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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS1976

Large Diameter Shuttle Launched-AEM (LDSL-AEM) study

A technical description of a Large Diameter Shuttle Launched-AEM (LDSL-AEM), an AEM base module adapted to carry 5 ft diameter payloads in the shuttle with propulsion for carrying payloads to higher altitude orbits from a 150 NM shuttle orbit, is described. The AEM is designed for launch on the scout launch vehicle. Onboard equipment provides capability to despin, acquire the earth, and control the vehicle in an earth pointing mode using reaction wheels for torque with magnets for all attitude acquisition, wheel desaturation, and nutation damping. Earth sensors in the wheels provide pitch and roll attitude. This system provides autonomous control capability to 1 degree in pitch and roll and 2 degrees in yaw. The attitude can be determined to .5 degrees in pitch and roll and 2 degrees in yaw.

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NASA NTRS1993

Preliminary AEM study of the microstructure and composition of metal particles in ordinary chondrites

The purpose of this study is to examine the microstructure and composition of the metal particles in ordinary chondrites using analytical electron microscopy (AEM) techniques. Since the phases produced within the metal particles are very fine, the application of various AEM techniques for structural and chemical characterization is critical. However, thin specimen preparation for AEM study has proven very difficult because of the matrix silicate which is present. This is the first AEM study of the metal particles in chondrites. A type 6 chondrite, Saint Severin (LL6), was selected for examination because the metal phases have been reheated into the single phase taenite region (greater than 700 C), and cooled slowly to lower temperatures. A combination of electron optical instruments was employed including a field emission gun (FEG) JEOL 840F high resolution scanning electron microscope (HRSEM), a JEOL 6300F FEG-HRSEM, a Philips 400T AEM, and a JEOL 733 electron probe microanalyzer (EPMA).

Yang, C. W.↗
NASA NTRS1974

Applications Explorer Missions (AEM): Mission planners handbook

The Applications Explorer Missions (AEM) Program is a planned series of space applications missions whose purpose is to perform various tasks that require a low cost, quick reaction, small spacecraft in a dedicated orbit. The Heat Capacity Mapping Mission (HCMM) is the first mission of this series. The spacecraft described in this document was conceived to support a variety of applications instruments and the HCMM instrument in particular. The maximum use of commonality has been achieved. That is, all of the subsystems employed are taken directly or modified from other programs such as IUE, IMP, RAE, and Nimbus. The result is a small versatile spacecraft. The purpose of this document, the AEM Mission Planners Handbook (AEM/MPH) is to describe the spacecraft and its capabilities in general and the HCMM in particular. This document will also serve as a guide for potential users as to the capabilities of the AEM spacecraft and its achievable orbits. It should enable each potential user to determine the suitability of the AEM concept to his mission.

Smith, S. R.↗
DOE OSTI2023

LTE-P-22 Alkaline Stability of AEMs

A procedure for ex-situ evaluation of chemical (alkaline) stability of anion exchange membranes (AEM). The IEC and ionic conductivity of an AEM is measured before and after being heated (typically at 80C in 1 M KOH) for ~1000 hours.

AEM↗
DOE OSTI2025

Reinforced AEM Separators Based on Triblock Copolymers for Electrode-decoupled RFBs

Washington University in St. Louis (WUSTL), in collaboration with The University of Texas at San Antonio (UTSA) and Giner Inc. developed highly selective anion exchange membranes (AEMs) and a novel electrode-decoupled redox flow battery (RFB) for grid scale energy storage as part of the ARPA-E IONICS program (with connections to the DAYS program in the later part of the project). RFBs exhibit the crucial characteristic of system-level decoupled scaling of energy and power which makes them cost effective for the multi-GWh scales envisioned for grid-scale energy storage solutions. This has led to extensive (and deserved) research interest and attention. This project aimed to enhance the design space available for redox-flow batteries (RFBs) by enabling the long-term separation of disparate cationic (elemental) actives using a highly selective membrane separator, while concurrently permitting the transport of anions to balance charge. The approach proposed was to design and develop a highly selective anion-exchange membrane (AEM), which would in turn permit the design and development of electrode-decoupled RFBs. Pairs of (different element) cationic species with redox reactions exhibiting a large difference in their standard electrode potentials were identified to develop high voltage, high power RFBs while disrupting the existing paradigm of using a single element which can ionize to more than two soluble oxidation states (e.g.: Vanadium).

25 ENERGY STORAGE↗
DOE OSTI2025

Uncovering Structure–Conductivity Relationships in Anion Exchange Membranes (AEMs) Using Interpretable Machine Learning

Anion exchange membranes (AEMs) play a vital role in the performance of water electrolyzers and fuel cells, yet their discovery and optimization remain challenging due to the complexity of structure–property relationships. In this study, we introduce a machine learning framework that leverages conditional graph neural networks (cGNNs) and descriptor-based models and a hybrid graph neural network (HGARE) to predict and interpret ionic conductivity. The descriptor-based pipeline employs principal component analysis (PCA), ablation, and SHAP analysis to identify factors governing anion conductivity, revealing electronic, topological, and compositional descriptors as key contributors. Beyond prediction, dimensionality reduction and clustering are performed by employing t-SNE and KMeans as well as SOM, which reveal distinct membranes clusters, some of which were enriched with high anion conductivity. Among graph-based approaches, the graph convolutional (GCN) achieved strong predictive performance, while the Hybrid Graph Autoencoder-Regressor Ensemble (HGARE) achieved the highest accuracy. Additionally, atom-level saliency maps from GCN provide spatial explanations for conductive behavior, revealing the importance of polarizable and flexible regions. This work contributes to the accelerated and data-driven design of high-performance AEMs.

Naghshnejad, Pegah [Department of Chemical Enginee↗
DOE OSTI2025

Enhancing water and oxygen transport through electrode engineering for AEM water electrolyzers

Anion-exchange membrane water electrolyzers (AEMWEs) can accelerate the deployment of more efficient and affordable hydrogen production solutions. Here, electrode structure is shown to affect water back-diffusion and oxygen transport, which, in return, governs overpotential behaviors in AEMWEs. Measurements indicate that electrode with copious catalytic sites produces water close to the AEM, creating a higher water gradient and driving water back-diffusion, which improves membrane hydration and mass transport. In situ measurement reveals a high pH gradient near the anode surface, which affects anode kinetics. Operando measurement shows reduced oxygen accumulation when decoupling oxygen production and transport on anode. Catalyst ink rheology and stability are tuned with additives to realize scalable fabrication of electrodes with enhanced transport features, allowing AEMWE to operate at 2 A cm−2 for over 1,000+ h at a 2.3 μV h−1 degradation rate. Analysis during and post-durability provides insights into degradation mechanisms. This work demonstrates an electrode design strategy for efficient and durable AEMWEs.

AEM↗
DOE OSTI2023

LTE-P-7 IEC AEM SOP

A procedure for measuring the ion exchange capacity (IEC) of an anion exchange membrane (AEM). This is done via a titration method (automated or manual).

08 HYDROGEN↗
DOE OSTI2023

LTE-P-6 AEM Conductivity

A procedure for measuring the hydroxide conductivity of an anion exchange membrane (AEM). A four-electrode In-plane conductivity is measured as a function of relative humidity (RH).

08 HYDROGEN↗
NASA NTRS1977

AEMS implementation cost study for Boeing 727

Costs for airline operational implementation of a NASA-developed approach energy management system (AEMS) concept, as applied to the 727 airplane, were determined. Estimated costs are provided for airplane retrofit and for installation of the required DME ground stations. Operational costs and fuel cost savings are presented in a cost-of-ownership study. The potential return on the equipment investment is evaluated using a net present value method. Scheduled 727 traffic and existing VASI, ILS, and collocated DME ground station facilities are summarized for domestic airports used by 727 operators.

Allison, R. L.↗
NASA NTRS1977

Heat capacity mapping radiometer for AEM spacecraft

The operation, maintenance, and integration of the applications explorer mission heat capacity mapping radiometer is illustrated in block diagrams and detail schematics of circuit functions. Data format and logic timing diagrams are included along with radiometric and electronic calibration data. Mechanical and electrical configuration is presented to provide interface details for integration of the HCMR instrument to AEM spacecraft.

Sonnek, G. E.↗
DOE OSTI2024

High-Performance AEM LTE with Advanced Membranes, Ionomers and PGM-Free Electrodes

Alkaline low temperature electrolysis (LTE) systems enjoy several potential advantages over acid-based LTE systems including facile oxygen evolution reaction (OER) kinetics and electrodes that can use little to no platinum group metals (PGM). The polymer membranes and membrane electrode assembly (MEA) structures going into alkaline electrochemical systems have seen significant advances in recent years. The objective of this project is to combine state-of-the-art alkaline polymer electrolyzer components into one optimized membrane electrode assembly (MEA) system to achieve DOE low temperature electrolysis (LTE) goals. The benefit of individual component advances cannot be fully appreciated until all aspects and components of the MEA are working at an equally high level of performance. New electrode fabrication methods were developed where solvent cast catalyst/ionomer solutions were used in place of insoluble ionomers to significantly improve adhesion. The membranes were improved in terms of durability and mechanical properties. The OER and HER catalysts were improved and made more durable.

08 HYDROGEN↗
DOE OSTI2026

Novel PtNi single-atom–nanocluster (SA–NC) ensembles promote Tafel kinetics and ampere-class AEM hydrogen evolution

The development of efficient, durable, and low-PGM electrocatalysts for the hydrogen evolution reaction (HER) in alkaline media is critical for next-generation electrolysis technologies. We report a facile two-step synthesis of highly dispersed PtNi and PtNi-nitride nanoclusters (NCs) (~2.3 nm) with ultralow Pt content (0.5 at.%) anchored on N-doped Vulcan carbon. Structural and compositional characterization via XAS, XPS, HAADF-STEM, HRTEM, and EDS mapping established key structure–activity relationships across varying Pt/Ni ratios and pyrolysis temperatures. The Pt0.5Ni0.5/C-750 catalyst, an ensemble of PtNi M-N-C type single-atom (SA) moieties with neighboring PtNi nanoclusters (NC), exhibited superior HER performance in alkaline media, achieving overpotentials of 30, 115, and 210 mV at 10, 100, and 500 mA cm−2, respectively. Despite at a lower Pt content, this novel SA–NC ensemble outperformed commercial Pt/C by ~36%. A standardized literature comparison with contemporary Pt- and Ru-doped analogues reveals the as-prepared Pt0.5Ni0.5/C-750 to sit at the apex of Tafel-limited kinetics and low overpotential at 100 mA cm−2. Tafel-limited Tafel slopes in both alkaline and acidic regimes confirm favorable proton recombination kinetics. Mass activities at 200 mV reached 13.8 and 18.84 A mgPt−1 in alkaline and acidic media, respectively. However, excessive nitridation (e.g., at 650 °C) adversely altered Pt electronic structure and HER kinetics. While Ni enhanced alkaline HER, acidic HER favored Ni-free analogues. Pt0.5Ni0.5/C-750 also demonstrated robust temperature responsiveness and 300-h operational stability at high current densities (0.5–1.0 A cm−2) in MEA tests. This work presents a scalable strategy for designing thermally responsive, durable, and compositionally tunable NC catalysts with neighboring SA moieties for alkaline electrolysis.

AEMWE↗
NASA NTRS1977

Analytic investigation of the AEM-A/HCMM attitude control system performance

The Heat Capacity Mapping Mission (HCMM), scheduled for launch in 1978, will be three-axis stabilized relative to the earth in a 600-kilometer altitude, polar orbit. The autonomous attitude control system consists of three torquing coils and a momentum wheel driven in response to error signals computed from data received from an infrared horizon sensor and a magnetometer. This paper presents a simple model of the attitude dynamics and derives the equations that determine the stability of the system during both attitude acquisition (acquisition-mode) and mission operations (mission-mode). Modifications to the proposed mission-mode control laws which speed the system's response to transient attitude errors and reduce the steady-state attitude errors are suggested. Numerical simulations are performed to validate the results obtained with the simple model.

Lerner, G. M.↗
NASA NTRS1979

SAGE ground truth plan: Correlative measurements for the Stratospheric Aerosol and Gas Experiment (SAGE) on the AEM-B satellite

The ground truth plan is outlined for correlative measurements to validate the Stratospheric Aerosol and Gas Experiment (SAGE) sensor data. SAGE will fly aboard the Applications Explorer Mission-B satellite scheduled for launch in early 1979 and measure stratospheric vertical profiles of aerosol, ozone, nitrogen dioxide, and molecular extinction between 79 N and 79 S. latitude. The plan gives details of the location and times for the simultaneous satellite/correlative measurements for the nominal launch time, the rationale and choice of the correlative sensors, their characteristics and expected accuracies, and the conversion of their data to extinction profiles. In addition, an overview of the SAGE expected instrument performance and data inversion results are presented. Various atmospheric models representative of stratospheric aerosols and ozone are used in the SAGE and correlative sensor analyses.

Russell, P. B.↗
NASA NTRS1982

AEM of extraterrestrial materials

Modifications to and maintenance of the JEOL 100 CX electron microscope are discussed. Research activity involving extraterrestrial matter, cosmic dust, stratosphere dust, and meteorites is summarized.

Mackinnon, I. D. R.↗
NASA NTRS1998

Animal Enclosure Module (AEM)

The primary objective of this research project is to test the hypothesis that corticosteroids contribute to the adverse skeletal effects of space flight. To achieve this objective, serum corticosteroids, which are known to increase during space flight, must be maintained at normal physiologic levels in flight rats by a combination of adrenalectomy and corticosteroid supplementation via implanted hormone pellets. Bone analyses in these animals will then be compared to those of intact flight rats that, based on past experience, will undergo corticosteroid excess and bone loss during space flight. The results will reveal whether maintaining serum corticosteroids at physiologic levels in flight rats affects the skeletal abnormalities that normally develop during space flight. A positive response to this question would indicate that the bone loss and decreased bone formation associated with space flight are mediated, at least in part, by corticosteroid excess.

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