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First Trials with EMPHASIS

This report presents a series of three EMPHASIS trial problems we ran in March 2019, to demonstrate (1) that we can set up and run an SGEMP calculation, and (2) that we understand the nature and units of the input specifications and the output results. As these are the first EMPHASIS problems we have set up and run, we present some of the input decks and some of the lessons learned, to better orient a reader who might also be a new user of EMPHASIS. The EMPHASIS manual and the ITS manual are both good, but not complete enough to set up and run these applications. Substantial trial and error was still required. The trial problems are all based on an evacuated aluminum cylinder with 1 m inner radius and 1 m inner height. The cylinder is 100 mil thick. We take the axis of symmetry to be the z axis. The aluminum cylinder will be treated as perfectly conducting. The trial problems are (1) the cavity driven with a short pulse on an antenna at the center of the cavity, (2) the cavity driven by a prescribed short pulse of photocurrent injected normally from the bottom inside of the cylinder, and (3) the cavity driven by a prescribed short pulse of x-rays normally incident on the bottom outside of the cylinder.

42 ENGINEERING↗

Building Interfaces with Echo Using R

The following report details the functionality that was developed to directly query the MongoDB and read in echo records from within R, and the ability to create a cinema database directly from echo records. Both of these efforts used the data collected under the MINOS project for development. The nuclear facility under consideration is the High-Flux Isotope Reactor (HFIR) and co-located Radiochemical Engineering Development Center (REDC) at Oak Ridge National Laboratory in Oak Ridge, TN. HFIR is an 85 MW research reactor and is used primarily for production of a medical radioisotopes, material irradiation experiments, neutron activation, and neutron scattering. Targets for the reactor are fabricated and processed and dissolved at REDC, in addition to other glove-box and hot-cell type activities. An overhead view of the facility is provided. The rest of the report is organized as follows: Section 2 describes how to query the MongoDB and load in echo records from within R, with background information on the database type, MongoDB, and the file format of echo records, hdf5, as well as lessons learned during the development phase. Section 3 details the functionality and usage of creating a cinema database directly from echo records within R. A series of appendixes display all the R code (Section 5), some example scripts where the code is used (Section 6), and useful links for further exploration (Section 7).

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Concentrating Solar Power Best Practices Study

The primary objective of this Concentrating Solar Power Best Practices Study is to publish best practices and lessons learned from the engineering, construction, commissioning, operations, and maintenance of existing concentrating solar power (CSP) parabolic trough and power tower systems. To accomplish this objective, information was solicited from many owners, operators, and engineering, procurement, and construction (EPC) contractors, independent engineers, and other stakeholders of parabolic trough and central receiver plants (also commonly referred to as power towers). Information was gathered through in-person or online meetings, site visits, and questionnaires sent to participants. The project team held about 50 information-gathering sessions with participants over the course this effort; and in the process, it collected information from participants representing nearly 80% of CSP plants operating worldwide.

14 SOLAR ENERGY↗

Blind Modeling Validation Exercises Using the Horizontal Dry Cask Simulator

The U.S. Department of Energy (DOE) established a need to understand the thermal-hydraulic properties of dry storage systems for commercial spent nuclear fuel (SNF) in response to a shift towards the storage of high-burnup (HBU) fuel (> 45 gigawatt days per metric ton of uranium, or GWd/MTU). This shift raises concerns regarding cladding integrity, which faces increased risk at the higher temperatures within spent fuel assemblies present within HBU fuel compared to low-burnup fuel (≤ 45 GWd/MTU). A dry cask simulator (DCS) was built at Sandia National Laboratories (SNL) in Albuquerque, New Mexico to produce validation-quality data that can be used to test the accuracy of the modeling used to predict cladding temperatures. These temperatures are critical to evaluating cladding integrity throughout the storage cycle of commercial spent nuclear fuel. A model validation exercise was previously carried out for the DCS in a vertical configuration. Lessons learned during the previous validation exercise have been applied to a new, blind study using a horizontal dry cask simulator (HDCS). Three modeling institutions – the Nuclear Regulatory Commission (NRC), Pacific Northwest National Laboratory (PNNL), and Empresa Nacional del Uranio, S.A., S.M.E. (ENUSA) – were granted access to the input parameters from the DCS Handbook, SAND2017-13058R, and results from a limited data set from the horizontal BWR dry cask simulator tests reported in the HDCS update report, SAND2019-11688R. With this information, each institution was tasked to calculate peak cladding temperatures and air mass flow rates for ten HDCS test cases. Axial as well as vertical and horizontal transverse temperature profiles were also calculated. These calculations were done using modeling codes (ANSYS/Fluent, STAR-CCM+, or COBRA-SFS), each with their own unique combination of modeling assumptions and boundary conditions. For this validation study, the ten test cases of the horizontal dry cask simulator were defined by three independent variables – fuel assembly decay heat (0.5 kW, 1 kW, 2.5 W, and 5 kW), internal backfill pressure (100 kPa and 800 kPa), and backfill gas (helium and air). The plots provided in Chapter 3 of this report show the axial, vertical, and horizontal temperature profiles obtained from the dry cask simulator experiments in the horizontal configuration and the corresponding models used to describe the thermal-hydraulic behavior of this system. The tables provided in Chapter 3 illustrate the closeness of fit of the model data to the experiment data through root mean square (RMS) calculations of the error in peak cladding temperatures (PCTs), PCT axial locations, axial temperature profiles, vertical and horizontal temperature profiles at two different axial locations, and air mass flow rates for the ten test cases, normalized by the experimental results. The model results are assigned arbitrary model numbers to retain anonymity. Due to the relatively flat axial temperature profiles, small temperature gradients resulted in large deviations of all models’ PCT axial location from the experimental PCT axial location. When the PCT axial location error is excluded in the calculation of the combined RMS of the normalized errors that considers PCT, the temperature profiles, and the air mass flow rates, the model data fits the experimental data to within 5%. When the vault information is excluded, the model data fits the experimental data to within 2.5%. An error analysis was developed further for one model, using the model and experimental uncertainties in each validation parameter to calculate validation uncertainties. The uncertainties for each parameter were used to define quantifiable validation criteria. For this analysis, the model was considered validated for a given comparison metric if the normalized error in that metric divided by the validation uncertainty was less than or equal to 1. When considering the combined RMS of the normalized errors of all metrics divided by their validation uncertainties, the model was found to have satisfied the criterion for model validation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Shape Optimization for Control and Isolation of Structural Vibrations in Aerospace and Defense Applications

Among the main challenges in shape optimization is the coupling of Finite Element Method (FEM) codes in a way that facilitates efficient computation of shape derivatives. This is particularly difficult with multi-physics problems involving legacy codes, where the costs of implementing and maintaining shape derivative capabilities are prohibitive. There are two mathematically equivalent approaches to computing the shape derivative: the volume method, and the boundary method. Each has a major drawback: the boundary method is less accurate, while the volume method is more invasive to the FEM code. Prior implementations of shape derivatives at Sandia have been based on the volume method. We introduce the strip method, which computes shape derivatives on a strip adjacent to the boundary. The strip method makes code coupling simple. Like the boundary method, it queries the state and adjoint solutions at quadrature nodes, but requires no knowledge of the FEM code implementations. At the same time, it exhibits the higher accuracy of the volume method. The development of the strip method also offers us the opportunity to share some lessons learned about implementing the volume method and boundary method, to show shape optimization results on problems of interest, and to begin addressing the other main challenges at hand: constraints on optimized shapes, and their interplay with optimization algorithms.

97 MATHEMATICS AND COMPUTING↗

High operating temperature heat transfer fluids for solar thermal power generation. Final report

This is the final technical report for the DOE MURI project on developing high-operating temperature heat transfer fluids for solar thermal power generation. This project aimed to evaluate liquid metals as a heat-transport fluid and potential energy storage medium for concentrated solar powered (CSP) systems. The project consisted of five phases, starting with fluid selection and screen and ending with potential CSP integration. The initial fluid selection arrived at heavy liquid metals as candidate fluids such as lead bismuth eutectic (LBE) as the prime liquid-alloy candidate to be studied, given the conditions above. Fifty-seven liquid compositions were initially identified with liquidus temperatures lower than 200°C, composed of elements that provide no driving force to the reduction of Cr 2 O 3 or Al 2 O 3 passivation layers in pipe material which is required for corrosion prevention. LBE was identified as the primary candidate fluid after these compositions were compared against computational thermodynamic modeling to screen all of the selected systems that would be compatible with our design objectives. Twenty-eight of these compositions were also investigated with the rapid characterization methods; the accuracies of the liquidus temperature and the specific heats predicted by the computations were better than 3 percent and 9 percent, respectively. We conducted numerus corrosion tests of various Fe-Cr-Al based steels in LBE and its variants at temperate as high as 800°C. It was found that minor additions to the liquid did not provide sufficient corrosion protection to warrant their use in real applications. Furthermore, we investigated the detailed mechanism of corrosion between heavy liquid metal and the pipe material at these very high temperatures. A liquid metal loop was constructed to operate at these high temperatures. The loop construction and operation lead to valuable lessons learned that will be needed for industrial scale loops. Furthermore, we learned that electromagnetic pumps at these extreme temperatures will have to be reengineered and redesigned to be used for CSP applications.

14 SOLAR ENERGY↗

Measuring and Extracting Activity from Time Series Data

This report summarizes the results of an LDRD focused on developing and demonstrating statistically rigorous methods for analyzing and comparing complex activities from remote sensing data. Identifying activity from remote sensing data, particularly those that play out over time and span multiple locations, often requires extensive manual effort because of the variety of features that describe the activity and the required domain expertise. Our results suggest that there are some hidden challenges in extracting and representing activities in sensor data. In particular, we found that the variability in the underlying behaviors can be difficult to overcome statistically, and the report identifies several examples of the issue. We discuss key lessons learned in the context of the project, and finally conclude with recommendations on next steps and future work.

97 MATHEMATICS AND COMPUTING↗

Design for Additive Manufacturing: Exploring Remelt Strategies to Tailor Density and Microstructure

The potential advantages of AM (e.g. weight reduction, novel geometries) are well understood within a systems context. However, adoption of AM at the system level has been slow due to the relative uncertainty in the final material properties, which leaves capabilities and/or performance gains unrealized. Utilizing remelt strategies it may be possible to expand the available process window to provide densities and microstructures beyond what is capable with standard scan strategies. This work explored remelting strategies for 316L stainless steel to tailor grain size and increase density. Twelve scan strategies were explored experimentally and computationally to understand the limitations of remelt strategies and the robustness of the current simulation package. Results show tailoring of grain size, density, and texture is achievable through remelting and several key lessons learned were made to improve the texture evaluation through simulation.

36 MATERIALS SCIENCE↗

Discovering Blind Geothermal Systems in the Great Basin Region: An Integrated Geologic and Geophysical Approach for Establishing Geothermal Play Fairways: All Phases

Most geothermal resources in the Great Basin region of the western USA are blind, and thus the discovery of new commercial-grade systems requires synthesis of favorable characteristics for geothermal activity. The geothermal play fairway concept involves integration of multiple parameters indicative of geothermal activity to identify promising areas for new development. This project integrated multiple datasets to apply the play fairway concept and assess geothermal potential in a large region of the Great Basin in Nevada. It is therefore referred to as the Nevada play fairway project. This project was a strong collaborative effort between several organizations, led by the Nevada Bureau of Mines and Geology at the University of Nevada, Reno, but with key support from the U.S. Geological Survey, ATLAS Geosciences, Inc,, Hi-Q Geophysical, Inc., Lawrence Berkeley National Laboratory, Utah Geological Survey, and Innovative Geothermal Ltd. In Budget Period 1 of this project, available data for nine geologic, geochemical, and geophysical parameters were initially synthesized to produce a new detailed geothermal potential map of 96,000 km2 from west-central to eastern Nevada. These parameters were grouped into subsets and individually weighted to delineate rankings for local permeability, intermediate permeability, regional permeability, and thermal potential, which collectively defined geothermal play fairways (i.e., most likely locations for significant geothermal fluid flow). This initial work was aimed at reducing the risks in regional exploration and therefore facilitating discovery of new commercial-grade systems in blind settings, as well as in areas with surface expressions of geothermal activity. Budget Period 2 of the project involved detailed analysis of some of the most promising areas identified in Phase 1. Twenty-four highly prospective areas, including both known undeveloped systems and previously undiscovered potential blind systems, were identified for further analysis. After reconnaissance of these areas, five of the most promising sites were selected for detailed studies. Multiple techniques were employed in the detailed studies, including geologic mapping, shallow temperature surveys, gravity surveys, Lidar, geochemical studies, seismic reflection analysis, and 3D modeling. The goal of the detailed studies was to identify specific areas with the highest likelihood for high permeability and thermal fluids, such that drill sites could be targeted. Three main sets of predictive maps were generated for each detailed study area: 1) play fairway maps, 2) play fairway error maps, and 3) direct evidence maps. Local- and intermediate-scale permeability models were revised to reflect results of the detailed geologic, geophysical, and geochemical analyses. Budget Period 3 of the project involved more detailed geophysical analyses and temperature-gradient (TG) drilling in southeastern Gabbs Valley and northern Granite Springs Valley, deemed the two most promising sites, with the goal of providing preliminary validation of the play fairway methodology. In southeastern Gabbs Valley, the collocation of a favorable structural setting (displacement transfer zone and fault intersections), Quaternary faults, intersecting and terminating gravity gradients, magnetic low, shallow (2 m) temperature anomaly, low resistivity anomaly, and promising geothermometry from nearby water wells provided evidence for a blind system. Drilling of six TG holes defines an apparent geothermal system at this locality with temperatures as high as 124°C at 152 m. This system is blind, with no surface hot springs, fumaroles, or paleo-geothermal deposits. For northern Granite Springs Valley, a favorable structural setting (termination of a major Quaternary normal fault), terminating gravity gradient, magnetic gradient, newly discovered sinter deposits, nearby warm water wells, previously drilled TG holes in the vicinity, and promising geothermometry suggest a hidden system. Drilling of six new TG holes yields temperatures of ~96°C at ~250 m, suggesting the presence of a geothermal system. Major lessons learned in the course of this project include: 1) initially identified sites commonly include multiple favorable structural settings at a finer scale; 2) promising sites in Cenozoic basins cannot be recognized without detailed geophysical surveys; and 3) play fairway analysis should be refined as the exploration program vectors into the most promising sites and finer-scale data are acquired. In addition to producing copious amounts of data, this project resulted in 16 published papers, 10 abstracts, more than 40 presentations across the U.S. and abroad (including several keynote addresses), 2 Masters theses, and 7 media reports.

15 GEOTHERMAL ENERGY↗

November 2019 Initial Deployment of LiDAR in the H-Canyon Exhaust Tunnel

The H-Canyon Exhaust Tunnel (CAEX) structure is periodically inspected under the Structural Integrity Program using camera equipped crawlers or poles to remotely perform visual inspections. To explore the use of enhanced inspection methods a “Proof of Concept” using the Light Detection and Ranging (LiDAR) technology was performed over a 2-day period in November 2019. The purpose of the “Proof of Concept” deployment was to confirm whether a commercially available LiDAR unit could successfully operate and remotely transmit data from the tunnel CAEX environment and whether the data would provide quantitative information to establish baseline measurements. The LiDAR performance requirement was a measurement accuracy of ± 0.25-inches over a 30-foot distance. This report documents the work activities leading to the deployment, the deployment and processing of data, lessons learned from the deployment and the post data processing methods that will be applied to future deployments.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Lessons in Commercial PACE Leadership: The Path from Legislation to Launch

This resource from the U.S. Department of Energy and Lawrence Berkeley National Laboratory aims to fast track the set-up of commercial property assessed clean energy (C-PACE) programs for state and local governments by capturing the lessons learned from leaders.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

NM Tech Mercury Spill Response

NM Institute of Mining and Technology, NM Tech, reached out to Sandia National Laboratories to perform a causal analysis resulting in lessons learned for a mercury spill on campus earlier in the academic year. That causal analysis meeting was held on October 30, 2018 on the NM Tech campus and this report is a result of interviews and information gathered prior to, during, and after that meeting.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Workspace and Office Design: A Review of the Literature

The Systems Analysis & Decision Support (02150) group completed a review of the research literature on workspace and office design in 2016 for the Asset Management Department (04853). The goal was to characterize results and lessons learned from existing research to understand the effectiveness of current workspaces at Sandia National Laboratories and inform guidance for future workspace design. The study team reviewed 96 documents, published primarily since the year 2000, covering a range of factors associated with workspace design - workspace costs, acoustics, collaboration and privacy, generational preferences, employee health, performance and productivity, organizational retention, and workspace satisfaction. The research literature consistently highlighted the relative deficiencies of open-plan office spaces as compared to traditional private enclosed offices for knowledge workers. While open-plan offices can provide some cost savings, they may not be cost effective in the long term due to future hidden costs incurred by degradations in employee productivity, increased attrition, and increased sickness absences as well as any post-construction modifications needed to resolve emerging workspace issues. The chief deficiencies of open-plan offices include lower levels of employee satisfaction due to reduced visual and auditory privacy, increased interruptions, distractions from irrelevant background speech, less physical space, and more ambient noise. The drawbacks reported in the literature tend to outweigh any benefits associated with potential facilitation of coworker interactions and collaboration. Key suggestions identified in the literature to guide and optimize workspace and office design are provided.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

Planning Considerations for Energy Storage in Resilience Applications. Outcomes from the NELHA Energy Storage Conference's Policy and Regulatory Workshop

This report presents the proceedings and lessons learned at a conference workshop that discussed the role of energy storage in supporting electric system resilience, which took place at the Natural Energy Laboratory of Hawaii Authority’s (NELHA) Conference on Energy Storage Trends and Opportunities in December 2018. Staff from the Pacific Northwest National Laboratory (PNNL) made two presentations on the topic of resilience: the first covering a conceptual framework for incorporating resilience into resource planning processes, and the second covering a tool developed for microgrid planning that can assist in identifying resource mixes that will meet site-specific resilience needs. Throughout the presentations, presenters and workshop participants discussed the obstacles to improving electric system resilience and potential solutions for overcoming them. Following the workshop, the authors conducted additional research to further contextualize the topics discussed at the workshop and to frame the resulting recommendations for future engagement on this subject by the Department of Energy and the national laboratories.

25 ENERGY STORAGE↗

Integrated Mid-Continent Stacked Carbon Storage Hub Project Phase II (Final Summary Report)

The Phase II Integrated Midcontinent Stacked Carbon Storage Hub (IMSCS-HUB) is part of the Carbon Storage Assurance Facility Enterprise (CarbonSAFE) established by the United States Department of Energy (DOE) National Energy Technology Laboratory (NETL). CarbonSAFE is phased to support the development of commercial-scale (50 million metric tonnes [Mt] over a 30-year period) carbon capture, utilization, and storage (CCUS) in the United States. The IMSCS-HUB study area comprises carbon dioxide (CO 2 ) sources in Iowa, Kansas, and Nebraska (the source corridor), and CO 2 sinks in Kansas and Nebraska (the storage corridor), representing the first large-scale project for the Midcontinent region. The stacked storage corridor is characterized by alternating sequences of deep saline formations, oil-bearing reservoirs, shale, and evaporite units that are conducive to vertically stacked CO 2 injection for geologic storage and enhanced oil recovery (EOR). Three sites within the IMSCS-HUB stacked storage corridor were evaluated in Phase II for commercial CCUS feasibility: one in southwest-central Nebraska, Sleepy Hollow Field (SHF), a second in southwestern Nebraska near Madrid (Madrid), and a third in southwestern Kansas, the Patterson Site (composed of the Patterson, Heinitz, Hartland, and Oslo fields). In Phase II, the team assessed the feasibility of storage complexes at the potential storage sites in Nebraska and Kansas to support a commercial-scale storage hub that integrates proven CO 2 capture technology and transport from nearby ethanol sources. Building on lessons learned from the DOE-NETL Regional Carbon Sequestration Partnerships (RCSPs), the Project Team has identified a clear strategy to meet DOE’s 2025 objective of commercial carbon capture and storage (CCS) implementation by developing a CO 2 market and infrastructure that relies on multiple ethanol-based CO 2 sources in the short term and the incorporation of multiple coal-fired power plant CO 2 sources when commercial capture is economically viable. The team also leveraged the updated 45Q tax credit to develop capture and transport infrastructure. Commercial-scale CCUS is feasible at two candidate storage sites studied, the Madrid, Nebraska Site and the Patterson Site in Kearny County, Kansas. The Sleepy Hollow Field in Nebraska was found to be an attractive candidate for stacked storage with CO 2 -EOR (Battelle 2020e). Outreach efforts facilitated engagement from industry, government, and research sectors (Battelle and GPI, 2020) and an outreach plan for future phases of the project was developed to address issues that are of concern in the IMSCS-HUB project area (Battelle, 2020f). All components of a CCUS project were determined to be feasible in the IMSCS-HUB region and Risk Mitigation Plan was developed and includes strategies to mitigate risks associated with each project component (Battelle, 2020j). A roadmap was developed to obtain the required UIC permits for an integrated CCUS project (Battelle, 2020k). The regional storage resource characterization demonstrated significant opportunity for commercial-scale projects in the IMSCS-HUB storage corridor with 577.4 Mt of stacked CO 2 storage capacity and the potential to produce 181.9 MMbbls of oil via EOR across 17 individual storage areas (Battelle and ARI, 2020). The pipeline assessment study found viable pipeline routes that connected 45Q-eligible ethanol plants, coal fired power plants, and other sources in the IMSCS-HUB corridor. The comprehensive results of subsurface characterization, modeling efforts, outreach assessment, and regulatory analysis from were integrated to develop a Detailed Commercial Development Plan for the IMSCS-HUB (Battelle, 2020n). Commercialization efforts will involve obtaining Class VI UIC permits, establishing and finalizing the pipeline route, and evaluating capture projects at participating CO 2 sources. Phases I and II of the IMSCS-HUB CarbonSAFE provide a strong foundation for safely, efficiently, and cost-effectively characterizing and permitting commercial-scale project sites in the region. The plan for implementation of commercial-scale CCUS projects in the IMSCS-HUB is aligned with the objectives of CarbonSAFE Phase III: Site Characterization and CO 2 Capture Assessment.

20 FOSSIL-FUELED POWER PLANTS↗

Carbon Fiber Prepreg Recycling- Automated Perform Manufacturing Equipment (Final Technical Report)

Discontinuous fiber composites have a compelling business case as related to light metals such as aluminum and magnesium machined or die cast components. DFC’s have been in commercial production using carbon fiber/epoxy prepreg for both commercial aircraft and for military applications for a number of years and their usage is expanding into automotive and consumer goods components. Reasons for this include significantly lower cost as compared to continuous fiber composites easier design and understanding of the material by metal traditionalists, higher degree of part complexity with relatively simple and low cost molds when compared to high-pressure die casting, and potential for near zero waste. IACMI’s 10-year goals of reduction in carbon fiber reinforced plastics manufacturing cost by 25%, reduction in their embodied energy by 50%, and recyclability of 95% can all be advanced through robust recycling. With recycling We have shown that a 15% contribution in manufacturing cost reduction is feasible, that a significant reduction in embodied energy (over 90% for the recycled fraction) is achievable, and that when combined with primary pyrolysis recycling, the 95% target can be met. Large-scale application of advanced composites began with the aerospace industry, and CRTC’s location in Washington State provided access to a waste stream of nearly 900 tonnes/year that was going to landfill. As the aerospace industry has automated parts production, their material forms have become significantly easier to recycle, and some evidence of this exists for the future automotive and wind turbine components as well. CRTC decided to focus on re-purposing the carbon fiber/epoxy aerospace scrap streams through materials reformatting and reuse, and not on primary recycling (pyrolysis mainly) as this technology is commercially available. The main reasons for this were that it offers a route to effective use of the most widely available and consistent feedstock called edge-trim, as well as allows creation of complex and low-cost parts using rapid and cost-effective compression molding technologies. The reasons also include leading the way for potential automotive pre-preg recycling as the combination of roughly 85% virgin pre-preg and 15% recycled pre-preg directly supports IACMI’s goals and enables significant part cost reduction and a path to zero-waste composite manufacturing at the OEMs or Tier 1’s. The purpose of the project was to develop equipment and technology to transform continuous fiber pre-preg in roll forms into smaller chip-format DFC feedstock, and to determine impacts on moldability and performance based on lessons learned along the path. The availability of scrap from pre-preg manufacturers was a significant value to the program even though the aerospace pre-preg is designed to be autoclave molded thus has handling, tackiness, and processing factors that are not ideal for DFCs. The scope of the project was to develop a Phase 1 system that could identify and resolve some of the major hurdles, determine where to focus effort on building a commercial-scale Phase 2 system, and develop technology for handling a wide variety of incoming scrap materials to produce the most usable product. A chopping system was developed and reduced to practice via an experimental approach that enabled all forms of scrap coming from the pre-preg manufacturers and some forms of the scrap coming from OEM production lines to be very effectively re-purposed. The systems that were developed were not considered to be production robust but rather identified and resolved some of the major technical hurdles, and demonstrated the path towards effective full-scale commercialization.

36 MATERIALS SCIENCE↗

Monitoring, Reporting, and Verification (MRV) Plan - Meeting EPA Guidelines for GHGRP and Subpart RR

The Midwest Regional Carbon Sequestration Partnership (MRCSP) was founded in 2003 as part of the U.S. Department of Energy’s (DOE’s) Regional Carbon Sequestration Partnership initiative. Since its founding, MRCSP has made significant strides toward making CCUS a viable option for states in the region. The public/private consortium, funded through the DOE Regional Carbon Sequestration Initiative, brings together nearly 40 industry partners and 10 states. Battelle, as the project lead, oversees research, development and operations and coordinates activities among the partners. The incremental, phased approach has built a valuable knowledge base for the industry and paved the way for commercial-scale adoption of CCUS technologies. From 2008 to 2020, MRCSP Phase III focused on the development of large-scale injection projects. This report is part of a series of reports prepared under the Midwestern Regional Carbon Sequestration Partnership (MRCSP) Phase III (Development Phase). These reports summarize and detail the findings of the work conducted under the Phase III project. This report summarizes the steps for successfully submitting a Monitoring, Reporting and Verification (MRV) plan to the U.S. Environmental Protection Agency (EPA). This work used the lessons learned from various MRCSP tasks to demonstrate the geologic understanding of the reefs in Northern Niagaran Pinnacle Reef Trend (NNPRT), successful monitoring and accounting methodologies, understanding of potential risks and leakage pathways, and mass balance of CO2 baseline and net storage. The plan encompasses ten reefs and provides a reporting plan for future reef development.

01 COAL, LIGNITE, AND PEAT↗