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At least 19 records

Heat-induced drift reduction of time of flight in fused quartz acoustic waveguides via annealing process

High temperature structural acoustic sensors play an important role in many applications. Fused quartz waveguide is a popular choice due to its resistance to harsh environments and its convenience of modification. However, time of flight between pulse and echo, which is widely used in these sensors, tends to encounter drifts in fast temperature changing process even after temperature returns to initial value. In this article, different annealing process are performed for a special modified fused quartz waveguide with a sensor node. Annealing treatment is found able to reduce the drift when the waveguide undergoes a sudden temperature spike to 1000 °C at 500 kHz operating acoustic frequency, and the best annealing condition could make the drift one magnitude smaller. A following temperature test up to 1000 °C shows consistent measurement readings.

Hileman, Zachary (ORCID:0000000226529274)↗

Behavior of the Fused Quartz Suspended Core Acoustic Waveguide Sensor in Gamma Radiation

Previously, a fused-quartz acoustic waveguide named the suspended core waveguide with tight-field confinement in a small diameter was developed and its sensing potential in harsh environment was demonstrated with the fabricated periodic acoustic fiber Bragg grating. In this paper, the acoustic sensor was exposed to around 70 Gy/h gamma radiation at room temperature for 3550 h at Oak Ridge National Laboratory. For comparisons, a thermocouple and two optical fiber Bragg gratings were tested under the same conditions. The central frequency reading of the acoustic sensor was found to encounter a relatively fast decrease of 0.5 kHz in the first 800 hours. The reading then became stable, centering at 478.5 kHz with a fluctuation of ±0.2 kHz, and responded to small environmental temperature variations less than 1.2 °C. The major effect to the fluctuation was concluded to be radiation-induced material compaction and expansion. For optical fiber Bragg gratings, the same one-directional fast change of readings in the first 500 hours were observed as well. Although the optical gratings were able to track temperature changes, they also showed continuous drifts. The survivability and consistency of the acoustic sensor under long-term gamma radiation could lead to new sensing methods in nuclear applications.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Hybrid semiconductor-piezoacoustic radiofrequency device

An amplifying radiofrequency device includes a piezoelectric film and a semiconductor amplifier layer. The piezoelectric film is conformed as an acoustic waveguide. The piezoelectric film has a principal acoustic propagation direction parallel to the principal conduction direction of the amplifier layer. Interdigitated transducers are positioned on the piezoelectric film to respectively launch an acoustic wave in response to an input RF signal, and transduce the acoustic wave back to an output RF signal. There is a distance of less than the acoustic wavelength between the semiconductor amplifier layer and the piezoelectric film. The piezoelectric film has a thickness of less than the acoustic wavelength. According to a method for making such a device, a stack of III-V layers is epitaxially grown on a III-V substrate, wherein the stack comprises a first etch stop layer, a second etch stop layer, an amplifier layer, and a contact layer. The stack is bonded to a lithium niobate film. The III-V substrate is removed by etching down to the first etch stop layer. Deposition windows are opened by etching from the first etch stop layer down to the contact layer. Metal contact electrodes are deposited in the deposition windows.

36 MATERIALS SCIENCE↗

Thermal Modulation of Gigahertz Surface Acoustic Waves on Lithium Niobate

Surface-acoustic-wave (SAW) devices have a wide range of applications in microwave signal processing. Microwave SAW components benefit from higher quality factors and much smaller crosstalk when compared to their electromagnetic counterparts. Efficient routing and modulation of SAWs are essential for building large-scale and versatile acoustic wave circuits. Here, we demonstrate integrated thermoacoustic modulators using two SAW platforms: bulk lithium niobate and thin-film lithium niobate on sapphire. In both approaches, the gigahertz-frequency SAWs are routed by integrated acoustic waveguides, while on-chip microheaters are used to locally change the temperature, and thus, control the phase of the SAW. Using this approach, we achieve phase changes of over 720° with the responsibility of 2.6°/mW for bulk lithium niobate and 0.52°/mW for lithium niobate on sapphire. Furthermore, we demonstrate amplitude modulation of SAWs using acoustic Mach-Zehnder interferometers. Our thermoacoustic modulators can enable reconfigurable acoustic signal processing for next-generation wireless communications and microwave systems.

42 ENGINEERING↗

Ultrasonic Thermometer Sticking Mitigation Assessment

Ultrasonic thermometers have potential to improve on current technologies for very high temperature measurements. One issue limiting their adoption is the formation of diffusion bonds between the acoustic waveguide used as the sensor, and its surroundings (in some cases, a protective sheath). Several potential methods for reducing this diffusion bonding (known as sticking) have been identified. Prototype ultrasonic thermometers were fabricated and tested to high temperatures in order to evaluate these methods. Several showed promise for low temperature use. The most promising option was 3-D printed ceramic spacers.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Development of INL Ultrasonic Thermometer

This document summarizes the development at Idaho National Laboratory of an ultrasonic thermometer. The ultrasonic thermometer is a temperature sensor capable of multi-point measurements at very high temperatures with a high level of radiation tolerance. All of the components of the ultrasonic thermometer have been improved over the course of this work. The base technology, a magnetosrictive transducer, has been shown to be highly radiation tolerant. The solenoidal coil used in the transducer has been redesigned to operate at higher frequencies that previously possible. Materials used for the acoustic waveguide (the sensing portion of the device) have been tested and ideal candidates identified. Finally, a solution to the sticking issue (diffusion bonding between the waveguide and a protective sheath) has been developed and tested.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Selective Heating Through Y-Junction Waveguide Designed by Acoustic Shape Optimization

Unlike phononic crystals or systems designed by topology optimization, waveguides designed by shape optimization do not have voids or internal defects, making the fabrication process more suitable for additive manufacturing. By designing a Y-junction waveguide through shape optimization, an ultrasonic wave can be controlled so that it propagates to a predetermined location just by adjusting its frequency. These demultiplexed ultrasonic waves can be used to transport signals or stimulate nearby materials. As an example, the ultrasonic wave is converted to heat at different locations, which can be applied to mechanisms that can take advantage of heating. First, shape optimization is performed on a cylindrical structure to selectively propagate ultrasonic waves of a particular frequency while attenuating others, which is analyzed through a finite element model. The numerical study results are compared with experimental measurements from samples fabricated through additive manufacturing methods. After verifying the concept, the Y-junction waveguide is fabricated to demultiplex the wave and selectively heat different locations. Here the results show that the method of combining shape optimization with additive manufacturing is exceptionally simple and capable of demultiplexing ultrasonic waves, which can replace complex electrical components with single-material waveguides.

36 MATERIALS SCIENCE↗

Ultrasonic waveguide for improved ultrasonic thermometry

An improved ultrasonic waveguide for an ultrasonic thermometry system is provided. The waveguide includes a series of sensing zones, each of which is tuned to a specific narrow frequency band. The waveguide is acoustically coupled to a transducer, which launches a longitudinal elastic wave of desired waveform and frequency. The wave propagates down the waveguide, and is reflected from the sensing zone that is tuned to that frequency. Each sensing zone is designed to be highly reflective to a narrow frequency band while being transparent to other frequencies.

Cetiner, Nesrin O.↗

A Fabrication Strategy for Reconfigurable Millimeter–Scale Metamaterials

Rather than depending on material composition to primarily dictate performance metrics, metamaterials can leverage geometry to achieve specific properties of interest. For example, reconfigurable metamaterials have enabled programmable shape transformations, tunable mechanical properties, and energy absorption. While several methods exist to fabricate such structures, they often place severe restrictions on manufacturing materials, or require significant manual assembly. Moreover, these arrays are typically composed of unit cells that are either macro–scale or micro–scale in dimension. Here, the fabrication gap is bridged, and laminate manufacturing is used to develop a method for designing reconfigurable metamaterials at the millimeter–scale, that is compatible with a wide range of materials, and that requires minimal manual assembly. In addition to showing the versatility of this fabrication method, how the use of laminate manufacturing affects the behavior of these multi–component arrays is also characterized. To this end, a numerical model that captures the deformations exhibited by the structures is developed, and an analytic model that predicts the strain of the structure under compressive stress is built. Overall, this approach can be leveraged to develop millimeter–scale metamaterials for applications that require reconfigurable materials, such as in the design of tunable acoustics, photonic waveguides, and electromagnetic devices.

36 MATERIALS SCIENCE↗

Scalable phononic metamaterials: Tunable bandgap design and multi-scale experimental validation

Phononic metamaterials offer unprecedented control over wave propagation, making them essential for applications such as vibration isolation, waveguiding, and acoustic filtering. However, achieving scalable and precisely tunable bandgap properties across different length scales remains challenging. This study presents a user-friendly design framework for phononic metamaterials, enabling ultra-wide bandgap tunability (B/ω c ratios up to 172 %) across multiple frequency ranges and scales. Using finite element simulations of a Yablonovite-inspired unit cell, we establish a comprehensive parametric design space that illustrates how geometric parameters, such as sphere size and beam diameter, controls bandgap width and frequency. The scalability and robustness of the framework are validated through experimental testing on additively manufactured structures at both macro (10 mm) and micro (80 µm) scales, fabricated using Stereolithography and Two-Photon Polymerization. Transmission loss measurements, conducted with piezoelectric transducers and laser vibrometry, closely match simulations in the kHz and MHz frequency ranges, confirming the reliability and consistency of the bandgap behavior across scales. This work bridges theory and experiments at multiple scales, offering a practical methodology for the rapid design of phononic metamaterials and expanding their potential for diverse applications across a broad range of frequencies.

36 MATERIALS SCIENCE↗

Monolithic AlScN/SiC phononic waveguides for scalable acoustoelectric and quantum devices

Unlike conventional surface acoustic wave devices, phononic waveguide systems enable higher circuit density and stronger strain and piezoelectric fields, making them promising for advanced acoustoelectric and quantum applications. One such material system for generating and guiding phonons at gigahertz frequencies is AlScN on SiC, which can be synthesized by sputter depositing AlScN directly onto SiC wafers. The AlScN on the SiC platform allows for tightly vertically-confined acoustic modes with high electromechanical coupling, high speed of sound, and simple fabrication of strip and rib waveguides. Until now, this system has only been studied as a slab waveguide platform, i.e., without any lateral waveguiding. Here, we demonstrate a two-dimensionally confined phononic architecture in AlScN on SiC that supports guided modes at 2.95 and 4.05 GHz. These modes exhibit strong electromechanical coupling coefficients (k 2 = 4.27%) and propagation losses on the order of 10 dB/mm. Furthermore, this architecture is well-suited for phononic routing and power-efficient active or nonlinear devices such as amplifiers, mixers, and oscillators, and is compatible with the integration of quantum systems, including vacancy centers, charge carriers, photons, and spins, either embedded in SiC or heterogeneously integrated on the surface.

Electrical components↗

Ultrasonic sensors and methods of using the ultrasonic sensors

An ultrasonic sensor comprises a transducer in operable communication with a power source, a waveguide comprising a metal and at least one of a fissile material or a fertile material in operable communication with the transducer and configured to propagate and reflect acoustic waves generated by the transducer, the transducer configured to convert reflected acoustic waves to an electric signal, a thermally insulative material proximate the waveguide, and a control system in operable communication with the transducer, the control system configured to determine at least a temperature of the waveguide based on the reflected acoustic waves. Related methods are also disclosed.

Woolstenhulme, Nicolas E.↗

Magnetostrictive Ultrasonic Waveguide Transducer for In-Pile Thermometry

Real-time and reliable temperature measurement on nuclear fuels is crucial for the safe operation of existing pressurized-water reactors and future advanced nuclear reactors. Magnetostrictive materials deform when subjected to a magnetic field or exhibit magnetization variation when stressed. Here, based on these properties, this study prototyped an ultrasonic thermometer (UT) consisting of a magnetostrictive waveguide, a dc coil providing appropriate magnetic biasing, and an ac coil generating an acoustic impulse and detecting the resulting acoustic echoes. By tracking the time of flight between the excitation pulse and the echoes, the UT can potentially detect nuclear fuel cladding temperature from a long distance. In this study, magnetostrictive iron–gallium alloys, or Galfenol, were selected as the waveguide due to their large magnetostriction, superior temperature survivability, excellent radiation resilience, and high mechanical robustness. A multiphysics finite-element model considering electrical, magnetic, and mechanical dynamics in the magnetostrictive UT was then developed. The model exhibited an error of 0.24% in time-of-flight simulation and, therefore, enabled computer-aided design and guided signal processing. Between room temperature and 120 °C, the new Galfenol-based UT exhibits a linear sensitivity of 162.8×10 ₋6 °C ₋1 , which is 51.7% higher than a previous magnetostrictive UT based on iron–cobalt–vanadium alloys.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Modeling Seismic Recordings of High-Frequency Guided Infrasound on Mars

NASA's Interior Exploration using Seismic Investigations, Geodesy and Heat Transport (InSight) mission records several high-frequency (>0.5 Hz) dispersive seismic signals on Mars. These signals are due to the acoustic-to-seismic coupling of infrasound generated by the entry and impact of meteorites. This dispersion property is due to infrasound propagating in a structured atmosphere, and we refer to this dispersive infrasound as guided infrasound. We propose to model the propagation of guided infrasound and the seismic coupling to the ground analytically; we use a 1D layered atmosphere on a three-layer solid subsurface medium. The synthetic ground movements fit the observed dispersive seismic signals well and the fitting indicates that the regolith beneath InSight is about 40-m in thickness. We also examine and validate the previously-published subsurface models derived from InSight ambient seismic vibration data.

58 GEOSCIENCES↗

Integrated phononic waveguide on thin-film lithium niobate on diamond

Here, we demonstrate wavelength-scale phononic waveguides formed by transfer-printed thin-film lithium niobate (LN) on bulk diamond, a material stack that combines the strong piezoelectricity of LN with the high acoustic velocity and color-center compatibility of diamond. We characterize a delay line based on a 100 μm long phononic waveguide at room and cryogenic temperatures. The total insertion loss through the device at 4 K is −5.8 dB, corresponding to a $>$ 50 % transducer efficiency, at a frequency of 2.8 GHz. Our work represents a step toward phonon-mediated hybrid quantum systems consisting of strain-sensitive color centers in diamond.

Malik, Sultan [Stanford Univ., CA (United States)]↗