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At least 163 records · Page 9

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NASA NTRS1981

Fatigue behavior of graphite-epoxy laminates at elevated temperatures

An examination and analysis is presented of the elevated temperature fatigue behavior of multidirectional graphite-epoxy laminates in terms of single lamina behavior. The laminate strength is predicted by considering the cyclic stress field in each lamina, the interlaminar stresses, and the experimentally determined temperature-effect 'shifting factors'. The initial failure of a lamina in a laminate is examined first in terms of stress redistribution, and then in terms of total failure and final laminate fracture; these analytical results are then compared with the actual fatigue behavior of T300/5208 graphite-epoxy composite laminates. In view of the agreement obtained, it is concluded that the temperature 'shifting factors' introduced here enable one to predict long-term behavior at a given temperature from short-time testing at elevated temperatures.

Rotem, A.↗

NASA NTRS2013

Unit-Sphere Multiaxial Stochastic-Strength Model Applied to Anisotropic and Composite Materials

Models that predict the failure probability of brittle materials under multiaxial loading have been developed by authors such as Batdorf, Evans, and Matsuo. These "unit-sphere" models assume that the strength-controlling flaws are randomly oriented, noninteracting planar microcracks of specified geometry but of variable size. This methodology has been extended to predict the multiaxial strength response of transversely isotropic brittle materials, including polymer matrix composites (PMCs), by considering (1) flaw-orientation anisotropy, whereby a preexisting microcrack has a higher likelihood of being oriented in one direction over another direction, and (2) critical strength, or K (sub Ic) orientation anisotropy, whereby the level of critical strength or fracture toughness for mode I crack propagation, K (sub Ic), changes with regard to the orientation of the microstructure. In this report, results from finite element analysis of a fiber-reinforced-matrix unit cell were used with the unit-sphere model to predict the biaxial strength response of a unidirectional PMC previously reported from the World-Wide Failure Exercise. Results for nuclear-grade graphite materials under biaxial loading are also shown for comparison. This effort was successful in predicting the multiaxial strength response for the chosen problems. Findings regarding stress-state interactions and failure modes also are provided.

Nemeth, Noel, N.↗

NASA NTRS1976

A study to improve the mechanical properties of silicon carbide ribbon fibers

Preliminary deposition studies of SiC ribbon on a carbon ribbon substrate showed that the dominant strength limiting flaws were at the substrate surface. Procedures for making the carbon ribbon substrate from polyimide film were improved, providing lengths up to 450 meters (1,500 ft.) of flat carbon ribbon substrate 1,900 microns (75 mils) wide by 25 microns (1 mil) thick. The flaws on the carbon ribbon were smaller and less frequent than on carbon ribbon used earlier. SiC ribbon made using the improved substrate, including a layer of pyrolytic graphite to reduce further the severity of substrate surface flaws, showed strength levels up to the 2,068 MPa (300 Ksi) target of the program, with average strength levels over 1,700 MPa (250 Ksi) with coefficient of variation as low as 10% for some runs.

Debolt, H. E.↗

NASA NTRS2005

Graphite Nanoreinforcements for Aerospace Nanocomposites

New advances in the reinforcement of polymer matrix composite materials are critical for advancement of the aerospace industry. Reinforcements are required to have good mechanical and thermal properties, large aspect ratio, excellent adhesion to the matrix, and cost effectiveness. To fulfill the requirements, nanocomposites in which the matrix is filled with nanoscopic reinforcing phases having dimensions typically in the range of 1nm to 100 nm show considerably higher strength and modulus with far lower reinforcement content than their conventional counterparts. Graphite is a layered material whose layers have dimensions in the nanometer range and are held together by weak Van der Waals forces. Once these layers are exfoliated and dispersed in a polymer matrix as nano platelets, they have large aspect ratios. Graphite has an elastic modulus that is equal to the stiffest carbon fiber and 10-15 times that of other inorganic reinforcements, and it is also electrically and thermally conductive. If the appropriate surface treatment can be found for graphite, its exfoliation and dispersion in a polymer matrix will result in a composite with excellent mechanical properties, superior thermal stability, and very good electrical and thermal properties at very low reinforcement loadings.

Drzal, Lawrence T.↗

NASA NTRS1975

Carbide coated fibers in graphite-aluminum composites

The NASA-supported program at the Los Alamos Scientific Laboratory (LASL) to develop carbon fiber-aluminum matrix composites is described. Chemical vapor deposition (CVD) was used to uniformly deposit thin, smooth, continuous coats of TiC on the fibers of graphite tows. Wet chemical coating of fibers, followed by high-temperature treatment, was also used, but showed little promise as an alternative coating method. Strength measurements on CVD coated fiber tows showed that thin carbide coats can add to fiber strength. The ability of aluminum alloys to wet TiC was successfully demonstrated using TiC-coated graphite surfaces. Pressure-infiltration of TiC- and ZrC-coated fiber tows with aluminum alloys was only partially successful. Experiments were performed to evaluate the effectiveness of carbide coats on carbon as barriers to prevent reaction between alluminum alloys and carbon. Initial results indicate that composites of aluminum and carbide-coated graphite are stable for long periods of time at temperatures near the alloy solidus.

Imprescia, R. J.↗

NASA NTRS1968

Metal carbide-graphite composites

Carbon sources effects on niobium carbides, and determination of high temperature flexural strength, flexural creep, and thermal expansion up to 2550 deg C for various materials

Source record↗

NASA NTRS1982

A thermoplastic polyimidesulfone

A polymer system has been prepared which has the excellent thermoplastic properties generally associated with polysulfones, and the solvent resistance and thermal stability of aromatic polyimides. This material, with improved processability over the base polyimide, can be processed in the 260-325 C range in such a manner as to yield high quality, tough unfilled moldings; strong, high-temperature-resistant adhesive bonds; and well consolidated, graphite-fiber-reinforced moldings (composities). The unfilled moldings have physical properties that are similar to aromatic polysulfones which demonstrates the potential as an engineering thermoplastic. The adhesive bonds exhibit excellent retention of initial strength levels even after thermal aging for 5000 hours at 232 C. The graphite-fiber-reinforced moldings have mechanical properties which makes this polymer attractive for the fabrication of structural composites.

St.clair, T. L.↗

NASA NTRS1984

A thermoplastic polyimidesulfone

A polymer system has been prepared which has the excellent thermoplastic properties generally associated with polysulfones, and the solvent resistance and thermal stability of aromatic polyimides. This material, with improved processability over the base polyimide, can be processed in the 260-325 C range in such a manner as to yield high quality, tough unfilled moldings; strong, high-temperature-resistant adhesive bonds; and well consolidated, graphite-fiber-reinforced moldings (composites). The unfilled moldings have physical properties that are similar to aromatic polysulfones which demonstrates the potential as an engineering thermoplastic. The adhesive bonds exhibit excellent retention of initial strength levels even after thermal aging for 5000 hours at 232 C. The graphite-fiber-reinforced moldings have mechanical properties which makes this polymer attractive for the fabrication of structural composites.

St. Clair, T. L.↗

NASA NTRS1979

Effects of moisture on torsion and flexure properties of graphite-epoxy composites

The effects of moisture and temperature on unidirectional and multi-ply laminates of T300/934 and AS/3501 graphite-epoxy systems were investigated. Properties studied were static flexure strength, and flexure and torsion fatigue strengths at room temperature and at 74 C. Specimens with increased moisture content showed a reduced static flexure strength; water as the test environment had only a negligible influence. In flexure fatigue and torsion fatigue, the water environment caused somewhat reduced fatigue strengths at room temperature and significantly greater degradation in 74 C water. The failure mode in all cases was interlaminar delamination.

Sumsion, H. T.↗

NASA NTRS1982

Failure characteristics of graphite-epoxy structural components loaded in compression

Failure characteristics of compressively loaded graphite-epoxy components are described. Experimental results for both strength-critical laminates and structural components with postbuckling strength are presented. Effects of low speed impact damage and circular holes on compressive strength are discussed. Delamination and shear crippling failure mechanisms that limit the performance of strength-critical laminates are described. Transverse shear and skin-stiffener separation failure mechanisms that limit the performance of components with postbuckling strength are also described. The influence of matrix properties on compressive strength improvements for impact damaged laminates is discussed. Experimental data and results from a failure analysis for strength-critical laminates with cutouts are discussed and compared with impact damage results. Typical postbuckling test results are compared with analytical predictions.

Starnes, J. H., Jr.↗

NASA NTRS1983

Failure characteristics of graphite-epoxy structural components loaded in compression

Starnes, J. H., Jr.↗

NASA NTRS1984

Impact properties of rubber-modified epoxy resin-graphite-fiber composites

To improve the impact resistance of graphite-fiber composites, a commercial and an experimental epoxy resin were modified with liquid reactive rubber and a brominated epoxy resin. The commercial epoxy was a tetrafunctional resin, and the experimental epoxy was a trifunctional resin. The reactive rubber was a carboxyl-terminated butadiene-acrylonitrile copolymer. The rubber content was varied from 0 to 25 percent (wt). The brominated epoxy resin was used at Br levels of 4, 19, and 35 percent of the resin. Composites were prepared with woven graphite cloth reinforcement. The composites were evaluated by using flexural strength in the dry state and an elevated temperature after saturation with water. The impact properties were determined by measuring shear strength after falling-ball impact and instrumented impact. The rubber-modified, trifunctional resin exhibited better properties, when tested in hot-wet conditions in a heated oven at 366 K (after boiling the material for 2 h in demineralized water), than the tetrafunctional resin. Improved impact resistance was observed with the addition of the reactive rubber to the epoxy resin. Further improvement was observed with the addition of the brominated epoxy resin.

Gilwee, W. J.↗

NASA NTRS1986

Specimen geometry effects on graphite/PMR-15 composites during thermo-oxidative aging

Studies were conducted to establish the effects of specimen geometry on the thermo-oxidative stability and the mechanical properties retention of unidirectional Celion 12000 graphite fiber reinforced PMR-15 polyimide composites. Weight loss, flexural strength and interlaminar shear strength are measured at isothermal aging times as long as 1639 hr at a temperature of 316 C for three different specimen geometries. It is found that the three different types of specimen surfaces exhibit different values of weight loss/unit area. The mechanical properties retention is also found to be dependent on geometry for these composites. The interlaminar shear strength decreases significantly over the complete range of aging times. The flexural strength retention starts showing geometric dependency after about 1000 hr of aging at 316C. Weight loss fluxes, associated with the three different types of exposed surfaces, are calculated and used to develop an empirical mathematical model for predicting the weight loss behavior of unidirectional composites of arbitrary geometries. Data are presented comparing experimentally determined weight loss with weight loss values predicted using the empirical model.

Bowles, K. J.↗

NASA NTRS1987

Bearing-bypass loading on bolted composite joints

The effects of simultaneous bearing and bypass loading on a graphite-epoxy (T300/5208) laminate were investigated. Onset damage and ultimate strengths were determined for each test case. A finite element stress analysis was conducted for each test case. The computed local stresses were used with appropriate failure criteria to analyze the observed failure modes and strengths. An unexpected interaction of the effect of the bypass and bearing loads was found for the onset of compression reacted bearing damage. The interaction was caused by a decrease in the bolt-hole contact arc and a corresponding increase in the severity of the bearing loads. The amount of bolt-hole contact had a significant effect on local stresses and, thus, on the calculated damage-onset and ultimate strengths. An offset-compression failure mode was identified for laminate failure under compression bearing-bypass loading.

Crews, J. H., Jr.↗

NASA NTRS1986

Specimen geometry effects on graphite/PMR-15 composites during thermo-oxidative aging

Studies were conducted to establish the effects of specimen geometry on the thermo-oxidative stability and the mechanical properties retention of unidirectional Celion 12000 graphite fiber reinforced PMR-15 polyimide composites. Weight loss, flexural strength and interlaminar shear strength are measured at isothermal aging times as long as 1639 hr at a temperature of 316 C for three different specimen geometries. It is found that the three different types of specimen surfaces exhibit different values of weight loss/unit area. The mechanical properties retention is also found to be dependent on geometry for these composites. The interlaminar shear strength decreases significantly over the complete range of aging times. The flexural strength retention starts showing geometric dependency after about 1000 hr of aging at 316 C. Weight loss fluxes, associated with the three different types of exposed surfaces, are calculated and used to develop an empirical mathematical model for predicting the weight loss behavior of unidirectional composites of arbitrary geometries. Data are presented comparing experimentally determined weight loss with weight loss values predicted using the empirical model.

Bowles, K. J.↗

NASA NTRS1993

Buckling analysis of laminated thin shells in a hot environment

Results are presented of parametric studies to assess the effects of various parameters on the buckling behavior of angle-ply, laminated thin shells in a hot environment. These results were obtained by using a three-dimensional finite element analysis. An angle-ply, laminated thin shell with fiber orientation of (theta/-theta)(sub 2) was subjected to compressive mechanical loads. The laminated thin shell had a cylindrical geometry. The laminate contained T300 graphite fibers embedded in an intermediate-modulus, high-strength (IMHS) matrix. The fiber volume fraction was 55 percent and the moisture content was 2 percent. The residual stresses induced into the laminate structure during the curing were taken into account. Parametric studies were performed to examine the effect on the critical buckling load of the following parameters: cylinder length and thickness, internal hydrostatic pressure, different ply thicknesses, different temperature profiles through the thickness of the structure, and different lay up configurations and fiber volume fractions. In conjunction with these parameters the ply orientation was varied from 0 deg to 90 deg. Seven ply angles were examined: 0 deg, 15 deg, 30 deg, 45 deg, 60 deg, 75 deg, and 90 deg. The results show that the ply angle theta and the laminate thickness had significant effects on the critical buckling load. The fiber volume fraction, the fiber orientations, and the internal hydrostatic pressure had important effects on the critical buckling load. The cylinder length had a moderate influence on the buckling load. The thin shell with (theta/-theta)(sub 2) or (theta/-theta)(sub s) angle-ply laminate had better buckling-load performance than the thin shell with (theta)(sub 4) angle-ply laminate. The temperature profiles through the laminate thickness and various laminates with the different ply thicknesses has insignificant effects on the buckling behavior of the thin shells.

Gotsis, Pascal K.↗

NASA NTRS1994

Laminated Thin Shell Structures Subjected to Free Vibration in a Hygrothermal Environment

Parametric studies were performed to assess the effects of various parameters on the free-vibration behavior (natural frequencies) of (+/- theta)(sub 2) angle-ply, fiber composite, thin shell structures in a hygrothermal environment. Knowledge of the natural frequencies of structures is important in considering their response to various kinds of excitation, especially when structures and force systems are complex and when excitations are not periodic. The three dimensional, finite element structural analysis computer code CSTEM was used in the Cray YMP computer environment. The fiber composite shell was assumed to be cylindrical and made from T300 graphite fibers embedded in an intermediate-modulus, high-strength matrix. The following parameters were investigated: the length and the laminate thickness of the shell, the fiber orientation, the fiber volume fraction, the temperature profile through the thickness of the laminate, and laminates with different ply thicknesses. The results indicate that the fiber orientation and the length of the laminated shell had significant effects on the natural frequencies. The fiber volume fraction, the laminate thickness, and the temperature profile through the shell thickness had weak effects on the natural frequencies. Finally, the laminates with different ply thicknesses had an insignificant influence on the behavior of the vibrated laminated shell. Also, a single through-the-thickness, eight-node, three dimensional composite finite element analysis appears to be sufficient for investigating the free-vibration behavior of thin, composite, angle-ply shell structures.

Gotsis, Pascal K.↗

NASA NTRS1995

Free Vibration of Fiber Composite Thin Shells in a Hot Environment

Results are presented of parametric studies to assess the effects of various parameters on the free vibration behavior (natural frequencies) of (plus or minus theta)2, angle-ply fiber composite thin shells in a hot environment. These results were obtained by using a three-dimensional finite element structural analysis computer code. The fiber composite shell is assumed to be cylindrical and made from T-300 graphite fibers embedded in an intermediate-modulus high-strength matrix (IMHS). The residual stresses induced into the laminated structure during curing are taken into account. The following parameters are investigated: the length and the thickness of the shell, the fiber orientations, the fiber volume fraction, the temperature profile through the thickness of the laminate and the different ply thicknesses. Results obtained indicate that: the fiber orientations and the length of the laminated shell had significant effect on the natural frequencies. The fiber volume fraction, the laminate thickness and the temperature profile through the shell thickness had a weak effect on the natural frequencies. Finally, the laminates with different ply thicknesses had insignificant influence on the behavior of the vibrated laminated shell.

Gotsis, Pascal K.↗