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NDE Technology Engineering Program for Hanford DST Non-Visual Volumetric Inspection Technology: Phase II RAVIS Radiation Tolerance Test Report

This test report provides the results of radiation tolerance robustness testing that was performed on samples of robotic components and an ultrasonic guided wave air-slot sensor that represent components/sub-systems of the Robotic Air-slot Volumetric Inspection System (RAVIS) that has been engineered for volumetric inspection of Hanford tank bottom plates via under-tank refractory pad air-slots. The specific components tested for 1) functionality during active irradiation and 2) tolerance to cumulative radiation dose (until failure or upon reaching a cumulative dose test limit) were: • four samples each of a printed circuit board (PCB) and direct current (DC) motor, which are robotic components, and • 26 ultrasonic piezoelectric elements (samples) inside an air-slot sensor. The robotic components are part of the RAVIS air-slot inspection crawler drive control system that is responsible for remote communication with and actuation of the air-slot inspection crawler. The failure of either of these components during under-tank deployment would require manual retrieval via the crawler’s tether, which risks damage to the robot/refractory/tank. Preemptive replacement of the components at appropriately conservative dose/time intervals informed by failure dose would reduce the likelihood of under-tank failure. The components were included in radiation tolerance testing to quantify their failure doses to inform replacement intervals. The air-slot sensor is responsible for collecting ultrasonic inspection data (scan images) for the tank bottom plates during under-tank deployment. Compromised signal quality due to elevated noise levels caused by gamma radiation would compromise inspection performance. The air-slot sensor was included in radiation tolerance testing to quantify the impact of active irradiation on sensor signal quality. The irradiation and in-situ functional tests of the PCBs, DC motors and air-slot sensor took place in June and July 2020 at the Pacific Northwest National Laboratory. Testing was performed at a gamma dose rate near 300 rad/hr., which, in the absence of under-tank dose rate data, has been conservatively estimated to be the upper-bound dose rate beneath the primary tanks at Hanford. Irradiation took place at elevated temperatures of 150-200°F to determine failure doses that reflect the compounding effects of gamma radiation and heat. The test results revealed: • The DC motors can tolerate being actively irradiated at the high dose rate at 200°F and can tolerate a cumulative dose of 300,000 rad, that which would be incurred after 5 years of service at the 300 rad/hr dose rate. The component therefore meets minimum and preferred radiation tolerance and lifecycle requirements for robotic components. • The air-slot sensor can tolerate being actively irradiated at the high dose rate at 150°F and can tolerate a cumulative dose of 60,000 rad, that which would be incurred after 1 year of service at the 300 rad/hr dose rate. The sensor therefore meets minimum radiation tolerance and lifecycle requirements. • The PCB can tolerate being actively irradiated at the high dose rate, but can only tolerate a cumulative dose of 19,000 rad at 150-200°F. The PCB does not meet minimum radiation tolerance and lifecycle requirements; however, because the component is considered replaceable, it can be replaced before a cumulative dose of 19,000 rad is reached, determined through either monitoring with a dosimeter or scheduled time intervals that are calculated based on conservative estimates of under-tank dose rates.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

NDE Technology Development Program for Non-Visual Volumetric Inspection Technology: Technology Screening Report

The Pacific Northwest National Laboratory (PNNL) located in Richland, Washington, hosted and administered a Technology Screening test that allowed four different participants to demonstrate the NDE volumetric inspection technologies that were proposed in response to the WRPS EOI. This document provides a Technology Screening test report for the initial part of Phase I of a three-phase NDE Technology Development Program designed to identify and mature a system or set of non-visual volumetric NDE technologies for Hanford DST primary liner bottom inspection. Phase I of the program will baseline the performance of current or emerging non-visual volumetric NDE technologies for their ability to detect and characterize primary liner bottom flaws, and identify candidate technologies for adaptation and maturation for Phase II of the program.

42 ENGINEERING↗

NDE Technology Development Program for Non-Visual Volumetric Inspection Technology; Sensor Effectiveness Testing Report

The Pacific Northwest National Laboratory (PNNL) located in Richland, Washington, hosted and administered Sensor Effectiveness Testing that allowed four different participants to demonstrate the NDE volumetric inspection technologies that were previously demonstrated during the Technology Screening session. This document provides a Sensor Effectiveness Testing report for the final part of Phase I of a three-phase NDE Technology Development Program designed to identify and mature a system or set of non-visual volumetric NDE technologies for Hanford DST primary liner bottom inspection. Phase I of the program will baseline the performance of current or emerging non-visual volumetric NDE technologies for their ability to detect and characterize primary liner bottom flaws, and identify candidate technologies for adaptation and maturation for Phase II of the program.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Progress on Advancing Robotic Ultrasonic Volumetric Inspection Technology for Hanford Under-tank Inspection - 19474

The Hanford River Protection Project is reliant on safe interim storage of high-level waste at the Hanford site and will continue to depend on it until the waste has been treated and vitrified by the Hanford Waste Treatment and Immobilization Plant (WTP). The Hanford double-shell tanks (DSTs) have provided interim storage since the DSTs were put into service (1971 - 1986) and the RPP will continue to rely on their service until least 2050, at which time the 27 in-service DSTs will be 14-54 years beyond their original design lives. As the DSTs continue to age and be operated beyond design life, reliable leak integrity assessments of primary tanks and secondary liners will become increasingly important in order to provide situational awareness to tank operations personnel and to support risk-informed decisions on the selection of DSTs as waste feed staging tanks and the order and timing of future DST refurbishment or, alternatively, DST retrieval sequence. This paper summarizes progress made in fiscal year (FY) 2018 on the engineering of a robotic air-slot volumetric inspection system (RAVIS) that is designed to perform ultrasonic (volumetric) leak integrity inspections of physically inaccessible primary tank bottom plates and welds. Leak integrity inspections performed with the RAVIS will supplement today's primary tank leak integrity inspections, which are currently limited to physically accessible sidewall plates and welds. The RAVIS will be deployed into air slots of the insulating concrete (refractory) pad beneath the primary tanks and use its ultrasonic guided wave phased-array (GWPA) sensor to electronically steer an ultrasonic beam 360-degrees around the sensor to volumetrically examine adjacent carbon steel plates and welds covered by refractory pad material. Deployments of RAVIS down multiple air-slots will be performed to determine which regions of a tank bottom have sound leak integrity or which regions are in need of future wall thickness restoration or weld repair due to pitting corrosion, general corrosion, or heat/stress-induced cracks. The initial RAVIS design and the flaw detection test results for the first air-slot GWPA sensor that was designed to fit inside the air-slots will be presented in this paper. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NDE Technology Development Program for Non-Visual Volumetric Inspection Technology - Phase I Summary Report

This report provides a summary of the outcomes and findings of the sensor testing and evaluation work performed in FY2017 and first quarter of FY2018 under Phase I of the NDE Technology Development Program. The objective of this summary report is to provide a condensed version of the information provided in the Phase I program plan, Phase I test plan, the two comprehensive Phase I interim test reports issued for Technology Screening and advanced Sensor Effectiveness Testing, and the results from testing and demonstrations conducted Post-Sensor Effectiveness Testing for the purpose of supporting the selection of sensor technologies for maturation under Phase II. The orthogonal research and planning that should accompany technology maturation to support Phase II and Phase III are also included. The full details of the test mock-ups and flaws, sensor technologies, tests, evaluation criteria, and evaluation results are included in Phase I and provided in the interim Phase I test reports on Technology Screening and Sensor Effectiveness Testing.

47 OTHER INSTRUMENTATION↗

NDE Technology Development Program for Hanford DST Non-Visual Volumetric Inspection Technology – Phase II; Technical Letter Report on Air-slot NDE Sensor Maturation Testing

The Pacific Northwest National Laboratory (PNNL) located in Richland, Washington, hosted and administered Phase II Flaw Detection Performance Tests in August 2018 that allowed the newly matured ultrasonic guided wave phased-array (GWPA) air-slot NDE sensor—“Hanford-Probe A”—developed by Guidedwave to be evaluated for its flaw detection capability and repeatability. A portion of the Phase II Flaw Detection Performance Tests was performed on a subset of test flaws on which the original GWPA sensor was evaluated during Phase I Sensor Effectiveness Testing (SET) to facilitate a comparison in flaw detection performance between Hanford-Probe A and the original GWPA sensor demonstrated in Phase I. The objective of the performance comparison was to determine the extent to which GWPA sensor design changes impacted the flaw detection performance upon which selection of the sensor technology was originally based for the purpose of determining whether the flaw detection performance of the newly matured Hanford-Probe A GWPA air-slot NDE sensor is at least equal to that of the original GWPA sensor evaluated under Phase I SET. This technical letter report presents the results produced by the new Hanford-Probe A on the Phase I test flaws and the results of the flaw detection performance comparison between Hanford-Probe A and the original GWPA sensor demonstrated in Phase I.

47 OTHER INSTRUMENTATION↗

Progress on Advancing the Robotic Air-slot Volumetric Inspection System (RAVIS) for Hanford Under-tank Inspection - 20519

The 27 in-service double-shell tank (DST) systems at Hanford provide interim storage for nearly 56 million gallons of nuclear and hazardous chemical legacy waste. The safe and reliable storage of the waste is critical to the site's extended cleanup mission. While in service, the leak integrity of the DSTs must be demonstrated to satisfy the Washington Administrative Code, inform decisions on tank management, and gauge fitness for continued service beyond originally intended design lives. The carbon steel plates and welds that comprise DST primary tank sidewalls and lower knuckles are routinely 'sampled' for volumetric non-destructive testing using ultrasonic inspection technology to determine whether corrosion pitting, cracking, or general corrosion are occurring that could compromise tank leak integrity. However, the carbon steel plates and welds that comprise the bottoms of primary tanks have not been thoroughly inspected since the DSTs were constructed (i.e., since 1968-1986) due to limited physical access to the exterior tank bottoms. The Robotic Air-slot Volumetric Inspection System, or 'RAVIS,' is being engineered to overcome the challenge of tank bottom in-service inspection. The system will be deployed under primary tanks within the small cooling channels/air-slots in the refractory pads upon which the tanks rest and will use ultrasonic guided wave inspection technology to volumetrically inspect physically inaccessible regions that make up ∼90% of a tank bottom, as well as regions that are physically accessible from the air-slots but comprise only ∼10% of a tank bottom. This paper describes the air-slot sensor and robotic deployment system and focuses on the testing approach and methods that are being applied to support (1) design feedback and performance acceptance (requirement verification) and (2) performance repeatability/reliability assessments (qualification) to ensure the RAVIS is prepared for successful inservice inspections of primary tank bottoms. Test progress made against the test plan, the results of 2019 testing, and the future outlook are included. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Sensor Fusion Techniques for Phased-Array Eddy Current and Phased-Array Ultrasound Data

Sensor (or Data) fusion is the process of integrating multiple data sources to produce more consistent, accurate and comprehensive information than is provided by a single data source. Sensor fusion may also be used to combine multiple signals from a single modality to improve the performance of a particular inspection technique. Industrial nondestructive testing may utilize multiple sensors to acquire inspection data depending upon the object under inspection and the anticipated types of defects that can be identified. Sensor fusion can be performed at various levels of signal abstraction with each having its strengths and weaknesses. A multimodal data fusion strategy first proposed by Heideklang and Shokouhi that combines spatially scattered detection locations to improve detection performance of surface-breaking and near-surface cracks in ferromagnetic metals is shown using a surface inspection example and is then extended for volumetric inspections. Utilizing data acquired from an Olympus Omniscan MX2 from both phased array eddy current and ultrasound probes on test phantoms, single and multilevel fusion techniques are employed to integrate signals from the two modalities. Preliminary results demonstrate how confidence in defect identification and interpretation benefit from sensor fusion techniques. Lastly, techniques for integrating data into radiographic and volumetric imagery from computed tomography are described and results are presented.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Hanford Under-tank Inspection with Ultrasonic Volumetric Non-destructive Examination Technology - 18470

The U.S. Department of Energy (DOE) and the Hanford Site Tank Operations Contractor Washington River Protection Solutions, LLC (WRPS) are sponsoring a non-destructive evaluation (NDE) technology development program to identify and mature volumetric (non-visual) NDE technology that will enable the examination of Hanford double-shell tank (DST) bottoms. NDE technology for Hanford under-tank examination will be made possible through technology maturation that includes adaptation of NDE sensor technology to overcome access challenges presented by tank risers and refractory pad air-slots, followed by integration with robotic delivery systems, and ultimately qualification and deployment of the inspection systems. The stages of technology maturation and the testing and evaluation required to support the process are organized under three program phases: Phase I - NDE Capability Testing: Identify and down-select NDE technologies based on flaw detection and characterization abilities only; Phase 2 - NDE Delivery System Testing: Mature promising NDE technologies to adapt transducer hardware and robotic delivery system to address access challenges; Phase 3 - Full-scale Demonstration of Integrated NDE System: Demonstrate adapted NDE technologies in a cold test platform to challenge flaw detection and navigation abilities. Phase I of the program, which was initiated and completed in FY2017, focused on completing the following five key activities: 1. Identifying a broad cross section of potentially applicable NDE volumetric inspection technologies for under-tank examination. 2. Down-selecting the broad set of NDE technologies to a set of strong candidates based on initial flaw detection performance and potential to be adapted/matured to overcome primary tank access challenges posed by access risers and/or refractory pad air-slots. 3. Evaluating the flaw detection performance of the candidate sensors through testing. 4. Using the test results to baseline sensor performance against the flaw detection requirements established for high-level waste tanks. 5. Assessing the trade-offs and vulnerabilities of the candidate sensors that would negatively impact sensor performance reliability or complicate tank inspection operations. The completion of the first three key activities satisfied the first two Phase I test objectives, which were to complete Technology Screening and Sensor Effectiveness Testing. Completion of the fourth key activity satisfied the final test objective of Phase I, which was to determine the extent to which the sensors can satisfy high-level waste tank flaw detection requirements. Sensor flaw detection performance testing yielded several suitable sensor technology options, although each has specific risks or challenges that would need to be accepted or overcome. Thus, the fifth key activity was performed to evaluate sensor risks and challenges for consideration with flaw detection performance. The Phase I evaluation outcomes will be used to support the Phase I programmatic objective, which is to identify one or more NDE sensor technologies for adaptation and maturation for the DST environment. Selection of one or more sensors will mark the culmination of Phase I of the NDE Technology Development Program and allow progression to Phase II.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Draft ASME Code Case to qualify L-PBF 316H material for Section III, Division 5 applications

This report documents the AMMT program’s development and submission of a draft ASME Code Case to qualify Laser Powder Bed Fusion (L PBF) Type 316H stainless steel for Section III, Divi-sion 5 Class A and SM high temperature nuclear applications. It summarizes the technical basis, the comprehensive high temperature mechanical test database assembled between 2023–2026, and the proposed code language and qualification framework submitted to ASME. The work was co-ordinated across multiple national laboratories and leverages prior ASME efforts to integrate additive manufacturing into the Boiler & Pressure Vessel Code. The body of the report describes the experimental database and analysis supporting the Code Case: tensile, creep, fatigue, creep fatigue, and thermal aging tests collected from multiple additive manufacturing sites, machine types, and powder lots, with material processed by a solution anneal heat treatment. The dataset — including both full size and subsized specimens and tests oriented parallel and perpendicular to build direction — shows limited tensile anisotropy, tensile properties comparable to wrought 316H, creep strength within the scatter of wrought material, but markedly reduced creep ductility above about 650 °C associated with rapid σ phase formation in L PBF microstructures. The draft Code Case itself prescribes a staged qualification model (manufacturing process qualification, component qualification, and per build witness testing), treats L PBF components as equivalent to Type 316 weld metal for design and inspection, and requires mechanical, chemical, and metallographic controls tied to ASTM/ISO 52946. Key acceptance criteria include tensile tests within a 90% prediction interval of the AMMT dataset, a creep fatigue screening test adapted from ASME Section III, Division 5, Subsection HB, HBB 2800 but with the cycle acceptance reduced to 100 for L PBF material, and double volumetric inspection of production components. The report concludes that the present data support treating L PBF 316H as analogous to conventional fusion weld metal for Division 5 design and inspection, while highlighting important caveats: the σ phase driven loss of creep ductility above ~650 °C, preliminary indications of enhanced creep fatigue sensitivity in some lots, and remaining gaps in long term aging and additional cyclic testing. Recommended next actions include completing outstanding cyclic and long duration creep/aging tests on the solution annealed condition, supporting inclusion of the 316H chemistry and heat treatment in ASTM/ISO 52946, and continuing engagement with ASME and NRC during balloting and review to enable industry adoption.

Messner, Mark C. (ORCID:0000000200404385)↗

Study of ultrasonic characterization and propagation in austenitic welds: The MOSAICS project

Regulatory requirements enforce a volumetric inspection of welded components of nuclear equipments. However, the multi-pass austenitic welds are characterized by anisotropic and heterogeneous structures which lead to numerous disturbances of the ultrasonic beam. The MOSAICS project supported by the ANR (French National Research Agency) aims at matching various approaches to improve the prediction of the ultrasonic testing in those welds. The first stage consists in characterizing the weld structure (determination of the columnar grain orientation and measurements of elastic constants and attenuation coefficients). The techniques of characterization provide input data for the modeling codes developed in another task of the project. For example, a 3D version of the finite elements code ATHENA is developed by EDF R and D to take into account anisotropic texture in any direction. Semi-analytical models included in CIVA software are also improved to better predict the ultrasonic propagation in highly anisotropic and heterogeneous structures. The last stage deals with modeling codes validation based on experimental inspections on representative mock-ups containing calibrated defects. The objective of this paper is to give an overview of the MOSAICS project and to present specific results illustrating the various tasks.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Double-Shell Tank Primary Bottom Inspection Development - 19067

Double-Shell Tank (DST) integrity at Hanford is maintained with a variety of activities such as ultrasonic and visual inspections, chemistry controls, corrosion monitoring and structural analyses methods [1]. A pressing need for the Double-Shell Tank Integrity Program is the ability to inspect the bottom of the tanks. Though the DSTs' annulus spaces (the space between the internal and external tank walls) have been inspected visually since 1992 and with Ultrasonic Testing (UT) since 1996, WRPS has been unable to conduct inspections of the tank bottoms due to limitations of available technology, omitting about 40 percent of the tank surface below the maximum fill level from routine inspection. Visual inspections of the tank annulus have been conducted up to five times in some DSTs and the annulus space for all of the DSTs has been inspected twice with UT. The annulus region includes the walls of the primary tank and secondary liner along with accessible portions of the secondary liner bottom. Due to the lack of under-tank inspection technology, degradation of the primary tank bottom in Tank AY-102 was undetected until the tank leaked into its annulus space, confirmed in 2012 [2]. Since that time, WRPS has been working with the nondestructive examination community and the Pacific Northwest National Laboratory to evaluate potential technologies to conduct these challenging remote inspections. Recent work has included the development, testing, and deployment of several remote visual inspection technologies to observe the condition of the primary tank bottom of the DSTs by leveraging air distribution slots in the refractory pad on which it rests. Robotic solutions to conduct this inspection were developed with a detailed understanding of the physical configuration and operational logistics. Understanding and subsequent communication of these details to vendors within the robotics and nondestructive examination community was a critical component to the successful production of these new tools. In total, two remote visual inspection tools were produced by two vendors. The first tool was designed to leverage existing ultrasonic testing magnetic wall crawler technology in use within the double-shell tank annuli at Hanford. This resulted in a cost savings, immediate familiarization with the equipment, and a more streamlined shop to field experience. The second tool was developed from the ground up, and represents a more tailored and purpose-built solution to the problem. While costlier and more complex, it is also more versatile and capable of future growth or adaptation. Initial design of both tools began in early FY17 with fabrication and testing completed in early FY18. The tools were designed to be deployed alongside existing inspection operations and expand coverage. Development of visual inspection tools to evaluate the primary tank bottom region of the double-shell tanks was planned as the first stage of inspection. Continued development of volumetric sensors and incorporation of these inspection tools into Hanford's ongoing Double-Shell Tank Integrity Program are the next steps, continuously seeking to expand understanding of asset integrity and remaining useful life. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Double-Shell Tank Primary Bottom Visual Inspection Results - 20025

A pressing need for the Double-Shell Tank Integrity Program at Hanford is of the ability to inspect the bottom of the tanks. Though the DSTs' annulus spaces (the space between the internal and external tank walls) have been inspected visually since 1992 and with Ultrasonic Testing (UT) since 1996, inspections of the tank bottoms have been able to be conducted due to limitations of available technology, omitting about 40 percent of the tank surface below the maximum fill level from routine inspection. Visual inspections of the tank annulus have been conducted up to five times in some DSTs and portions of the annulus space for all of the DSTs has been inspected twice with UT. This region includes the walls of the primary tank and secondary liner along with accessible portions of the secondary liner bottom. Due to this lack of technology, the degradation of the primary tank bottom in Tank AY-102 was undetected until the tank leaked into its annulus space, confirmed in 2012. Since that time, WRPS has been working with the nondestructive examination community and the Pacific Northwest National Laboratory, to evaluate potential technologies to conduct these challenging remote inspections. Recent work has included the development, testing, and deployment of several remote visual inspection technologies to observe the condition of the primary tank bottom of the DSTs by leveraging air distribution slots in the refractory pad on which it rests. Robotic solutions to conduct this inspection were developed with a detailed understanding of the physical configuration and operational logistics. Understanding and subsequent communication of these details to vendors within the robotics and nondestructive examination community was a critical component to the successful production of these new tools. Throughout the FY16-FY18 years, vendors from nondestructive examination community were solicited for ideas to meet the tank bottom inspection challenge. Two tank bottom visual inspection solutions were then pursued to meet that challenge. Both tools were successfully deployed at Tank AP-107, and provided valuable visuals, never before obtained from the under tank environment of a double-shell tank. While there are minor opportunities for improvement identified with each system, general outcomes were overwhelmingly positive. Both systems were successfully able to navigate the refractory air slot pattern from the outer edge to the tank center and record video footage. The micro-crawler provided high quality and very stable footage through the air slot pattern, but took longer to deploy into the slots and traverse through them than the alternative system. The push-pull tethered camera was able to navigate all seven of its target air slots in a matter of a few hours, which included deployment, movement between slot entrances, and complete removal of the system from the annulus environment. Through these air slots, new information was gained about the tank bottom and refractory pad condition of tank AP-107, AP-106, AP-108, and AN-102. While some debris was noted in the air slots, including sand, chipped refractory, and construction materials, the refractory was found to be structurally stable and adequately supporting the primary tank bottom through the full diameter of the tank. Primary tank bottom steel exterior was found to be in good condition, free of ongoing or aggressive corrosion conditions. Looking toward the future, robotic access to and visual inspection of refractory air slots and the primary tank bottom steel has now proven viable. Incorporating periodic air slot inspections as a regular practice within the Double-Shell Tank Integrity Program is the next step, allowing trending of any changes in condition. As ultrasonic testing infrastructure was leveraged to complete the initial system deployments described in this report, it makes sense to adopt that same strategy for ongoing periodic examinations and deploy these primary tank bottom inspection tools alongside ultrasonic testing operations. Development of visual inspection tools to evaluate the primary tank bottom region of the double-shell tanks was planned as the first stage of inspection. Continued development of volumetric sensors and incorporation of these inspection tools into Hanford's ongoing Double-Shell Tank Integrity Program are the next steps, seeking to continuously expand understanding of asset integrity and remaining useful life. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Selection of Shear Horizontal Wave Transducers for Robotic Nondestructive Inspection in Harsh Environments

Harsh environments and confined spaces require that nondestructive inspections be conducted with robotic systems. Ultrasonic guided waves are well suited for robotic systems because they can provide efficient volumetric coverage when inspecting for various types of damage, including cracks and corrosion. Shear horizontal guided waves are especially well suited for robotic inspection because they are sensitive to cracks oriented perpendicular or parallel to the wave propagation direction and can be generated with electromagnetic acoustic transducers (EMATs) and magnetostrictive transducers (MSTs). Both types of transducers are investigated for crack detection in a stainless steel plate. The MSTs require the robot to apply a compressive normal force that creates frictional force coupling. However, the coupling is observed to be very dependent upon surface roughness and surface debris. The EMATs are coupled through the Lorentz force and are thus noncontact, although they depend on the lift off between transducer and substrate. After comparing advantages and disadvantages of each transducer for robotic inspection the EMATs are selected for application to canisters that store used nuclear fuel.

Choi, Sungho↗

Technology Development for Under Tank Inspection of Double-Shell Tanks - 20045

The Department of Energy (DOE) Office of River Protection (DOE-ORP) is responsible for management and cleanup of the tank farms located at the Hanford Site. Nuclear waste at Hanford is stored in 149 single-shell tanks (SSTs) and 27 double-shell tanks (DSTs). The vast majority of the liquid radioactive waste is stored in the DSTs. The 27 DSTs, located in six tank farms, were constructed from 1967 to 1986 and, compared to the SSTs, provide greatly improved protection from leakage and better accessibility for inspection. The DSTs and ancillary equipment are expected to exceed their design life before their waste is removed and sent to the Waste Treatment and Immobilization Plant. The DST Integrity Project (DSTIP) must ensure that the DST system can meet the River Protection Project mission goals. This paper provides a programmatic overview of the DSTIP with a focus on development of under-tank inspection technologies. Currently, two categories of nondestructive examination (NDE) techniques for DSTs are implemented on the Hanford site: (1) surface (SNDE) and (2) volumetric (VNDE). Further discussion on current inspection techniques is provided in this paper. The technology development approach for advanced VNDE techniques will also be generally discussed as a precursor for another more detailed WM2020 paper and presentation by PNNL. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Micro X-ray computed tomography examination of mini plate fuel with hot isostatic pressed aluminum cladding

In order to minimize proliferation risks and improve security of nuclear material, the United States high performance research and test reactors (USHPRR) program is tasked with converting nuclear reactors that are fueled with highly enriched uranium (HEU) fuels to operate with low-enriched uranium (LEU) nuclear fuels. One favorable LEU fuel configuration is plate fuel with a metallic uranium-molybdenum foil clad within an aluminum alloy (AA 6061). In this fuel, the aluminum cladding is bonded with a hot isostatic pressing (HIP) method to seal the cladding around the fuel meat. However, the HIP process parameters influence the cladding performance, as a defective or incomplete bond can cause a pathway for corrosion. Micro X-ray computed tomography (XCT), a nondestructive technique that provides volumetric imaging, can be applied to inspect fuel plate cladding at the engineering scale. In this work, XCT methodology was developed and successfully utilized to not only observe the bond line of unirradiated mini fuel plates, but to also identify subsurface abnormalities in the plates’ cladding. Importantly, in future work, this technique could be applied to fuel plates, pre- and post-irradiation, to quantify irradiation effects on cladding defects and bond line integrity.

36 MATERIALS SCIENCE↗

X-ray tomographic in-service inspection of girth welds - The European project TomoWELD

The new standard 'ISO 17636-2:2013: Non-destructive testing of welds - Radiographic testing - Part 2: X- and gamma-ray techniques with digital detectors', defines the practice for radiographic inspection of welded pipes for manufacturing and in-service inspection. It is applied in Europe for inspections of pipe welds in nuclear power plants as well as in chemical plants and allows a faster inspection with digital detector arrays (DDA) than with film. Nevertheless, it does not allow the evaluation of the depth and shape of volumetric and planar indications. In 2001 a planar tomography scanner, TomoCAR, was introduced for mechanized radiographic testing (RT) inspection and non-destructive measurement of cross sections. The project TomoWELD is based on a new concept of the scan geometry, an enhanced GPU based reconstruction, and the application of a new generation of photon counting DDAs based on CdTe crystal CMOS hybrids. The new detector permits the selection of energy thresholds to obtain an optimum energy range and reduction of the influence of scattered radiation. The concept and first measurements are presented. Flaw depth and shape of volumetric and planar irregularities can be determined.

36 MATERIALS SCIENCE↗

Comparative study of helium bubbles in a Ti-Ta alloy and a Ti/Ta nanocomposite

Here, we investigated the size, density, and distribution of helium (He) bubbles in a Ti-Ta single-phase alloy and a Ti/Ta dual-phase nanocomposite using transmission electron microscopy. The Ti/Ta nanocomposite was fabricated via phase separation during high-temperature annealing of the single-phase Ti-Ta alloy. He ion implantation in the Ti-Ta single-phase alloy leads to the formation of nano-scale He bubbles (~1.7 nm in size, ~2.6×10 5 /μm 3 in volumetric density). He bubbles were found to segregate to grain boundaries. Under identical implantation conditions, numerous He bubbles also formed in the Ti/Ta nanocomposite. Closer inspection revealed that He bubbles in the Ti-rich phase are smaller and of higher volumetric density (~1.2 nm, ~8.4×10 5 /μm 3 ) than those in the Tarich phase (~3 nm, ~1.8×10 5 /μm 3 ) and the single-phase alloy. He bubbles were also observed to decorate phase boundaries, but they were generally smaller than those on grain boundaries. These results suggest that Ti/Ta phase boundaries are less conducive to the growth of large He bubbles than grain boundaries in the Ti-Ta single phase alloy.

36 MATERIALS SCIENCE↗