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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS2011

Vibration Considerations for Cryogenic Tanks Using Glass Bubbles Insulation

The use of glass bubbles as an efficient and practical thermal insulation system has been previously demonstrated in cryogenic storage tanks. One such example is a spherical, vacuum-jacketed liquid hydrogen vessel of 218,000 liter capacity where the boiloff rate has been reduced by approximately 50 percent. Further applications may include non-stationary tanks such as mobile tankers and tanks with extreme duty cycles or exposed to significant vibration environments. Space rocket launch events and mobile tanker life cycles represent two harsh cases of mechanical vibration exposure. A number of bulk fill insulation materials including glass bubbles, perlite powders, and aerogel granules were tested for vibration effects and mechanical behavior using a custom design holding fixture subjected to random vibration on an Electrodynamic Shaker. The settling effects for mixtures of insulation materials were also investigated. The vibration test results and granular particle analysis are presented with considerations and implications for future cryogenic tank applications. A thermal performance update on field demonstration testing of a 218,000 L liquid hydrogen storage tank, retrofitted with glass bubbles, is presented. KEYWORDS: Glass bubble, perlite, aerogel, insulation, liquid hydrogen, storage tank, mobile tanker, vibration.

Werlink, Rudolph J.↗
NASA NTRS2010

Glass Bubbles Insulation for Liquid Hydrogen Storage Tanks

A full-scale field application of glass bubbles insulation has been demonstrated in a 218,000 L liquid hydrogen storage tank. This work is the evolution of extensive materials testing, laboratory scale testing, and system studies leading to the use of glass bubbles insulation as a cost efficient and high performance alternative in cryogenic storage tanks of any size. The tank utilized is part of a rocket propulsion test complex at the NASA Stennis Space Center and is a 1960's vintage spherical double wall tank with an evacuated annulus. The original perlite that was removed from the annulus was in pristine condition and showed no signs of deterioration or compaction. Test results show a significant reduction in liquid hydrogen boiloff when compared to recent baseline data prior to removal of the perlite insulation. The data also validates the previous laboratory scale testing (1000 L) and full-scale numerical modeling (3,200,000 L) of boiloff in spherical cryogenic storage tanks. The performance of the tank will continue to be monitored during operation of the tank over the coming years.

Glass bubble↗
NASA NTRS2017

Research and Development History of Glass Bubbles Bulk-Fill Thermal Insulation Systems for Large-Scale Cryogenic Liquid Hydrogen Storage Tanks

Based on the published literature record, this document provides an overview of the research and development of glass bubbles bulk-fill thermal insulation systems for cryogenic equipment in general and, in particular, for large-scale cryogenic liquid hydrogen (LH2) storage spheres. Glass bubbles (also known as hollow glass microspheres) are used in place of perlite powder which began use in double-wall cryogenic tanks in the 1930s. Included in this overview is a historical summary, a development timeline, a selected publications list, and the key technical points from those publications.

Cryogenic storage tanks↗
NASA NTRS1968

Reducing bubbles in glass coatings improves electrical breakdown strength

Helium reduces bubbles in glass coatings of accelerator grids for ion thrustors. Fusing the coating in a helium atmosphere creates helium bubbles in the glass. In an argon atmosphere, entrapped helium diffuses out of the glass and the bubbles collapse. The resultant coating has a substantially enhanced electrical breakdown strength.

Banks, B.↗
NASA NTRS1984

Dissolving Bubbles in Glass

Analytical expression used to calculate time it takes for stationary bubbles of oxygen and carbon dioxide to dissolve from glass melt. Technique based on analytical expression for bubble radius as function time, with consequences of surface tension included.

Weinberg, M. C.↗
NASA NTRSDate not supplied

Energy Efficient Large-Scale Storage of Liquid Hydrogen

World’s largest LH2storage tanks constructed in mid-1960s at NASA/KSC. These vacuum-perlite insulated tanks, still in service today, are 3,200 m3capacity (ea.). In 2018, construction began on an additional 4,700 m3LH2storage tank at LC-39B•NASA’s new Space Launch System (SLS) heavy lift rocket for Artemis program holds 2,033 m3of LH2in its 8.4-m diameter by 40-m height. Two new energy-efficient technologies are included: glass bubbles insulation system and an Integrated Refrigeration and Storage (IRAS) heat exchanger for passive + active thermal control:•Evacuated glass bubbles insulation system has been shown to reduce LH2boiloff by 46% versus perlite in field demonstrations. Controlled storage via IRAS, when fully implemented, will provide full control of ullage pressure, zero boiloff, and even production of densified LH22CEC-2021

cryogenics↗
NASA NTRSDate not supplied

Energy Efficient Large-Scale Storage of Liquid Hydrogen

The world’s largest liquid hydrogen storage tanks were constructed in the mid-1960sat the NASA Kennedy Space Center. These two vacuum-jacketed, perlite powder insulated tanks, still in service today, have 3,200 m3 of useable capacity. In 2018, construction began on an additional storage tank at Launch Complex 39B. This new tank will give an additional storage capacity of 4,700 m3 for a total on-site storage capacity of roughly 8,000 m3. NASA’s new Space Launch System (SLS) heavy lift rocket for the Artemis program includes an LH2tank that makes up the bulk of the vehicle, holding 2,033 m3 of LH2 in its 8.4-m diameter by40-m height. The new storage tank includes two new energy-efficient technologies: a glass bubbles insulation system in lieu of perlite, and an Integrated Refrigeration and Storage (IRAS)heat exchanger for controlled storage capability. The evacuated glass bubbles insulation system is based on the prior two decades of research to prove the thermal performance benefits as well as the mechanical and vacuum integrity; and has been shown to reduce LH2 boiloff by 46%versus perlite in field demonstrations. The IRAS capability is centered on a heat exchanger system that is built within the inner vessel to reject heat from the bulk liquid through the future implementation of an external helium refrigerator. Controlled storage via IRAS, when fully implemented, will provide full control of the ullage pressure, zero boiloff, and even production of densified LH2 pending its adoption on future launch vehicles. The design basics are described along with main construction and testing processes involved. The key features of the new technology items and implications on simplified operations and long-term energy savings are addressed

cryogenics↗
NASA NTRS2006

Microspheres in Plasma Display Panels

Filling small bubbles of molten glass with gases is just as difficult as it sounds, but the technical staff at NASA is not known to shy away from a difficult task. When Microsphere Systems, Inc. (MSI), of Ypsilanti, Michigan, and Imaging Systems Technology, Inc. (IST), of Toledo, Ohio, were trying to push the limits of plasma displays but were having difficulty with the designs, NASA s Glenn Garrett Morgan Commercialization Initiative (GMCI) assembled key personnel at Glenn Research Center and Ohio State University for a brainstorming session to come up with a solution for the companies. They needed a system that could produce hollow, glass micro-sized spheres (microspheres) that could be filled with a variety of gasses. But the extremely high temperature required to force the micro-sized glass bubbles to form at the tip of a metal nozzle resulted in severe discoloration of the microspheres. After countless experiments on various glass-metal combinations, they had turned to the GMCI for help. NASA experts in advanced metals, ceramics, and glass concluded that a new design approach was necessary. The team determined that what was needed was a phosphate glass composition that would remain transparent, and they went to work on a solution. Six weeks later, using the design tips from the NASA team, Tim Henderson, president of MSI, had designed a new system in which all surfaces in contact with the molten glass would be ceramic instead of metal. Meanwhile, IST was able to complete a Phase I Small Business Innovation Research (SBIR) grant supported by the National Science Foundation (NSF) and supply a potential customer with samples of the microspheres for evaluation as filler materials for high-performance insulations.

Source record↗
NASA NTRSDate not supplied

Vacuum Pump-Down of the Annular Insulation Space for Large Field-Erected Liquid Hydrogen Storage Tanks

Insulation systems are critical to liquid hydrogen storage tank performance. Tanks in the capacity range of 100 to 1,000 m 3 are typically shop built and designed with high-vacuum (HV) multi-layer insulation (MLI), whereas storage vessels larger than 1,000 m 3 are typically field-erected and supplied with bulk fill insulation working at moderate vacuum (MV) levels (1-100 millitorr). For large, field-erected vessels, two types of bulk fill insulation typically used: perlite and hollow glass microspheres (glass bubbles). Selection of either material is driven by a tradeoff between CAPEX and OPEX, such as the material and construction cost versus operating thermal performance and maintenance. In either case, the vacuum level needed to achieve optimum performance is likely to drive the field testing and commissioning portion of the construction schedule. A primary goal of this paper is to present practical experience and data for warm vacuum pressure (WVP) and cold vacuum pressure (CVP) levels. Recommended WVP levels needed prior to cooldown consider both perlite powder and glass bubbles. Pumping time expected to achieve target vacuum levels, considering a variety of factors, is also discussed. Recommendations for a standard practice in vacuum-insulated tank commissioning are based on historical NASA data, and those collected during recent projects.

A M Swanger↗
NASA NTRS1981

Driving bubbles out of glass

Surface tension gradient in melt forces gas bubbles to surface, increasing glass strength and transparency. Conventional chemical and buoyant fining are extremely slow in viscous glasses, but tension gradient method moves 250 um bubbles as rapidly as 30 um/s. Heat required for high temperature part of melt is furnished by stationary electrical or natural-gas heater; induction and laser heating are also possible. Method has many applications in industry processes.

Mattox, D. M.↗
NASA NTRS2006

Microsphere Insulation Panels

Microsphere insulation panels (MIPs) have been developed as lightweight, longlasting replacements for the foam and vacuum-jacketed systems heretofore used for thermally insulating cryogenic vessels and transfer ducts. The microsphere core material of a typical MIP consists of hollow glass bubbles, which have a combination of advantageous mechanical, chemical, and thermal-insulation properties heretofore available only separately in different materials. In particular, a core filling of glass microspheres has high crush strength and low density, is noncombustible, and performs well in soft vacuum.

Mohling, R.↗
NASA NTRS2006

Optical and Mechanical Properties of Glass Blown In Vacuo

Theoretically, the strength of glass processed in vacuum should be higher due to outgassing of contaminants normally present in the glass, such as bulk water in the form of OH bonds that tends to weaken the glass structure. In this research, small discs of a few types of glass have been subjected to various temperatures for extended periods of time in vacuum. Their strength was then tested using a standard flexure technique, facilitated by a custom-designed test fixture, and the results were compared to glass tested in air using the same fixture. The purpose of the glass blowing investigation was to prove the basic feasibility of a high-level concept for in-space manufacture of optical elements. The central requirement was that the glass bubble had to be blown into a support structure such that the bubble could be handled by manipulation of the structure. The blown bubble attached itself to a mullite ring geometrically and mechanically, as a demonstration in the initial experiments described here, by expanding through and around it. The vacuum system used was custom made, as were most of the components of the system, such as the heating element, the glass and ring support structure, and the gas inlet system that provided the pressure needed to blow the glass.

Manning, andrew↗
NASA NTRS1989

Aligning Plasma-Arc Welding Oscillations

Tool aids in alignment of oscillator probe on variable-polarity plasma-arc welding torch. Probe magnetically pulls arc from side to side as it moves along joint. Tensile strength of joint depends on alignment of weld bead and on alignment of probe. Operator installs new tool on front of torch body, levels it with built-in bubble glass, inserts probe in slot on tool, and locks probe in place. Procedure faster and easier and resulting alignment more accurate and repeatable.

Norris, Jeff↗
NASA NTRS2007

Numerical Modeling of Propellant Boiloff in Cryogenic Storage Tank

This Technical Memorandum (TM) describes the thermal modeling effort undertaken at Marshall Space Flight Center to support the Cryogenic Test Laboratory at Kennedy Space Center (KSC) for a study of insulation materials for cryogenic tanks in order to reduce propellant boiloff during long-term storage. The Generalized Fluid System Simulation program has been used to model boiloff in 1,000-L demonstration tanks built for testing the thermal performance of glass bubbles and perlite insulation. Numerical predictions of boiloff rate and ullage temperature have been compared with the measured data from the testing of demonstration tanks. A satisfactory comparison between measured and predicted data has been observed for both liquid nitrogen and hydrogen tests. Based on the experience gained with the modeling of the demonstration tanks, a numerical model of the liquid hydrogen storage tank at launch complex 39 at KSC was built. The predicted boiloff rate of hydrogen has been found to be in good agreement with observed field data. This TM describes three different models that have been developed during this period of study (March 2005 to June 2006), comparisons with test data, and results of parametric studies.

Majumdar, A. K.↗
NASA NTRS2007

Cost-Efficient Storage of Cryogens

NASA's cryogenic infrastructure that supports launch vehicle operations and propulsion testing is reaching an age where major refurbishment will soon be required. Key elements of this infrastructure are the large double-walled cryogenic storage tanks used for both space vehicle launch operations and rocket propulsion testing at the various NASA field centers. Perlite powder has historically been the insulation material of choice for these large storage tank applications. New bulk-fill insulation materials, including glass bubbles and aerogel beads, have been shown to provide improved thermal and mechanical performance. A research testing program was conducted to investigate the thermal performance benefits as well as to identify operational considerations and associated risks associated with the application of these new materials in large cryogenic storage tanks. The program was divided into three main areas: material testing (thermal conductivity and physical characterization), tank demonstration testing (liquid nitrogen and liquid hydrogen), and system studies (thermal modeling, economic analysis, and insulation changeout). The results of this research work show that more energy-efficient insulation solutions are possible for large-scale cryogenic storage tanks worldwide and summarize the operational requirements that should be considered for these applications.

Fesmire, J. E.↗
NASA NTRS2007

Cryogenic Thermal Performance Testing of Bulk-Fill and Aerogel Insulation Materials

The research testing and demonstration of new bulk-fill materials for cryogenic thermal insulation systems was performed by the Cryogenics Test Laboratory at NASA Kennedy Space Center. Thermal conductivity testing under actual-use cryogenic conditions is a key to understanding the total system performance encompassing engineering, economics, and materials factors. A number of bulk fill insulation materials, including aerogel beads, glass bubbles, and perlite powder, were tested using a new cylindrical cryostat. Boundary temperatures for the liquid nitrogen boil-off method were 293 K and 78 K. Tests were performed as a function of cold vacuum pressure from high vacuum to no vacuum conditions. Results are compared with other complementary test methods in the range of 300 K to 20 K. Various testing techniques are shown to be required to obtain a complete understanding of the operating performance of a material and to provide data for answers to design engineering questions.

Scholtens, B. E.↗
NASA NTRS2019

Advanced Cryogenic Insulation Systems

New materials in recent decades have enabled advances in thermal insulation systems for storage and transfer of cryogens. To preserve the cold and achieve efficient cryogenic systems, a combination of materials, testing, and engineering is required. The total heat leak into any cryogenic assembly is comprised of three main parts: 1) heat leak through the insulation, 2) heat leak through the support structures, and 3) heat leak attributed to piping penetrations and feedthroughs (and their negative effects on the insulation). This "cold triangle" approach provides a basis for evaluating performance benefits of new materials and analyzing the cost effectiveness in overall system design. Provided are thermophysical data for aerogels, aerogel composites, novel multilayered composites, and glass bubbles for standard test conditions of 293 K and 78 K under conditions from high vacuum to ambient pressure. Examples of cryogenic storage tanks show the relative importance of both insulation and structural materials for achieving designs of highest energy efficiency.

Multilayer Insulation↗