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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records
All sourcesNASA NTRSDOE OSTI
NASA NTRS1998

Detection of Metallic Compounds in Rocket Plumes Using Ion Probes

This grant experimentally verified that ion probes can consistently detect metallic compounds in a hybrid rocket plume. Two electrostatic detection methods were tested. The first method used an unbiased ion probe. It responded to collisions or near collisions with charged particulates. The amplitude of the response to metallic ions always exceeded that of the combustion products. The second device was a cylindrical Gaussian surface that surrounded, but did not touch, the plume. A charge imbalance in the plume induced a current in cylinder that was detected by a sensitive amplifier. The probe was more sensitive to metallic compounds than the cylinder. However, the Gaussian cylinder demonstrated sufficient sensitivity to warrant serious future consideration. Since the cylinder is nonintrusive, it is particularly attractive. Apparently, ions formed during combustion transfer to the metallic impurities. The formation of these metallic ions slows the ion recombination rate and helps preserve charges in the plume. The electrostatic detectors, in turn, respond to the charges carried by the metallic impurities.

Dunn, Robert W.↗
NASA NTRS2006

Optical Microscopy Techniques to Inspect for Metallic Whiskers

Metal surface finishes of tin, zinc and cadmium are often applied to electronic components, mechanical hardware and other structures. These finishes sometimes unpredictably may form metal whiskers over periods that can take from hours to months or even many years. The metal whiskers are crystalline structures commonly having uniform cross sectional area along their entire length. Typical whisker dimensions are nominally on the order of only a few microns (um) across while their lengths can extend from a few microns to several millimeters. Metal whiskers pose a reliability hazard to electronic systems primarily as an electrical shorting hazard. The extremely narrow dimensions of metal whiskers can make observation with optical techniques very challenging. The videos herein were compiled to demonstrate the complexities associated with optical microscope inspection of electronic and mechanical components and assemblies for the presence or absence of metal whiskers. The importance of magnification, light source and angle of illumination play critical roles in being able to detect metal whiskers when present. Furthermore, it is demonstrated how improper techniques can easily obscure detection. It is hoped that these videos will improve the probability of detecting metal whiskers with optical inspection techniques.

Brusse, Jay A.↗
NASA NTRS1991

Detection of metal stress in boreal forest species using the 0.67-micron chlorophyll absorption band

Several recent studies have shown that a shift of the red-edge inflection near 0.70 micron in vegetation reflectance spectra is an indicator of metal stress, partially attributable to changes in chlorophyll concentration. This 'red-edge shift', however, is difficult to detect and has been reported both toward longer (red) and shorter (blue) wavelengths. Our work demonstrates that direct measurement of the depth and width of the chlorophyll absorption band at 0.67 micron using digital feature extraction and absorption band characterization procedures developed for the analysis of mineral spectra is a more consistent indicator of metal stress. Additionally, the magnitude of these parameters is generally greater than that of the red edge shift and thus should be more amenable to detection and mapping using field and aircraft spectrometers.

Singhroy, Vernon H.↗
NASA NTRS1986

Lidar detection of metallic species at the mesopause level

The measurement alkali species present in the atomic form at the mesopause level has been performed by lidar for more than ten years. Atomic and ionic calcium density profiles are obtained for 3 years by the same technique in the visible range, at 423 nm for atomic calcium, and 393 nm for ionic calcium Ca(+). The experimental set-up and the preliminary results have been presented elsewhere. The 423 nm wavelength is directly obtained by the emission of a dye laser pumped by the third harmonic of a Nd-YAG laser. For the generation of the 393 nm wavelength, frequency mixing was used: the emission at 624 nm of a dye laser pumped by the 2nd harmonic of a Nd-Yag laser is mixed with the fundamental infrared emission (remaining after frequency doubling), in a non-linear KDP crystal, which gives the 393 nm emission. The behavior of the two atomic species, calcium and sodium, which are in the same altitude range are compared. For 45% of the observations, no ionic calcium was detected: the ionic calcium abundance was thus below the detection threshold. Contrasting with the density profiles of the atomic species, sodium and calcium, the ionic calcium profile present important variations on small time scales. The main characteristics of theatomic and ionic calcium behaviors that can be deduced from the measurements made are given.

Granier, C.↗
NASA NTRS1977

Sulfur in lunar mare basalts as a function of bulk composition

Sulfur abundances and metallic iron abundances in 18 Apollo 12 mare basalts were determined. No correlation between sulfur abundance and metallic iron content was detected; metallic iron abundances are not primarily caused by S loss. Sulfur abundances, directly related to the bulk composition of the rocks and especially to the TiO2 content, increase with increasing degrees of fractionation and appear to result from S concentration in the melts during fractionation. Unlike the Apollo 17 melts, the Apollo 12 melts were unsaturated with respect to sulfide. Composition appears to control S content for Apollo 17 basalts, and cumulus processes may cause Fe-FeS enrichment.

Gibson, E. K., Jr.↗
NASA NTRS2003

Detector Apparatus and Method

Transceiver and methods are included that are especially suitable for detecting metallic materials, such as metallic mines, within an environment. The transceiver includes a digital waveform generator used to transmit a signal into the environment and a receiver that produces a digital received signal. A tracking module preferably compares an in-phase and quadrature transmitted signal with an in-phase and quadrature received signal to produce a spectral transfer function of the magnetic transceiver over a selected range of frequencies. The transceiver initially preferably creates a reference transfer function which is then stored in a memory. Subsequently measured transfer functions will vary depending on the presence of metal in the environment which was not in the environment when the reference transfer function was determined. The system may be utilized in the presence of other antennas, metal, and electronics which may comprise a plastic mine detector for detecting plastic mines. Despite the additional antennas and other metallic materials that may be in the environment due to the plastic mine detector, the magnetic transceiver remains highly sensitive to metallic material which may be located in various portions of the environment and which may be detected by sweeping the detector over ground that may contain metals or mines.

Arndt, G. Dickey↗
NASA NTRS2004

Microwave-Spectral Signatures Would Reveal Concealed Objects

A proposed technique for locating concealed objects (especially small antipersonnel land mines) involves the acquisition and processing of spectral signatures over broad microwave frequency bands. This technique was conceived to overcome the weaknesses of older narrow- band electromagnetic techniques like ground-probing radar and low-frequency electromagnetic induction. Ground-probing radar is susceptible to false detections and/or interference caused by rocks, roots, air pockets, soil inhomogeneities, ice, liquid water, and miscellaneous buried objects other than those sought. Moreover, if the radar frequency happens to be one for which the permittivity of a sought object matches the permittivity of the surrounding soil or there is an unfavorable complex-amplitude addition of the radar reflection at the receiver, then the object is not detected. Low-frequency electromagnetic induction works well for detecting metallic objects, but the amounts of metal in plastic mines are often too small to be detectable. The potential advantage of the proposed technique arises from the fact that wideband spectral signatures generally contain more relevant information than do narrow-band signals. Consequently, spectral signatures could be used to make better decisions regarding whether concealed objects are present and whether they are the ones sought. In some cases, spectral signatures could provide information on the depths, sizes, shapes, and compositions of objects. An apparatus to implement the proposed technique (see Figure 1) could be assembled from equipment already in common use. Typically, such an apparatus would include a radio-frequency (RF) transmitter/receiver, a broad-band microwave antenna, and a fast personal computer loaded with appropriate software. In operation, the counter would be turned on, the antenna would be aimed at the ground or other mass suspected to contain a mine or other sought object, and the operating frequency would be swept over the band of interest.

Arndt, G.↗
NASA NTRS1993

The Hubble Space Telescope quasar absorption line key project. I - First observational results, including Lyman-alpha and Lyman-limit systems

Spectra are presented for 37 quasars with small and moderate redshifts; the quasars were observed with the Faint Object Spectrograph of the HST. New higher resolution measurements of the absorption lines in the UV spectra of 11 quasars with emission-line redshifts that lie between 0.3 and 1.0 are reported. Calibrated spectra and continuum fits are shown for each object. A total of 104 extragalactic Ly-alpha systems are identified, nine of which are found at the same redshifts as metal-line systems. The local number density of Ly-alpha systems with rest equivalent widths larger than 0.32 A and without detected metal lines is about 15.1 +/- 4.3 Ly-alpha systems per unit redshift with gamma = 0.30 +/- 0.62 and W* = 0.22 +/- 0.02 A. A total of 10 Lyman-limit systems with an optical depth greater than 0.4 are identified. The paucity of damped Ly-alpha lines at small and moderate redshifts shows that the number density of damped absorption systems decreases with decreasing redshift.

Bahcall, John N.↗
NASA NTRS1971

Use a SEM on a production line

Scanning electron microscope for poor metallization detection in manufacturing cycle of semiconductor devices

Adolphsen, J. W.↗
NASA NTRS1972

Using the scanning electron microscope on the production line to assure quality semiconductors

The use of the scanning electron microscope to detect metallization defects introduced during batch processing of semiconductor devices is discussed. A method of determining metallization integrity was developed which culminates in a procurement specification using the scanning microscope on the production line as a quality control tool. Batch process control of the metallization operation is monitored early in the manufacturing cycle.

Adolphsen, J. W.↗
NASA NTRS1990

Rings of Earth detected by orbital debris radar

Small particles moving at an orbital velocity of 7.6 kilometers per second can present a considerable hazard to human activity in space. For astronauts outside of the protective shielding of their space vehicles, such particles can be lethal. The powerful radar at NASA's Goldstone Deep Communications Complex was used to monitor such orbital debris. This radar can detect metallic objects as small as 1.8 mm in diameter at 600 km altitude. The results of the preliminary survey show a flux (at 600 km altitude) of 6.4 objects per square kilometer per day of equivalent size of 1.8 mm or larger. Forty percent of the observed particles appear to be concentrated into two orbits. An orbital ring with the same inclination as the radar (35.1 degrees) is suggested. However, an orbital band with a much higher inclination (66 degrees) is also a possibility.

Goldstein, R.↗
NASA NTRS1991

Engine throat/nozzle optics for plume spectroscopy

The Task 2.0 Engine Throat/Nozzle Optics for Plume Spectroscopy, effort was performed under the NASA LeRC Development of Life Prediction Capabilities for Liquid Propellant Rocket Engines program. This Task produced the engineering design of an optical probe to enable spectroscopic measurements within the SSME main chamber. The probe mounts on the SSME nozzle aft manifold and collects light emitted from the throat plane and chamber. Light collected by the probe is transferred to a spectrometer through a fiber optic cable. The design analyses indicate that the probe will function throughout the engine operating cycle and is suitable for both test stand and flight operations. By detecting metallic emissions that are indicative of component degradation or incipient failure, engine shutdown can be initiated before catastrophic failure. This capability will protect valuable test stand hardware and provide enhanced mission safety.

Bickford, R. L.↗
NASA NTRS1992

Rings of earth

Small particles moving at an orbital velocity of 7.6 kilometers per second can present a considerable hazard to human activity in space. For astronauts outside of the protective shielding of their space vehicles, such particles can be lethal. The powerful radar at NASA's Goldstone Deep Communications Complex was used to monitor such orbital debris. This radar can detect metallic objects as small as 1.8 mm in diameter at 600 km altitude. The results of the preliminary survey show a flux (at 600 km altitude) of 6.4 objects per square kilometer per day of equivalent size of 1.8 mm or larger. Forty percent of the observed particles appear to be concentrated into two orbits. An orbital ring with the same inclination as the radar (35.1 degrees) is suggested. However, an orbital band with a much higher inclination (66 degrees) is also a possibility.

Goldstein, Richard M.↗
NASA NTRS2018

Results of the Aerosol Sampling Experiment on the International Space Station

The indoor air quality of the International Space Station (ISS), in terms of particulate matter, has been assessed through a sampling experiment that collected airborne debris for return to Earth. The Aerosol Sampling Experiment took place on ISS in December 2016 and January 2017, with sample return in February 2017. For redundancy, two different aerosol samplers collected particles in two size ranges spanning from 10 nm to hundreds of micrometers. Multiple analysis techniques have been used to characterize the particles, such as reflective light microscopy, manual scanning electron microscopy (SEM) analysis (secondary and backscattered imaging) with energy dispersive spectroscopy (EDS) x-ray analysis, computer controlled scanning electron microscopy (CCSEM) and Raman spectroscopy. Sampling took place in five locations on ISS, with the greatest deposition of particles in Node 3, followed by Node 1, the US Lab and Node 2. The PMM had very few airborne particles, as expected, owing to the lack of human presence. A large proportion of the sampled material consisted of fibers from clothing. Many particles had complex morphologies or contained multiple metals in a carbonaceous matrix. Metal particles were analyzed for each sampling location in terms of both weight and number percent, with 27 heavy metals detected. Fiberglass and TiO2 particles were present in every location. Quantitative analysis results are presented, and where possible, particle emission sources are identified with the intention to fuel discussions on mitigation.

Meyer, Marit E.↗
NASA NTRS1977

Detecting contamination on a metal surface

Thin layers of contaminant on metal surface are detected by measuring surface-potential difference between reference electrode and surface of interest. Procedure does not require mechanical contact with surface under examination.

Harris, J. M.↗
NASA NTRS1978

On the detectability of a metallized lunar core

Calculations are made of the expected complex electromagnetic gain of the moon using current models of the internal bulk electrical conductivity with the addition of conducting cores of varying radii. The results show that the phase of the response (gain) function is sensitive to the radius and conductivity. The gain amplitude varies in a complicated way for frequencies above (0) 10 microHz. Below this 'corner' frequency, the square of the gain amplitude varies approximately quadratically with frequency and therefore inverse quadratically with hydromagnetic wavelength in the solar wind. The addition of conducting cores alters this dependence. A 'flat' frequency independent range for the gain amplitude evolves, which is a second way, in principle, to detect a conducting core. The departure from the lambda to the -4th Rayleigh scattering law is due to a combination of the conductivity of the moon and the relative unimportance of confinement of the induced fields at the very low frequencies of interest for core detection. For some core parameters, detection is not feasible with current data, and data recording times varying from several months to centuries would be required.

Wiskerchen, M. J.↗
NASA NTRS2004

Precious-Metal Salt Coatings for Detecting Hydrazines

Substrates coated with a precious-metal salt KAuCl4 have been found to be useful for detecting hydrazine vapors in air at and above a concentration of the order of 0.01 parts per million (ppm). Upon exposure to air containing a sufficient amount of hydrazine for a sufficient time, the coating material undergoes a visible change in color.

Dee, Louis A.↗