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NASA NTRSDate not supplied

Improved Method for Increased-Rate Stitched Composites Manufacturing

Stitched composites, as defined herein, are created by stitching a dry preform, infusing the preform with resin and curing the resin. Stitched composites have been shown to have benefits over unstitched composites for stiffened structures, including improved damage tolerance, reduced weight, and fewer fasteners. However, conventional stitched composite structure production is very time and manual-labor intensive, and therefore is not conducive for high-rate production of commercial aircraft main structure. The National Aeronautics and Space Administration (NASA) Hi-Rate Composite Aircraft Manufacturing (HiCAM) Project has the objective to increase the manufacturing rate for future composite aircraft. Stitched resin infused (SRI) composites are one of the technologies being considered under the HiCAM Project, but to be viable, production rates must be increased (i.e., production time reduced). Previous work has shown that it is possible to reduce the time required to stitch a dry composite preform, such as a skin with integral stiffeners, but the stitching process is a small portion of the total time required to produce a stitched preform. To significantly reduce overall stitched preform production time, a study was undertaken to examine a new stitching method that would yield time reduction in the pre- and post-stitching activities that include all portions of a stitched preform production with the exception of the actual stitching process. The new method resulted in significant reduction in production time, from 27% to 40%, while at the same time reducing the costs associated with fabricating a stitched preform by eliminating stations within the production line, simplifying tooling, reducing labor, and reducing consumables.

Stitching↗

NASA NTRSDate not supplied

Improved Method for Increased-Rate Stitched Composites Manufacturing

Stitching↗

NASA NTRS2005

Life in the fast lane for protein crystallization and X-ray crystallography

The common goal for structural genomic centers and consortiums is to decipher as quickly as possible the three-dimensional structures for a multitude of recombinant proteins derived from known genomic sequences. Since X-ray crystallography is the foremost method to acquire atomic resolution for macromolecules, the limiting step is obtaining protein crystals that can be useful of structure determination. High-throughput methods have been developed in recent years to clone, express, purify, crystallize and determine the three-dimensional structure of a protein gene product rapidly using automated devices, commercialized kits and consolidated protocols. However, the average number of protein structures obtained for most structural genomic groups has been very low compared to the total number of proteins purified. As more entire genomic sequences are obtained for different organisms from the three kingdoms of life, only the proteins that can be crystallized and whose structures can be obtained easily are studied. Consequently, an astonishing number of genomic proteins remain unexamined. In the era of high-throughput processes, traditional methods in molecular biology, protein chemistry and crystallization are eclipsed by automation and pipeline practices. The necessity for high-rate production of protein crystals and structures has prevented the usage of more intellectual strategies and creative approaches in experimental executions. Fundamental principles and personal experiences in protein chemistry and crystallization are minimally exploited only to obtain "low-hanging fruit" protein structures. We review the practical aspects of today's high-throughput manipulations and discuss the challenges in fast pace protein crystallization and tools for crystallography. Structural genomic pipelines can be improved with information gained from low-throughput tactics that may help us reach the higher-bearing fruits. Examples of recent developments in this area are reported from the efforts of the Southeast Collaboratory for Structural Genomics (SECSG).

Review↗

NASA NTRS2026

Fatigue Life of Flow-Formed Aluminum 2195 and 6061 Alloys

The successful design and fabrication of metallic cryotanks for commercial aviation applications require lightweight, durable materials capable of withstanding high pressures and cryogenic temperatures through tens of thousands of thermomechanical refueling cycles. Flow forming is an advanced manufacturing technique that offers high-rate production and scalability for fabricating integrally stiffened cylinders suitable for cryotank applications. This work establishes the durability of flow-formed aluminum alloys by characterizing their fatigue life performance under conditions that mimic cryotank refueling cycles. Residual stresses in flow-formed aluminum-lithium (Al-Li) 2195-T6 cylinders were assessed using the contour method and found to be minimal. Fatigue life testing was conducted on flow-formed Al-Li 2195-T6 at room temperature and cryogenic temperatures (-321°F [-196°C]), with wrought Al-Li 2195-T6 serving as a baseline for comparison. Results showed that flow-formed materials exhibited fatigue performance comparable to or better than wrought materials, with no statistically significant differences observed between different specimen orientations relative to processing directions. Fractography revealed reduced delaminations in the flow-formed Al-Li 2195 samples as compared to wrought, indicating potential improvement to the microstructure that could result in improved service properties. Texture analysis using electron backscattered diffraction (EBSD) indicated recrystallization during heat treatment, potentially contributing to reduced delamination susceptibility. These findings demonstrating flow-formed material durability coupled with the high manufacturing efficiency of flow forming, makes flow forming an attractive process to produce aircraft cryotanks.

EBF3↗

NASA NTRS1991

Applications of diamond films and related materials; Proceedings of the 1st International Conference, Auburn, AL, Aug. 17-22, 1991

The present conference discusses the nucleation and growth of diamond from hydrocarbons, the cutting tool performance of CVD thick-film diamond, the characterization of CVD diamond grinding powder, industrial applications of crystalline diamond-coated tools, standardized SEM tribometry of diamond-coated substrates, residual stress in CVD diamond films, the optical properties of CVD diamond films, polycrystalline diamond films for optical applications, and diamond growth on ferrous metals. Also discussed are ion beam-irradiation smoothing of diamond films, electronic circuits on diamond substrates, diamond-laminated surfaces for evaporative spray cooling, electron devices based on the unique properties of diamond, diamond cold cathodes, thin-film diamond microstructure applications, Schottky diodes from flame-grown diamond, diamond films for thermionic applications, methods of diamond nucleation and selective deposition, high-rate/large-area diamond film production, halogen-assisted diamond growth, the economics of diamond technology, and the optical and mechanical properties of diamondlike films.

Tzeng, Yonhua↗

NASA NTRS2018

Use of Open Networks and Delay-Tolerant Protocol to Decrease WAN Latency of EOS near Real-Time Data

Since 1999, NASA's Earth Observing System Data Operations System (EDOS) project at Goddard Space Flight Center (GSFC) has provided high-rate data capture, level zero processing, and product distribution services for a majority of NASA's EOS (Earth Observing System) high-rate missions, including Terra, Aqua, Aura, ICESat, EO-1, SMAP, and OCO-2. EDOS high-rate science and engineering (150-300 Mbps) data-driven capture systems are deployed at 7 worldwide ground stations which are connected via both private (closed) and public (open) wide area networks (WANs) to the centralized EDOS Level Zero Processing Facility (LZPF) located at GSFC, where the data is processed and Level 0 products are distributed to users worldwide. All data transferred over the open networks to GSFC traverse an IPSec tunnel, providing the same level of security as a VPN connection. EDOS produces both time-based and near real-time products (session-based). Near real-time data products are produced from a single ground station contact; time-based products are produced from multiple ground station contacts. EDOS is the primary supplier of EOS Level 0 data to the NASA near real-time user community known as the Land, Atmosphere Near real-time Capability for EOS (LANCE). For the past few years, EDOS has streamlined its systems to reduce WAN latency for near real-time data delivery, including implementing Quality of Service (QoS), expanding closed network bandwidth, adding open network connections with more bandwidth, and implementing a delay-tolerant protocol to mitigate long round-trip times to remote ground stations.

Delay-Tolerant Protocol↗

NASA NTRS1998

LITE data processing

The Lidar In-space Technology Experiment (LITE) was a payload onboard the Space Shuttle Discovery as part of the September 1994 STS-64 mission. LITE successfully made both atmospheric and surface measurements at the 355 nm, 532 nm, and 1064 nm wavelengths [Winker et al., 1996]. At mission completion, nearly 45 Gbytes of data had been obtained. As the data were collected they were organized into three data sets. The largest of these data sets contained the single-shot full resolution digitized lidar signals for all three wavelengths. The other two data sets contained the instrument status data block (ISDB) and the quick look science data (QLSD). ISDB information was generated once per second and contained timing parameters and engineering data related to the health, status, and configuration of the instrument. The QLSD are 100shot averages of the 355 nm and 532 nm lidar signals and were generated at ten second intervals. As the LITE data were generated, they were output to low-rate and high-rate telemetry streams. The low-rate data contained the ISDB and QLSD. The lowrate data were transmitted to the ground by the Shuttle S-band system through the Tracking and Data Relay Satellite System (TDRSS). The high-rate data contained the full resolution digitized lidar signals for all three wavelengths, the ISDB, and QLSD. The high-rate data were transmitted in real time by the Ku-band system through TDRSS downlink to the LITE operations center at the Johnson Space Center (JSC). High-rate data were only obtained when the orbiter and TDRSS telemetry link coincided with the real-time operations of LITE. The low-rate data were backed up by a Shuttle recorder during periods when the telemetry link was unavailable, and the entire lowrate data stream was transferred to the ground over the course of the mission. A total of 53 hours of lowrate data and 45.5 hours of high-rate data were acquired. All of the LITE raw telemetry data have been archived at the NASA Langley Research Center (LaRC), and the LITE high-rate data have been processed to the level 1 data product. This paper describes the data processing steps required to convert the LITE raw, high-rate telemetry data to the LITE level 1 data product.

Powell, Kathleen A.↗

NASA NTRS2021

Atoms to Aircraft to Spacecraft

The next generation of aerospace systems requires materials and structures that combine high performance at high utilization in short missions with the possibility of high rate production, without excessive non-recurring cost, to allow for rate flexibility and shorter structural life cycles. The development of materials and structures that offer this flexibility in rate without negatively influencing performance and economic viability will require a matching and overlapping experimental and computational design approach. The objective is to go from Atom to Airframe to Spaceframe for thermoplastic unidirectional tape based fastener-free assemblies. Thermoplastic composites are chosen as the focus because these materials allow for reversible fusion bonding in every stage of their life cycle after synthesis. Our strategy is to combine multi-scale computational approaches with multi-scale experimental activities to develop an understanding of and capabilities to manufacture custom unidirectional thermoplastic tape. This tape will be the basis for our high-rate multiple-technology manufacturing approach validated by the production of two representative demonstrators for urban air mobility vehicle structures. The multi-disciplinary team will work in an integrated manner to effectively combine computational approaches with experimental approaches at each stage of characteristic manufacturing flows. The team aims for tools and technology to quantify the thermo-rheological aspects of unidirectional tape-based production and assembly of aerospace quality thermoplastic components as well as for validated tools for unidirectional tape-based thermoplastic preform and part design and manufacture. The work will be used to design and build two demonstration structural parts characteristic for urban air mobility vehicles.

Paul Ziehl↗

NASA NTRS2019

EDOS Initiatives to Decrease Latency of NRT Data for LANCE

NASA's EOS Data and Operations System (EDOS) is the primary supplier of NRT (near real-time) data to the NASA NRT user community known as the Land, Atmosphere NRT Capability for EOS (LANCE). EDOS provides NRT data for various instruments on the EOS missions Terra, Aqua, Aura, as well as for the NOAA missions Suomi NPP and NOAA-20. This poster describes an overview of the EDOS multi-mission system with emphasis on the NRT products distributed for LANCE elements: AIRS, MISR, MLS, MODIS, MOPITT, OMPS, OMI and VIIRS. Remote EDOS high-rate data capture systems are deployed at NASA ground stations which provide data-driven capture of high-rate science for EOS missions. The remote EDOS components transfer the science data via high-rate WANs to the centralized EDOS Level-zero processing systems located at Goddard Space Flight Center. EDOS produces session-based data sets especially for LANCE NRT use from a single ground station contact; this data is sent to dual LANCE destinations as part of the standard redundancy requirement for LANCE elements. EDOS has implemented various latency improvements with the ultimate goal to have EDOS processing of NRT data keep up with the spacecraft data downlink. EDOS enhancements have included implementation of priority-based QoS, expanded network architecture to include open networks, and use of a delay-tolerant protocol. EDOS has streamlined its systems and infrastructure to minimize latency for NRT data delivery for LANCE. EDOS begins to transfer the NRT data to the LANCE elements within minutes of the end of the contact session with an average packet latency from instrument observation to Level 0 product delivery to each LANCE element of just over one hour.

Michael, Karen↗

NASA NTRS2001

CDDIS Support of IGS LEO Activities

The Crustal Dynamics Data Information System (CDDIS) has served as a global data center for the International GPS Service (IGS) since its start in June 1992, providing on-line access to data from over 175 sites on a daily and hourly basis. This paper will present an overview about the current status of the CDDIS GPS data and products archive with a look to the future support of LEO (Low Earth Orbiting missions), including the archive of high-rate data and on-board GPS receiver data.

Noll, Carey E.↗

NASA NTRS1995

The trellis complexity of convolutional codes

It has long been known that convolutional codes have a natural, regular trellis structure that facilitates the implementation of Viterbi's algorithm. It has gradually become apparent that linear block codes also have a natural, though not in general a regular, 'minimal' trellis structure, which allows them to be decoded with a Viterbi-like algorithm. In both cases, the complexity of the Viterbi decoding algorithm can be accurately estimated by the number of trellis edges per encoded bit. It would, therefore, appear that we are in a good position to make a fair comparison of the Viterbi decoding complexity of block and convolutional codes. Unfortunately, however, this comparison is somewhat muddled by the fact that some convolutional codes, the punctured convolutional codes, are known to have trellis representations that are significantly less complex than the conventional trellis. In other words, the conventional trellis representation for a convolutional code may not be the minimal trellis representation. Thus, ironically, at present we seem to know more about the minimal trellis representation for block than for convolutional codes. In this article, we provide a remedy, by developing a theory of minimal trellises for convolutional codes. (A similar theory has recently been given by Sidorenko and Zyablov). This allows us to make a direct performance-complexity comparison for block and convolutional codes. A by-product of our work is an algorithm for choosing, from among all generator matrices for a given convolutional code, what we call a trellis-minimal generator matrix, from which the minimal trellis for the code can be directly constructed. Another by-product is that, in the new theory, punctured convolutional codes no longer appear as a special class, but simply as high-rate convolutional codes whose trellis complexity is unexpectedly small.

Mceliece, R. J.↗

NASA NTRSDate not supplied

Impact of Thermoplastic Composites: Testing and Modeling

Thermoplastic Composites (TPCs) are being increasingly considered for aerospace applications given their faster manufacturing cycles and lower cost. The NASA High-Rate Composite Aircraft Manufacturing (HiCAM) project aims to evaluate and mature thermoplastic manufacturing technologies to achieve a 4X – 6X increase in the production rate of Next Generation Single Aisle (NGSA) commercial aircraft. Within the purview of the NASA HiCAM project, this work investigates the response of thermoplastic composites under High Energy Dynamic Impact (HEDI) conditions. HEDI tests were conducted on panels fabricated with a carbon fiber reinforced low melt semi-crystalline resin TC1225 LMPAEK T700G (T700/LMPAEK) material system. A blunt metal projectile was chosen as the impactor which impacted the T700/LMPAEK panels over a range of impact velocities imparted by a gas gun test setup. As expected, lower velocity impacts caused the projectile to rebound, whereas higher velocity impacts resulted in the projectile penetrating the test panels. For the test cases in which the projectile rebounded, the predominant damage modes recorded with Ultrasonic (UT) scans included interlaminar delaminations which exhibited a “rotating fan” like structure when viewed in the through-thickness direction. Additionally, the dynamic deflection of the center point of the back face of the test panels and the velocity of the projectile was also measured during the test. Finite element models were developed to model a test case in which the projectile rebounded. These models were developed using LS-DYNA® wherein the primary objective was to evaluate the ability of the material model MAT299 to capture the dynamic response and damage modes in the T700/LMPAEK test panels. MAT299 is a Deformation Gradient Decomposition (DGD) based Continuum Damage Mechanics (CDM) material model. The interlaminar delaminations were modeled using the cohesive contact formulation available within LS-DYNA, wherein the mixed-mode fracture is captured via the Benzegaggh-Kenane (B-K) mode-dependent fracture energy interpolation law. The above-mentioned modeling methods have mostly been applied to thermoset composites and adapting them to TPCs involves addressing challenges associated with appropriately representing material behavior. Therefore, the proposed paper would discuss the systematic approach taken to adapt thermoset composites modeling practices for applications to TPCs, while appropriately addressing material behavior. The proposed paper would show that the predicted back face center point deflection correlated reasonably well with experimental data and the peak deflection was predicted to be within 5% of the experimental measurements. The projectile rebound velocity, while predicted to be higher than the experimental measurement, was within reasonable bounds. Additionally, it will be shown that the predicted delamination shapes were in reasonable agreement with experimental data.

Composite Materials↗

NASA NTRS1976

Contribution of the Spacelab data management system to lower cost space research

This paper reviews the design and operation of the Spacelab data management system as it has evolved. Significant improvements and extensions of the original baseline system have been incorporated and will be discussed. They include the capability for the remote control of Spacelab subsystems, improved remote data acquisition units, a high-rate digital data multiplexer, and an improved high-rate digital recorder. Emphasis will be placed on the overall system aspects, including considerations on the use of minicomputers as an adjunct to the basic Spacelab data system. The approach for experiment related software production and integration will be addressed as well. The paper focuses on the contributions of the data management system in reducing the cost of research in Spacelab.

Burger, J. J.↗

NASA NTRSDate not supplied

A Modern Load Relief Guidance Scheme for Space Launch Vehicles

Launch vehicle load relief algorithms are concerned with realizing a reduction of transient bending moments near maximum dynamic pressure. Traditional approaches to load relief typically use inner-loop acceleration feedback to reduce the wind-induced angle of attack. When implemented in the inner loop, load relief bandwidth is necessarily limited by the achievable stability margins, and when acceleration feedback is employed, by the uncertainty associated with structural modes that couple with the body-mounted accelerometer. The structure of inner loop load relief increases the dimensionality of the flight control gain and filter optimization problem. Most importantly, classical load relief laws do not take advantage of high-rate and high-accuracy GPS-aided inertial velocity data that is readily available from modern strap down IMUs. In this paper, a novel load relief guidance scheme is described that uses direct angle-of-attack feedback in a clever mechanization. The steering commands are determined by examining the wind-perturbed dynamics of a launch vehicle with respect to a gravity turn ascent trajectory. An angle of attack estimate is derived from GPS-aided inertial data and pre-launch range wind measurements, and it is shown that a reduction worst-case rigid-body loads can be realized without requiring air data. The algorithm also includes a high-rate navigation data preprocessing scheme that operates directly on the IMU delta-theta and delta-velocity measurements in order to produce a filtered acceleration estimate at the vehicle center of mass. The outer-loop guidance scheme simplifies the design process for the classical inner-loop autopilot. Algorithm performance is demonstrated using Monte Carlo analysis of a representative liquid booster in a production high fidelity launch vehicle simulation.

NESC↗

NASA NTRS2006

Coherent Detection of High-Rate Optical PPM Signals

A method of coherent detection of high-rate pulse-position modulation (PPM) on a received laser beam has been conceived as a means of reducing the deleterious effects of noise and atmospheric turbulence in free-space optical communication using focal-plane detector array technologies. In comparison with a receiver based on direct detection of the intensity modulation of a PPM signal, a receiver based on the present method of coherent detection performs well at much higher background levels. In principle, the coherent-detection receiver can exhibit quantum-limited performance despite atmospheric turbulence. The key components of such a receiver include standard receiver optics, a laser that serves as a local oscillator, a focal-plane array of photodetectors, and a signal-processing and data-acquisition assembly needed to sample the focal-plane fields and reconstruct the pulsed signal prior to detection. The received PPM-modulated laser beam and the local-oscillator beam are focused onto the photodetector array, where they are mixed in the detection process. The two lasers are of the same or nearly the same frequency. If the two lasers are of different frequencies, then the coherent detection process is characterized as heterodyne and, using traditional heterodyne-detection terminology, the difference between the two laser frequencies is denoted the intermediate frequency (IF). If the two laser beams are of the same frequency and remain aligned in phase, then the coherent detection process is characterized as homodyne (essentially, heterodyne detection at zero IF). As a result of the inherent squaring operation of each photodetector, the output current includes an IF component that contains the signal modulation. The amplitude of the IF component is proportional to the product of the local-oscillator signal amplitude and the PPM signal amplitude. Hence, by using a sufficiently strong local-oscillator signal, one can make the PPM-modulated IF signal strong enough to overcome thermal noise in the receiver circuits: this is what makes it possible to achieve near-quantum-limited detection in the presence of strong background. Following quantum-limited coherent detection, the outputs of the individual photodetectors are automatically aligned in phase by use of one or more adaptive array compensation algorithms [e.g., the least-mean-square (LMS) algorithm]. Then the outputs are combined and the resulting signal is processed to extract the high-rate information, as though the PPM signal were received by a single photodetector. In a continuing series of experiments to test this method (see Fig. 1), the local oscillator has a wavelength of 1,064 nm, and another laser is used as a signal transmitter at a slightly different wavelength to establish an IF of about 6 MHz. There are 16 photodetectors in a 4 4 focal-plane array; the detector outputs are digitized at a sampling rate of 25 MHz, and the signals in digital form are combined by use of the LMS algorithm. Convergence of the adaptive combining algorithm in the presence of simulated atmospheric turbulence for optical PPM signals has already been demonstrated in the laboratory; the combined output is shown in Fig. 2(a), and Fig. 2(b) shows the behavior of the phase of the combining weights as a function of time (or samples). We observe that the phase of the weights has a sawtooth shape due to the continuously changing phase in the down-converted output, which is not exactly at zero frequency. Detailed performance analysis of this coherent free-space optical communication system in the presence of simulated atmospheric turbulence is currently under way.

Vilnrotter, Victor↗

NASA NTRS2002

Architecture Studies Done for High-Rate Duplex Direct Data Distribution (D4) Services

A study was sponsored to investigate a set of end-to-end system concepts for implementing a high-rate duplex direct data distribution (D4) space-to-ground communications link. The NASA Glenn Research Center is investigating these systems (both commercial and Government) as a possible method of providing a D4 communications service between NASA spacecraft in low Earth orbit and the respective principal investigators using or monitoring instruments aboard these spacecraft. Candidate commercial services were assessed regarding their near-term potential to provide a D4 type of service. The candidates included K-band and V-band geostationary orbit and nongeostationary orbit satellite relay services and direct downlink (D3) services. Internet protocol (IP) networking technologies were evaluated to enable the user-directed distribution and delivery of science data. Four realistic, near-future concepts were analyzed: 1) A duplex direct link (uplink plus downlink communication paths) between a low-Earth-orbit spacecraft and a principal-investigator-based autonomous Earth station; 2) A space-based relay using a future K-band nongeosynchronous-orbit system to handle both the uplink and downlink communication paths; 3) A hybrid link using both direct and relay services to achieve full duplex capability; 4) A dual-mode concept consisting of both a duplex direct link and a space relay duplex link operating independently. The concepts were analyzed in terms of contact time between the NASA spacecraft and the communications service and the achievable data throughput. Throughput estimates for the D4 systems were based on the infusion of advanced communications technology products (single and multibeam K-band phased-arrays and digital modems) being developed by Glenn. Cost estimates were also performed using extrapolated information from both terrestrial and current satellite communications providers. The throughput and cost estimates were used to compare the concepts.

Source record↗

NASA NTRS1999

High-Speed TCP Testing

Transmission Control Protocol (TCP) is the underlying protocol used within the Internet for reliable information transfer. As such, there is great interest to have all implementations of TCP efficiently interoperate. This is particularly important for links exhibiting long bandwidth-delay products. The tools exist to perform TCP analysis at low rates and low delays. However, for extremely high-rate and lone-delay links such as 622 Mbps over geosynchronous satellites, new tools and testing techniques are required. This paper describes the tools and techniques used to analyze and debug various TCP implementations over high-speed, long-delay links.

Brooks, David E.↗

NASA NTRS2007

Process for High-Rate Fabrication of Alumina Nanotemplates

An anodizing process, at an early stage of development at the time of reporting the information for this article, has shown promise as a means of fabricating alumina nanotemplates integrated with silicon wafers. Alumina nanotemplates are basically layers of alumina, typically several microns thick, in which are formed approximately regular hexagonal arrays of holes having typical diameters of the order of 10 to 100 nm. Interest in alumina nanotemplates has grown in recent years because they have been found to be useful as templates in the fabrication of nanoscale magnetic, electronic, optoelectronic, and other devices. The present anodizing process is attractive for the fabrication of alumina nanotemplates integrated with silicon wafers in two respects: (1) the process involves self-ordering of the holes; that is, the holes as formed by the process are spontaneously arranged in approximately regular hexagonal arrays; and (2) the rates of growth (that is, elongation) of the holes are high enough to make the process compatible with other processes used in the mass production of integrated circuits. In preparation for fabrication of alumina nanotemplates in this process, one first uses electron-beam evaporation to deposit thin films of titanium, followed by thin films of aluminum, on silicon wafers. Then the alumina nanotemplates are formed by anodizing the aluminum layers, as described below. In experiments in which the process was partially developed, the titanium films were 200 A thick and the aluminum films were 5 m thick. The aluminum films were oxidized to alumina, and the arrays of holes were formed by anodizing the aluminum in aqueous solutions of sulfuric and/or oxalic acid at room temperature (see figure). The diameters, spacings, and rates of growth of the holes were found to depend, variously, on the composition of the anodizing solution, the applied current, or the applied potential, as follows: In galvanostatically controlled anodizing, regardless of the chemical composition of the solution, relatively high current densities (50 to 100 mA/cm2) resulted in arrays of holes that were more nearly regular than were those formed at lower current densities. . The rates of elongation of the holes were found to depend linearly on the applied current density: the observed factor of proportionality was 1.2 (m/h)/(mA/cm2). For a given fixed current density and room temperature, the hole diameters were found to depend mainly on the chemical compositions of the anodizing solutions. The holes produced in sulfuric acid solutions were smaller than those produced in oxalic acid solutions. The arrays of holes produced in sulfuric acid were more ordered than were those produced in oxalic acid. . The breakdown voltage was found to decrease logarithmically with increasing concentration of sulfuric acid. The breakdown voltage was also found to decrease with temperature and to be accompanied by a decrease in hole diameter. The hole diameter was found to vary linearly with applied potential, with a slope of 2.1 nm/V. This slope differs from slopes (2.2 and 2.77 nm/V) reported for similar prior measurements on nanotemplates made from bulk aluminum. The differences among these slopes may be attributable to differences among impurities and defects in bulk and electron-beam-evaporated aluminum specimens.

Myung, Nosang↗