrostatic Discharge on Electrical Characteristics of Discrete Electronic Components

This article reports on preliminary results of a study conducted to examine how temporary electrical overstress seed fault conditions in discrete power electronic components that cannot be detected with reliability tests but impact longevity of the device. These defects do not result in formal parametric failures per datasheet specifications, but result in substantial change in the electrical characteristics when compared with pristine device parameters. Tests were carried out on commercially available 600V IGBT devices using transmission line pulse (TLP) and system level ESD stress. It was hypothesized that the ESD causes local damage during the ESD discharge which may greatly accelerate degradation mechanisms and thus reduce the life of the components. This hypothesis was explored in simulation studies where different types of damage were imposed to different parts of the device. Experimental results agree qualitatively with the simulation for a number of tests which will motivate more in-depth modeling of the damage.

Wysocki, Phil↗

NASA Dataset Interoperability Recommendations for Earth Science

NASA ESDS (Earth Science Data and Information System) Dataset Interoperability Working Group has been developing recommendations since 2012 aimed at improving interoperability of EOS (Earth Observing System) datasets. The first set of recommendations were published in 2016 as ESDS RFC-028. The latest set of recommendations is currently undergoing review and will be available as ESDS RFC-036 soon.This talk will inform the ESIP (Earth Science Information Partners) community about the recommendations because their application is relevant to other data producers as well.

Jelenak, Aleksandar↗

An Analysis of the Role of Safety Nets in the National Airspace System

Safe operations of aircraft in the National Airspace System (NAS) may be attributed to many factors, including the application of a variety of safety nets (SNs) as a last line of defense. In preparation for the Next Generation Air Transportation System (NextGen), a review of Aviation Safety Reporting System (ASRS) reports for incidents with positive outcomes was conducted to investigate the importance of current safety nets. The examination of positive outcomes not only shows what went wrong, but also what went right to prevent accidents and “save the day.” More than 400 incident reports for 2015 from the voluntary ASRS reporting database were studied in detail to create event sequence diagrams (ESDs), illustrating the effectiveness of SNs. The developed ESDs are considered top-level, representative models and are limited with respect to being reliably quantitative because they are based on only reports from a single year. The ESDs could offer insights into human systems integration research, such as strategically using technologies as SNs without human interface or alleviating human workload with new technologies to provide resilient recovery from off-nominal conditions ensuring flight safety.

Geuther, Steven↗

ROSA and Solar Cell Module Combined Environments Test Plan

Roll-out solar array (ROSA) technology is an emerging component of the future of spacecraft photovoltaic power subsystems. Qualification and risk reduction testing are necessary to demonstrate design worthiness for spaceflight implementation of the array and solar cell modules. Maxar Space LLC and NASA have undertaken a rigorous combined environment (CE) test campaign for a ROSA design expected to be a part of the Power and Propulsion Element (PPE) for the NASA Gateway which will be an outpost orbiting the Moon. The CE tests consist of several simulated space environment exposures associated with the planned mission: UV radiation, electron/proton radiation, xenon ion plume exposures, and vacuum thermal cycling and electrostatic discharge (ESD). These tests are conducted on small coupons consisting of the planned ROSA flight elements, and all tests are performed at the NASA Marshall Space Flight Center. This paper discusses the test plan, requirements for each environment, and the functional testing performed. Of note is a new approach for the induced primary arc used in the ESD testing, which better simulates the plasma expansion during the ESD event. Progress on executing the test plan is presented.

Space Environments Effects Testing↗

Commercial Smallsat Data Acquisition Program On-ramp #2 Airbus U.S. Synthetic Aperture Radar (SAR) Evaluation Report

In 2017, NASA’s Earth Science Division (ESD) launched the Private-Sector Small Constellation Satellite Data Product Pilot, now referred to as the Commercial Smallsat Data Acquisition (CSDA) program. The objective of CSDA is to identify, evaluate, and acquire commercial remote sensing data that support NASA’s Earth science research and application activities. The Pilot successfully concluded in early 2020, when CSDA transitioned into a sustained program with on-ramping opportunities for new vendors as the industry emerges with new candidates and capabilities. In October 2019, a Request for Information (RFI) seeking capability statements from parties interested in providing data from spaceborne platforms was released for the CSDA on-ramp #2 evaluations. To be responsive to the RFI, the commercial satellite constellations had to consist of three or more operating spacecraft actively collecting data in a non-geostationary orbit with full latitudinal coverage and be U.S. companies. Two vendors responded to the RFI and were evaluated by a committee composed of NASA ESD leadership, program managers, and scientists. Both vendors satisfied the RFI requirements and were asked to respond to a Request for Proposal (RFP). After review of the proposals, NASA entered into a Blanket Purchase Agreement (BPA) with Airbus Defense and Space GEO, Inc. (Airbus) U.S. in September 2021 and with BlackSky Geospatial Solutions, Inc. (BlackSky) in November 2021. In this report, CSDA provides an evaluation of the usefulness of data provided by the Airbus U.S. Synthetic Aperture Radar (SAR) satellite constellation, consisting of TerraSAR-X (launched in 2007), TanDEM-X (launched in 2010), and PAZ (launched in 2018), for advancing NASA’s Earth system science research and applications. The evaluation of the BlackSky commercial data will be provided in a separate report. To conduct the Airbus evaluation, NASA’s ESD augmented 13 existing research projects that could potentially benefit from, and had the expertise to evaluate, the commercial data being considered for longer-term purchase. Investigators from NASA’s Research and Analysis Program science focus areas and from NASA’s Applied Sciences Program elements participated in the evaluation. A summary of the research areas evaluated by the Principal Investigator (PI) teams is presented in Figure 3. CSDA also funded a dedicated activity to evaluate the satellite data quality (calibration and geolocation) independently by assessing the accuracy of data from Airbus. Evaluation activities were carried out by the selected PIs from December 7, 2022, to December 7, 2023. Delivery of datasets requested by the researchers began in January 2023. The vendors were evaluated on the accessibility of data, accuracy and completeness of metadata, and promptness and quality of user support services. Datasets purchased during the evaluation have been archived by NASA and will be made available to current and future government-funded researchers in accordance with the End User License Agreement (EULA). This synthesis report distills and integrates the findings of research reports commissioned by NASA for the Airbus evaluation. This report also includes recommendations that inform the way ahead for the program. The scientific results from the evaluations demonstrated that the commercial data from Airbus were able to advance NASA research and applications. However, the PIs encountered limitations that diminished the usefulness of the data due to the amount of effort that was required to access, preprocess, and analyze these data. One significant issue encountered was the limited spatial and temporal coverage of the data in the Airbus archive that could be used to conduct time series analyses or assessments over large spatial scales. Overall, however, the utility and the quality of the evaluated data outweighed the difficulties encountered, and NASA has concluded that the Airbus SAR data would complement NASA’s existing Earth observation capabilities and Airbus U.S. would qualify to participate in the sustained phase of the program.

Batuhan Osmanoglu↗

NASA Earth Science Division’s Commitment to Increasing Safety in the Field

NASA's Earth Science Division (ESD) has led and supported field campaign research over many decades focused on advancing fundamental research, testing new instrument technologies, and promoting career development. ESD field campaign research is conducted over a wide range of projects that vary in size, science focus area, location, platform type, and people. ESD leadership has created a task team to address campaign physical and mental safety, with the goal of providing all participants in NASA field campaign research with an environment that promotes research, safety, inclusivity, and a positive experience. Building on resources that have been developed both within and outside NASA, we report on the task team’s accomplishments and near-term plans, including the recent establishment of a best practices document and guidelines for the development of “agreement of behaviors” document for field teams. We also describe progress in the development of an online training module for field campaign participation, the incorporation of campaign safety language in forthcoming NASA ROSES solicitations, and outreach activities. Finally, we report on recent joint interactions with the NASA Planetary Science Division’s Ethics in Fieldwork team.

Ocean-based measurements↗

JPL standard for electrostatic disharge control

This document establishes the requirements for protection of electronic parts and assemblies against ESD during the various stages of product development. This document is released and maintained by the Jet Propulsion Laboratory ESD Control Engineer within the Quality Assurance Office.

ESD electrostatic discharge control↗

Methods of Measuring Secondary Electron Emission and Analysis of Spacecraft Charging Simulation

The scope of the internship project was to help the Electrostatics and Surface Physics Laboratory (ESPL) at KSC gain an understanding as to what parameters related to secondary electron emission (SEE), and electrostatic discharge (ESD) could be measured within its own facilities. As well as assistance in developing a plan for the ESPL to acquire the capabilities to measure other necessary parameters, to reduce the reliance on measurement data from facilities outside of the agency. The intern also worked closely with agency customers of the Launch Services Program (LSP) in expanding the MAPTIS database to incorporate various electrostatic and physical properties of materials used in the Gateway Program. This involved cross-center collaboration with industry and NASA contracted academia members in order to fill in the gaps of data that is missing from the database. Overall, the internship provided assistance in coordinating the approval for more materials to be added to the MAPTIS database, and continuing to assist the team at the ESPL in their consulting work for the agency through the use of various spacecraft charging and ESD simulation programs (i.e., NASCAP, NUMIT2.1). As well as assisting in the CAD design and implementation of an electrodynamic dust shield (EDS) for use in upcoming spaceflight missions. This was all done with the aim of helping the ESPL demonstrate its capabilities for the agency, and to continue expanding and localizing measurement techniques at KSC to help streamline obtaining the information NASA needs to ensure safety in current and future missions.

dust↗

Halting Oxygen Evolution to Achieve Long Cycle Life in Sodium Layered Cathodes

Oxygen redox chemistries at high voltage have materialized as a revolutionary paradigm for cathodes with high-energy density; however, they are plagued by the challenges of labile oxygen loss and rapid degradations upon cycling, even after concerted endeavors from the research community. Here we propose a multi-concentration stratagem propelled by entropy reinforcement to enhance the electronic structure disorder (ESD) at high desodiation states for impeding undesired oxygen mobility and ensuring controlled oxygen activity, elucidated by density functional theory calculations. The increased disorder strengthens the reversible electrochemistry of lattice oxygen redox, leading to effectively suppressed P−O structural evolution and highly stable localized TMO 6 octahedral environments, as demonstrated by soft/hard X-ray absorption spectroscopy. Furthermore, through a comparative analysis of sodium-layered cathodes with different configuration entropy, we reveal that a high-entropy state induced by cationic disordering has the capacity to perturb cationic redox boundaries, significantly restraining the formation of detrimental O′3 phases. As a consequence, the high-voltage cycling stability has been greatly upgraded, up to 4.4 V versus Na + /Na, with an impressive 90.1 % capacity retention at 1 C over 100 cycles and 76.1 % capacity retention at 2 C over 300 cycles. In conclusion, the resilient oxygen redox, enabled through the control of ESD, broadens the horizons for entropy engineering and lays the foundation for advancements in high-energy, long-cycling, and safe batteries.

25 ENERGY STORAGE↗

Properties of different LLM-105 preparations

LLM-105 (2,6-diamino-3,5-dinitropyrazine-1-oxide) has been prepared at several different size quantities (~10–70 Kg) and not subjected to further purification, such as recrystallization. Chemical and physical properties were compared—small-scale safety testing (impact, friction, ESD), thermal (chemical reactivity, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), one-dimensional time-to-explosion (ODTX)), morphological (particle-size distribution (PSD), scanning electron microscopy (SEM), powder x-ray diffraction (PXRD), skeletal density). Each preparation had similar properties to the other preparations except for PSD and PXRD. For PSD, all preparations exhibited a mono-modal distribution with a variation in median values from ~ 40 μm to over 80 μm. All PXRD values indicated the same morphology with minor variations in crystal orientations. Possible polymorphism was also observed in a few cases. SEM images and PXRD indicate all preparations to be diamond-type and X-type crystals with some twinning. Impact, friction, and ESD and thermal sensitivities values are consistent with these type of crystal habits as seen in vast literature studies.

Explosive characterization↗

Plasma charging testing of communication satellites

A discussion is given of ESD as a radiated electromagnetic environment and compares the ESD environment to a standard EMI test environment. An arc generator used to assess the sensitivity of typical spacecraft electronics is described. The results of radiated susceptibility tests conducted on breadboard circuits and a satellite electrical model of a communication satellite are discussed.

Rosen, F.↗

Internal electrostatic discharge hazard risk assessment to the Galileo orbiter

A worst case assessment was performed on the Command Data System (CDS) multilayer printed circuit board and an output power transformer module in the power subsystem. An estimate of the Jovian environment during the 35 hour orbit insertion was supplied by JPL and used as an input to calculate the electron transport into the Galileo components. A radiation shielding analysis computer code, CHARGE, calculated the electron transport deposition trapped in the anticipated sensitive areas of the multilayer board and transformer module. Based on these trapped charge calculations electric fields were calculated between the identified isolated areas and the spacecraft ground. The results of the assessment of electrostatic discharge (DSD) in the CDS multilayer printed circuit board indicate that the probability of ESD in the FR4 is low. The probability of ESD in the components attached to the multilayer board, however, is uncertain based on a lack of prior experimental data.

Schmidt, R. E.↗

Electron-stimulated desorption study of hydrogen-exposed aluminum films

H2 adsorption of evaporated clean and H2-exposed aluminum films is investigated by using the electron-stimulated desorption (ESD) method. A strong H(+)ESD signal is observed on a freshly evaporated aluminum surface which is clean according to previously proposed cleanlines criteria. An increased H(+) yield on H2 exposure is also observed. However, the increasing rate of H(+) emission could be directly correlated with small increases in H2O partial pressure during H2 exposure. It is proposed that the oxidation of aluminum by water vapor and subsequent adsorption of H2 or water is the primary process of the enhanced high H(+) yield during H2 exposure.

Park, CH.↗

Simulation of external and internal electrostatic discharges at the spacecraft system test level

Environmental test activities concerned with space plasma-caused charging and discharing phenomena are discussed. It is pointed out that the origin of such an electrostatic discharge (ESD) is charging of spacecraft dielectrics by an energetic plasma in geosynchronous orbit, Jupiter's magnetosphere, or other similar space environments. In dealing with environmental testing problems, it is necessary to define the location and magnitude of any ESD's in preparation for a subsequent simulation of the given conditions. Questions of external and internal charging are discussed separately. The environmental hazard from an external discharge can be assessed by viewing the dielectric surface as one side of a parallel plate capacitor. In the case of internal charging, the level of environmental concern depends on the higher energy spectrum of the ambient electrons.

Whittlesey, A.↗

Moisture interaction and stability of ZOT (Zinc Orthotitanate) thermal control spacecraft coating

Two of the many performance requirements of the zinc orthotitanate (ZOT) ceramic thermal control paint covering parts of the Jupiter-bound Galileo spacecraft are that it be sufficiently electrically conductive so as to prevent electrostatic discharge (ESD) damage to onboard electronics and that it adhere to and protect the substrate from corrosion in terrestrial environments. The bulk electrical resistivity of ZOT on an aluminum substrate was measured over the ranges 22 C to 90 C and 0 percent RH to 100 percent RH, and also in soft (10 (minus 2) Torr) and hard (10 (minus 7) Torr) vacuums. No significant temperature dependence was evident, but measured resistivity values ranged over 9 orders of magnitude: 10 to the 5th power ohm-cm at 100 percent RH greater than 10 to the 12th power ohm-cm in a hard vacuum. The latter value violates the ESD criterion for a typical 0.019 cm thick coating. The corrosion study involved exposing typical ZOT substrate combinations to two moisture environments - 30 C/85 percent RH and 85 C/85 percent RH - for 2000 hours, during which time the samples were periodically removed for front-to-back electrical resistance and scratch/peel test measurements. It was determined that the ZOT/Al and ZOT/Mg systems are stable (no ZOT delamination), although some corrosion (oxide formation) and resistivity increases observed among the ZOT/Mg samples warrant that exposure of some parts to humid environments be minimized.

Mon, Gordon R.↗

SRM propellant, friction/ESD testing

Following the Pershing 2 incident in 1985 and the Peacekeeper ignition during core removal in 1987, it was found that propellant can be much more sensitive to Electrostatic Discharges (ESD) than ever before realized. As a result of the Peacekeeper motor near miss incident, a friction machine was designed and fabricated, and used to determine friction hazards during core removal. Friction testing with and electrical charge being applied across the friction plates resulted in propellant ignitions at low friction pressures and extremely low ESD levels. The objective of this test series was to determine the sensitivity of solid rocket propellant to combined friction pressure and electrostatic stimuli and to compare the sensitivity of the SRM propellant to Peacekeeper propellant. The tests are fully discussed, summarized and conclusions drawn.

Campbell, L. A.↗

Experience, problems, and subtleties of electrostatic discharge at JPL

Approaches used to control electrostatic discharge (ESD) at the JPL are discussed. ESD control problems generally occur in the following: (1) wrist straps; (2) outer garments that preclude the generation of static charge; and (3) materials, items, techniques, or processes permitting the development of a static charge. Consideration is given to the cleaning of antistatic materials, outside contracts, vapor degreasing, and electrostatically charged electrical cables.

Woods, William R.↗