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NASA NTRS2013

Standard Practices for Usage of Inductive Magnetic Field Probes with Application to Electric Propulsion Testing

Inductive magnetic field probes (also known as B-dot probes and sometimes as B-probes or magnetic probes) are useful for performing measurements in electric space thrusters and various plasma accelerator applications where a time-varying magnetic field is present. Magnetic field probes have proven to be a mainstay in diagnosing plasma thrusters where changes occur rapidly with respect to time, providing the means to measure the magnetic fields produced by time-varying currents and even an indirect measure of the plasma current density through the application of Ampère's law. Examples of applications where this measurement technique has been employed include pulsed plasma thrusters and quasi-steady magnetoplasmadynamic thrusters. The Electric Propulsion Technical Committee (EPTC) of the American Institute of Aeronautics and Astronautics (AIAA) was asked to assemble a Committee on Standards (CoS) for Electric Propulsion Testing. The assembled CoS was tasked with developing Standards and Recommended Practices for various diagnostic techniques used in the evaluation of plasma thrusters. These include measurements that can yield either global information related to a thruster and its performance or detailed, local data related to the specific physical processes occurring in the plasma. This paper presents a summary of the standard, describing the preferred methods for fabrication, calibration, and usage of inductive magnetic field probes for use in diagnosing plasma thrusters. Inductive magnetic field probes (also called B-dot probes throughout this document) are commonly used in electric propulsion (EP) research and testing to measure unsteady magnetic fields produced by time-varying currents. The B-dot probe is relatively simple in construction, and requires minimal cost, making it a low-cost technique that is readily accessible to most researchers. While relatively simple, the design of a B-dot probe is not trivial and there are many opportunities for errors in probe construction, calibration, and usage, and in the post-processing of data that is produced by the probe. There are typically several ways in which each of these steps can be approached, and different applications may require more or less vigorous attention to various issues.

Polzin, Kurt A.↗

NASA NTRS2015

Wideband Single Crystal Transducer for Bone Characterization

Phase II objectives: Optimize the Phase I transducer for sensitivity; Test different transmit signals for optimum performance; Demonstrate compatibility with electronics; Confirm additional transducer capabilities over conventional systems by calibrating with other methods.

Sahul, Raffi↗

NASA NTRS2017

Estimating Evaporative Fraction From Readily Obtainable Variables in Mangrove Forests of the Everglades, U.S.A.

A remote-sensing-based model to estimate evaporative fraction (EF) the ratio of latent heat (LE; energy equivalent of evapotranspiration -ET-) to total available energy from easily obtainable remotely-sensed and meteorological parameters is presented. This research specifically addresses the shortcomings of existing ET retrieval methods such as calibration requirements of extensive accurate in situ micro-meteorological and flux tower observations, or of a large set of coarse-resolution or model-derived input datasets. The trapezoid model is capable of generating spatially varying EF maps from standard products such as land surface temperature [T(sub s)] normalized difference vegetation index (NDVI)and daily maximum air temperature [T(sub a)]. The 2009 model results were validated at an eddy-covariance tower (Fluxnet ID: US-Skr) in the Everglades using T(sub s) and NDVI products from Landsat as well as the Moderate Resolution Imaging Spectroradiometer (MODIS) sensors. Results indicate that the model accuracy is within the range of instrument uncertainty, and is dependent on the spatial resolution and selection of end-members (i.e. wet/dry edge). The most accurate results were achieved with the T(sub s) from Landsat relative to the T(sub s) from the MODIS flown on the Terra and Aqua platforms due to the fine spatial resolution of Landsat (30 m). The bias, mean absolute percentage error and root mean square percentage error were as low as 2.9% (3.0%), 9.8% (13.3%), and 12.1% (16.1%) for Landsat-based (MODIS-based) EF estimates, respectively. Overall, this methodology shows promise for bridging the gap between temporally limited ET estimates at Landsat scales and more complex and difficult to constrain global ET remote-sensing models.

trapezoid↗

NASA NTRS2018

Updates to the Absolute Radiometric Accuracy of the AIRS on Aqua

The Atmospheric Infrared Sounder (AIRS) on the EOS Aqua Spacecraft was launched on May 4, 2002. The AIRS was designed to measure small changes in the global hydro-thermodynamic cycle and has demonstrated exceptional radiometric and spectral stability and accuracy in-orbit. This accuracy is achieved by transferring the calibration from a Large Area Blackbody (LABB) to the On-Board Calibrator (OBC) blackbody during preflight testing. The LABB theoretical emissivity is in excess of 0.9999 and temperature uncertainty is less than 50 mK. The LABB emitted radiance is NIST traceable through thermistors located on the internal surfaces. The AIRS also provides a full aperture space view every scan for offset calibration. AIRS nonlinearity and polarization calibration coefficients were based on pre-flight testing and have been amongst the highest uncertainty sources in the calibration. A recent method using on-board space view data has reduced the uncertainty of the polarization coefficients and use of separate A side and B side data from preflight testing has reduced the uncertainty of the nonlinearity estimates. An update to the system radiometric uncertainty is made based on the new data and is presented in this paper.

Weiler, Margaret H.↗

NASA NTRS2015

A plasma-based non-intrusive point source for acoustic beamforming applications

A laser-generated plasma acoustic point source is used to directly measure the point spread function (PSF) of a microphone phased array. In beamforming analysis of microphone phased array data, the true acoustic field is convolved with the array's PSF. By directly measuring the PSF, corrections to the array analysis can be computed and applied. The acoustic source is measured in an open-jet aeroacoustic facility to evaluate the effects of sampling rate, microphone installation, source shift, reflections, shear layer refraction and model presence. Results show that measurements exhibit behavior consistent with theory with regard to source shift and shear layer refraction. Application of a measured PSF in beamforming analysis shows the process provides an effective in-situ method for array calibration both with and without flow and allows for corrections to incorporate reflections and scattering. The technique improves the agreement of beamforming results with the true spectrum of a known source, especially in the presence of reflections.

phased array↗

DOE OSTI2016

Thermally determining flow and/or heat load distribution in parallel paths

A method including obtaining calibration data for at least one sub-component in a heat transfer assembly, wherein the calibration data comprises at least one indication of coolant flow rate through the sub-component for a given surface temperature delta of the sub-component and a given heat load into said sub-component, determining a measured heat load into the sub-component, determining a measured surface temperature delta of the sub-component, and determining a coolant flow distribution in a first flow path comprising the sub-component from the calibration data according to the measured heat load and the measured surface temperature delta of the sub-component.

42 ENGINEERING↗

DOE OSTI2017

Thermally determining flow and/or heat load distribution in parallel paths

42 ENGINEERING↗

DOE OSTI2017

Predicting uniaxial compressive strength from empirical relationships between ultrasonic p-wave velocities, porosity, and core measurements in a potential geothermal reservoir, Snake River Plain, Idaho

Empirical, core-based, predictive correlations for the calculation of uniaxial compressive strength (UCS) were developed from compressive sonic velocity measurements (55 whole core samples) and porosity, density, and unconfined compressive tests (110 whole core samples). The samples were collected at 55 different depths in a 550 m (1800 ft) interval of core from the MH-2 borehole located in southern Idaho, USA. The western Snake River Plain is a known region of high heat flow and the borehole was drilled into a potential geothermal reservoir characterized by artesian flow of high-temperature (~140°C) fluids from fractured basalt. UCS was measured in unconfined compressive tests, density and porosity were measured using a He-pycnometer, and p-wave velocities were measured in a pressure vessel under variable confining pressures. We use correlations between density and p-wave velocity (R 2 = 0.91), UCS and porosity (R 2 = 0.78), and UCS and p-wave velocity (R 2 = 0.79) in a method to calculate calibrated UCS from wireline logs. Here, the impact of this predictive correlation is that UCS can be calculated from as little as a bulk density log when sonic logs and core are not available, greatly increasing the number of wells in which we can obtain a local UCS estimate.

15 GEOTHERMAL ENERGY↗

DOE OSTI2026

Determining the Solubility Behavior of Kogarkoite in Simulated Nuclear Waste

Kogarkoite (Na 3 FSO 4 ) is a sparingly soluble fluoride–sulfate double salt that has been identified in high level nuclear waste sludge at the Hanford Site and, more recently, in sludge batch compilation samples at the Savannah River Site (SRS). Due to its complex dissolution behavior, which exhibits an inverse dependence on sodium ion activity, the presence of this mineral poses significant challenges to waste retrieval and processing. Incomplete dissolution during sludge washing can lead to the retention of fluoride and sulfate in the high-level waste feed, potentially causing the formation of corrosive, immiscible molten salt layers, known as "glass gall,” in vitrification melters. Current efforts to optimize flowsheet parameters and wash-water volumes are hindered by the absence of a commercially available, certified reference material, which prevents the accurate calibration of analytical methods and the verification of dissolution kinetics. To address this critical gap, this research focuses on the laboratory synthesis of pure Kogarkoite to serve as a standard for comprehensive solubility and washing performance testing. A coupled synthesis and simulant campaign was executed using an evaporative crystallization protocol designed to replicate the dynamic concentration effects observed in tank farm operations. Thirteen simulant matrices were prepared by dissolving systematically varied ratios of sodium fluoride (NaF) and sodium sulfate (Na 2 SO 4 ) in deionized water under three distinct caustic regimes: 0.0 g (control), 4.0 g (~1 M), and 12.0 g (~3 M) sodium hydroxide (NaOH). While thermodynamic equilibrium models suggest that high-caustic environments should favor the stability of the double salt7, results from this evaporative study at 25 0 C revealed a distinct kinetic divergence. Simulants with high hydroxide loading predominantly yielded large, blocky crystals of sodium sulfate decahydrate (Na 2 SO 4 .10H 2 O). Successful synthesis of pure Kogarkoite was achieved exclusively in specific NaOH-free compositional windows, where the precipitate manifested as fine, opaque granular aggregates. Ion chromatography (IC) analysis confirmed phase purity through the simultaneous stoichiometric depletion of both fluoride and sulfate from the supernatant. This successful synthesis establishes a reproducible route to generate bulk Kogarkoite, enabling the subsequent phase of quantitative dissolution testing using inhibited water to optimize sludge-batch assembly.

Sarker, Md Sharif [Florida International Univ. (FI↗

DOE OSTI2018

High-Throughput Material Characterization using the Virtual Fields Method

Modeling material and component behavior using finite element analysis (FEA) is critical for modern engineering. One key to a credible model is having an accurate material model, with calibrated model parameters, which describes the constitutive relationship between the deformation and the resulting stress in the material. As such, identifying material model parameters is critical to accurate and predictive FEA. Traditional calibration approaches use only global data (e.g. extensometers and resultant force) and simplified geometries to find the parameters. However, the utilization of rapidly maturing full-field characterization techniques (e.g. Digital Image Correlation (DIC)) with inverse techniques (e.g. the Virtual Feilds Method (VFM)) provide a new, novel and improved method for parameter identification. This LDRD tested that idea: in particular, whether more parameters could be identified per test when using full-field data. The research described in this report successfully proves this hypothesis by comparing the VFM results with traditional calibration methods. Important products of the research include: verified VFM codes for identifying model parameters, a new look at parameter covariance in material model parameter estimation, new validation techniques to better utilize full-field measurements, and an exploration of optimized specimen design for improved data richness.

36 MATERIALS SCIENCE↗

NASA NTRS2006

Insitu Calibration of Quartz Crystal Microbalances

Computer models that predict the rate at which molecular contamination will deposit on optical surfaces typically use outgassing source terms, measured with quartz crystal microbalances, as a basis for the prediction. The American Society of Testing and Materials, Standard Test Method for Contamination Outgassing Characteristics of Spacecraft Materials (Method E-1559), is probably the best know technique used by the aerospace community to measure the outgassing rates or source terms of materials. A simple method for the insitu calibration of quartz crystal microbalances, based on the heat of enthalphy of Adipic Acid, has been developed and demonstrated by the Marshall Space Flight Center, Environmental Effects Group. The calibration has been demonstrated over a sample temperature range of 25 to 66 degrees Celsius and deposition rates of 7 x 10 (exp -11) grams/cm(sup 2)-s and greater, for several measurement system configurations. This calibration technique is fully compatible with the American Society for Testing and Materials, Method E-1559, as well as other methodology. The calibration requires no modification of outgassing facilities employing an effusion cell and does not degrade the performance or function of typical vacuum systems.

Albyn, Keith↗

DOE OSTI2019

Can liquid cloud microphysical processes be used for vertically pointing cloud radar calibration?

Cloud radars are unique instruments for observing cloud processes, but uncertainties in radar calibration have frequently limited data quality. Thus far, no single robust method exists for assessing the calibration of past cloud radar data sets. Here, we investigate whether observations of microphysical processes in liquid clouds such as the transition of cloud droplets to drizzle drops can be used to calibrate cloud radars. Specifically, we study the relationships between the radar reflectivity factor and three variables not affected by absolute radar calibration: the skewness of the radar Doppler spectrum ( γ ), the radar mean Doppler velocity ( W ), and the liquid water path (LWP). For each relation, we evaluate the potential for radar calibration. For γ and W , we use box model simulations to determine typical radar reflectivity values for reference points. We apply the new methods to observations at the Atmospheric Radiation Measurement (ARM) sites North Slope of Alaska (NSA) and Oliktok Point (OLI) in 2016 using two 35 GHz K a -band ARM Zenith Radars (KAZR). For periods with a sufficient number of liquid cloud observations, we find that liquid cloud processes are robust enough for cloud radar calibration, with the LWP-based method performing best. We estimate that, in 2016, the radar reflectivity at NSA was about 1±1  dB too low but stable. For OLI, we identify serious problems with maintaining an accurate calibration including a sudden decrease of 5 to 7 dB in June 2016.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2015

Predictive Maturity of Multi-Scale Simulation Models for Fuel Performance

The project proposed to provide a Predictive Maturity Framework with its companion metrics that (1) introduce a formalized, quantitative means to communicate information between interested parties, (2) provide scientifically dependable means to claim completion of Validation and Uncertainty Quantification (VU) activities, and (3) guide the decision makers in the allocation of Nuclear Energy’s resources for code development and physical experiments. The project team proposed to develop this framework based on two complimentary criteria: (1) the extent of experimental evidence available for the calibration of simulation models and (2) the sophistication of the physics incorporated in simulation models. The proposed framework is capable of quantifying the interaction between the required number of physical experiments and degree of physics sophistication. The project team has developed this framework and implemented it with a multi-scale model for simulating creep of a core reactor cladding. The multi-scale model is composed of the viscoplastic self-consistent (VPSC) code at the meso-scale, which represents the visco-plastic behavior and changing properties of a highly anisotropic material and a Finite Element (FE) code at the macro-scale to represent the elastic behavior and apply the loading. The framework developed takes advantage of the transparency provided by partitioned analysis, where independent constituent codes are coupled in an iterative manner. This transparency allows model developers to better understand and remedy the source of biases and uncertainties, whether they stem from the constituents or the coupling interface by exploiting separate-effect experiments conducted within the constituent domain and integral-effect experiments conducted within the full-system domain. The project team has implemented this procedure with the multi- scale VPSC-FE model and demonstrated its ability to improve the predictive capability of the model. Within this framework, the project team has focused on optimizing resource allocation for improving numerical models through further code development and experimentation. Related to further code development, we have developed a code prioritization index (CPI) for coupled numerical models. CPI is implemented to effectively improve the predictive capability of the coupled model by increasing the sophistication of constituent codes. In relation to designing new experiments, we investigated the information gained by the addition of each new experiment used for calibration and bias correction of a simulation model. Additionally, the variability of ‘information gain’ through the design domain has been investigated in order to identify the experiment settings where maximum information gain occurs and thus guide the experimenters in the selection of the experiment settings. This idea was extended to evaluate the information gain from each experiment can be improved by intelligently selecting the experiments, leading to the development of the Batch Sequential Design (BSD) technique. Additionally, we evaluated the importance of sufficiently exploring the domain of applicability in experiment-based validation of high-consequence modeling and simulation by developing a new metric to quantify coverage. This metric has also been incorporated into the design of new experiments. Finally, we have proposed a data-aware calibration approach for the calibration of numerical models. This new method considers the complexity of a numerical model (the number of parameters to be calibrated, parameter uncertainty, and form of the model) and seeks to identify the number of experiments necessary to calibrate the model based on the level of sophistication of the physics. The final component in the project team’s work to improve model calibration and validation methods is the incorporation of robustness to non-probabilistic uncertainty in the input parameters. This is an improvement to model validation and uncertainty quantification stemming beyond the originally proposed scope of the project. We have introduced a new metric for incorporating the concept of robustness into experiment-based validation of numerical models. This project has accounted for the graduation of two Ph.D. students (Kendra Van Buren and Josh Hegenderfer) and two M.S. students (Matthew Egeberg and Parker Shields). One of the doctoral students is now working in the nuclear engineering field and the other one is a post-doctoral fellow at the Los Alamos National Laboratory. Additionally, two more Ph.D. students (Garrison Stevens and Tunc Kulaksiz) who are working towards graduation have been supported by this project.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2015

Contributed Review: Absolute spectral radiance calibration of fiber-optic shock-temperature pyrometers using a coiled-coil irradiance standard lamp

We describe an accurate and precise calibration procedure for multichannel optical pyrometers such as the 6-channel, 3-ns temporal resolution instrument used in the Caltech experimental geophysics laboratory. We begin with a review of calibration sources for shock temperatures in the 3000-30 000 K range. High-power, coiled tungsten halogen standards of spectral irradiance appear to be the only practical alternative to NIST-traceable tungsten ribbon lamps, which are no longer available with large enough calibrated area. However, non-uniform radiance complicates the use of such coiled lamps for reliable and reproducible calibration of pyrometers that employ imaging or relay optics. Careful analysis of documented methods of shock pyrometer calibration to coiled irradiance standard lamps shows that only one technique, not directly applicable in our case, is free of major radiometric errors. We provide a detailed description of the modified Caltech pyrometer instrument and a procedure for its absolute spectral radiance calibration, accurate to ±5%. We employ a designated central area of a 0.7× demagnified image of a coiled-coil tungsten halogen lamp filament, cross-calibrated against a NIST-traceable tungsten ribbon lamp. We give the results of the cross-calibration along with descriptions of the optical arrangement, data acquisition, and processing. We describe a procedure to characterize the difference between the static and dynamic response of amplified photodetectors, allowing time-dependent photodiode correction factors for spectral radiance histories from shock experiments. We validate correct operation of the modified Caltech pyrometer with actual shock temperature experiments on single-crystal NaCl and MgO and obtain very good agreement with the literature data for these substances. We conclude with a summary of the most essential requirements for error-free calibration of a fiber-optic shock-temperature pyrometer using a high-power coiled tungsten halogen irradiance standard lamp.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1989

A laboratory investigation into microwave backscattering from sea ice

The purpose of the research reported here was to determine the sources of scattering of artificial sea ice, to compare backscatter measurements semi-quantitatively with theoretical predictions, and to develop inexpensive polarimetric radars for sea ice backscatter studies. A brief review of the dielectric properties of sea ice and of commonly used surface and volume scattering theories is presented. We provide a description of the backscatter measurements performed and experimental techniques used. The development of inexpensive short-range polarimetric radars is discussed. We discuss limitations of this system and the development of a radar that avoids the oscillator instability problems of continuously tunable oscillators by doing measurements at discrete frequencies, using a synthesized frequency source. We present results of simple test of copolar phase capability and a simple method of doing phase calibrations. We discuss ice surface characterization data and techniques. We also present a method of estimating the standard deviation of rms height and correlation length for cases of few data points.

Bredow, Jonathan W.↗

NASA NTRSDate not supplied

Comparison of Detector Based and Source Based Absolute Radiance Standards

A detailed comparison of two separate radiometric calibration standards was conducted with analysis of error sources for each. One is a detector based standard, with radiance traceable to fundamental units using the electrical substitution method. The other is based on a calibrated field emission lamp (FEL) generating blackbody radiation. This study was motivated by the discontinuance of the FEL lamps by the manufacturer and a desire to calibrate sensors using non-blackbody spectral profiles. Three spectrometers were calibrated simultaneously by both methods to separate spectrometer artifacts from differences in the radiometric standards and error in the irradiance to radiance conversion procedure needed for the FEL. Conducting this study now is important to provide continuity between the extensive prior FEL based calibration database with a replacement method while calibrated FEL lamps are still available. This also begins a longer term repeatability study of the spectrometers used in this work for evaluation as calibrated transfer standards, usable with both monochromatic and broad spectrum radiance sources. Eliminating the tie to the FEL blackbody spectrum with a detector based standard allows for flexibility in the illumination source. In particular, for Earth science sensors intended for use with sunlit scenes, augmenting traditional tungsten halogen lighting with blue and ultraviolet light emitting diodes allows for a better match to the solar spectrum during laboratory testing.

radiometry↗

NASA NTRSDate not supplied

Comparison of Detector Based and Source Based Absolute Radiance Standards

radiometry↗

DOE OSTI2016

In situ wavelength calibration of the edge CXS spectrometers on JET

A method for obtaining an accurate wavelength calibration over the entire focal plane of the JET edge CXS spectrometers is presented that uses a combination of the fringe pattern created with a Fabry–Pérot etalon and a neon lamp for cross calibration. The accuracy achieved is 0.03 Å, which is the same range of uncertainty as when neglecting population effects on the rest wavelength of the CX line. For the edge CXS diagnostic, this corresponds to a flow velocity of 4.5 km/s in the toroidal direction or 1.9 km/s in the poloidal direction.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗