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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 19 records

New Insights on Subsurface Imaging of Carbon Nanotubes in Polymer Composites via Scanning Electron Microscopy

Despite many studies of subsurface imaging of carbon nanotube (CNT)-polymer composites via scanning electron microscopy (SEM), significant controversy exists concerning the imaging depth and contrast mechanisms. We studied CNT-polyimide composites and, by threedimensional reconstructions of captured stereo-pair images, determined that the maximum SEM imaging depth was typically hundreds of nanometers. The contrast mechanisms were investigated over a broad range of beam accelerating voltages from 0.3 to 30 kV, and ascribed to modulation by embedded CNTs of the effective secondary electron (SE) emission yield at the polymer surface. This modulation of the SE yield is due to non-uniform surface potential distribution resulting from current flows due to leakage and electron beam induced current. The importance of an external electric field on SEM subsurface imaging was also demonstrated. The insights gained from this study can be generally applied to SEM nondestructive subsurface imaging of conducting nanostructures embedded in dielectric matrices such as graphene-polymer composites, silicon-based single electron transistors, high resolution SEM overlay metrology or e-beam lithography, and have significant implications in nanotechnology.

Zhao, Minhua↗

Spaceborne radar subsurface imaging in hyperarid regions

Imaging data acquired with the Shuttle Imaging Radar (SIR-A) over the hyperarid region of Egypt/Sudan clearly show surface penetration through the sand cover. Even though absorption does occur in the sand layer, surface refraction leads to a steeper incidence angle at the sand/bedrock interface resulting in a stronger backscatter. A simple backscatter model shows that for a low-loss thin sand layer the presence of the covering layer enhances the capability to image the subsurface interface, particularly at large incidence angles and HH polarization.

Elachi, C.↗

Nanoscale Subsurface Imaging of Nanocomposites via Resonant Difference-Frequency Atomic Force Ultrasonic Microscopy

A scanning probe microscope methodology, called resonant difference-frequency atomic force ultrasonic microscopy (RDF-AFUM), has been developed. The method employs an ultrasonic wave launched from the bottom of a sample while the cantilever of an atomic force microscope engages the sample top surface. The cantilever is driven at a frequency differing from the ultrasonic frequency by one of the contact resonance frequencies of the cantilever. The nonlinear mixing of the oscillating cantilever and the ultrasonic wave at the sample surface generates difference-frequency oscillations at the cantilever contact resonance. The resonance-enhanced difference-frequency signals are used to create amplitude and phase-generated images of nanoscale near-surface and subsurface features. RDF-AFUM phase images of LaRC-CP2 polyimide polymer containing embedded nanostructures are presented. A RDF-AFUM micrograph of a 12.7 micrometer thick film of LaRC-CP2 containing a monolayer of gold nanoparticles embedded 7 micrometers below the specimen surface reveals the occurrence of contiguous amorphous and crystalline phases within the bulk of the polymer and a preferential growth of the crystalline phase in the vicinity of the gold nanoparticles. A RDF-AFUM micrograph of LaRC-CP2 film containing randomly dispersed carbon nanotubes reveals the growth of an interphase region at certain nanotube-polymer interfaces.

Cantrell, Sean A.↗

Nanoscale Subsurface Imaging via Resonant Difference-Frequency Atomic Force Ultrasonic Microscopy

A novel scanning probe microscope methodology has been developed that employs an ultrasonic wave launched from the bottom of a sample while the cantilever of an atomic force microscope, driven at a frequency differing from the ultrasonic frequency by the fundamental resonance frequency of the cantilever, engages the sample top surface. The nonlinear mixing of the oscillating cantilever and the ultrasonic wave in the region defined by the cantilever tip-sample surface interaction force generates difference-frequency oscillations at the cantilever fundamental resonance. The resonance-enhanced difference-frequency signals are used to create images of embedded nanoscale features.

Cantrell, Sean A.↗

Scanning Tunneling Microscopy methods for spectroscopic imaging of subsurface interfaces

A new method for spatially-resolved, spectroscopic investigation of subsurface interface structure has been developed. The method, Ballistic Electron Emission Microscopy (BEEM), is based on Scanning Tunneling Microscopy (STM) techniques. BEEM combines STM vacuum tunneling with unique ballistic electron spectroscopy capabilities. BEEM enables, for the first time, direct imaging of subsurface interface electronic properties with nanometer spatial resolution. STM topographic images of surface structure and BEEM images of subsurface properties are obtained simultaneously. BEEM capabilities are demonstrated by investigation of important metal-semiconductor interfaces.

Bell, L. D.↗

Spaceborne imaging radar research in the 90's

The imaging radar experiments on SEASAT and on the space shuttle (SIR-A and SIR-B) have led to a wide interest in the use of spaceborne imaging radars in Earth and planetary sciences. The radar sensors provide unique and complimentary information to what is acquired with visible and infrared imagers. This includes subsurface imaging in arid regions, all weather observation of ocean surface dynamic phenomena, structural mapping, soil moisture mapping, stereo imaging and resulting topographic mapping. However, experiments up to now have exploited only a very limited range of the generic capability of radar sensors. With planned sensor developments in the late 80's and early 90's, a quantum jump will be made in our ability to fully exploit the potential of these sensors. These developments include: multiparameter research sensors such as SIR-C and X-SAR, long-term and global monitoring sensors such as ERS-1, JERS-1, EOS, Radarsat, GLORI and the spaceborne sounder, planetary mapping sensors such as the Magellan and Cassini/Titan mappers, topographic three-dimensional imagers such as the scanning radar altimeter and three-dimensional rain mapping. These sensors and their associated research are briefly described.

Elachi, Charles↗

Nondestructive SEM for surface and subsurface wafer imaging

The scanning electron microscope (SEM) is considered as a tool for both failure analysis as well as device characterization. A survey is made of various operational SEM modes and their applicability to image processing methods on semiconductor devices.

Propst, Roy H.↗

Differential Muon Tomography to Continuously Monitor Changes in the Composition of Subsurface Fluids

Muon tomography has been used to seek hidden chambers in Egyptian pyramids and image subsurface features in volcanoes. It seemed likely that it could be used to image injected, supercritical carbon dioxide as it is emplaced in porous geological structures being used for carbon sequestration, and also to check on subsequent leakage. It should work equally well in any other application where there are two fluids of different densities, such as water and oil, or carbon dioxide and heavy oil in oil reservoirs. Continuous monitoring of movement of oil and/or flood fluid during enhanced oil recovery activities for managing injection is important for economic reasons. Checking on leakage for geological carbon storage is essential both for safety and for economic purposes. Current technology (for example, repeat 3D seismic surveys) is expensive and episodic. Muons are generated by high- energy cosmic rays resulting from supernova explosions, and interact with gas molecules in the atmosphere. This innovation has produced a theoretical model of muon attenuation in the thickness of rock above and within a typical sandstone reservoir at a depth of between 1.00 and 1.25 km. Because this first simulation was focused on carbon sequestration, the innovators chose depths sufficient for the pressure there to ensure that the carbon dioxide would be supercritical. This innovation demonstrates for the first time the feasibility of using the natural cosmic-ray muon flux to generate continuous tomographic images of carbon dioxide in a storage site. The muon flux is attenuated to an extent dependent on, amongst other things, the density of the materials through which it passes. The density of supercritical carbon dioxide is only three quarters that of the brine in the reservoir that it displaces. The first realistic simulations indicate that changes as small as 0.4% in the storage site bulk density could be detected (equivalent to 7% of the porosity, in this specific case). The initial muon flux is effectively constant at the surface of the Earth. Sensitivity of the method would be decreased with increasing depth. However, sensitivity can be improved by emplacing a greater array of particle detectors at the base of the reservoir.

Coleman, Max↗

Space Exploration Synthetic Aperture Radar - Lunar Investigations Targeted Experiment (SESAR-LITE)

The SESAR-LITE (Space Exploration Synthetic Aperture Radar - Lunar Investigations Targeted Experiment) instrument is a compact P-band (70 cm wavelength) polarimetric synthetic aperture radar under development at the NASA Goddard Space Flight Center to measure the surface and subsurface of the Moon at full polarimetry and at meter-scale resolution. The radar will use a compact deployable antenna, distributed RF electronics, and multi-channel digital processing system to enable a set of focused mission goals for small payload opportunities. The instrument development is leveraging proven technology advancements recently developed and demonstrated at NASA Goddard Space Flight center for SESAR (Space Exploration Synthetic Aperture Radar), a flagship version of the instrument that was tailored for larger orbital missions. The development of SESAR-LITE addresses accommodation flexibility on multiple launch vehicle families that require small packages while providing unprecedented surface and subsurface imaging of the Moon called for NASA’s Artemis program.

Synthetic Aperture Radar↗

Space Exploration Synthetic Aperture Radar - Lunar Investigations Targeted Experiment (Sesar-Lite)

The SESAR-LITE (Space Exploration Synthetic Aperture Radar - Lunar Investigations Targeted Experiment) instrument is a compact P-band (70 cm wavelength) polarimetric synthetic aperture radar under development at the NASA Goddard Space Flight Center (GSFC) to measure the surface and upper subsurface of the Moon at full polarimetry and at meter-scale resolution. The radar will use a compact deployable antenna, distributed RF electronics, and multi-channel digital processing system to enable a set of focused mission goals for small payload opportunities. The instrument development leverages proven technology advancements recently developed and demonstrated at NASA GSFC for SESAR (Space Exploration Synthetic Aperture Radar), a flagship version of the instrument that was tailored for larger orbital missions. The development of SESAR-LITE addresses accommodation flexibility on multiple launch vehicle families that require small packages while providing unprecedented surface and subsurface imaging of the Moon as required by NASA’s Artemis program.

Synthetic Aperture Radar↗

Large area QNDE inspection for airframe integrity

Quantitative Nondestructive Evaluation (QNDE) technology is being developed to provide new options for cost effective inspection of airframes. An R&D effort based on five NDE technologies is addressing questions of structural bonding assessment, corrosion detection, multisite damage detection, and fatigue characterization. The research/applications are being conducted by prioritized focussing and staging of the following technologies: (1) thermal NDE; (2) ultrasonic NDE; (3) coherent optical NDE; (4) magnetic imaging NDE; and (5) radiographic NDE. The focus here is on the most recent applications of thermal NDE technology to large area inspection of lap-joint and stiffener bonds. The approach is based on pulsed radiant heating of the airframe and measurement of the surface temperature of the structure with an infrared imager. Several advantages of the technique are that it is noncontacting, inspects one square meter area in a period of less than 2 minutes and has no difficulty inspecting typical curvatures of the fuselage. Numerical models of heat flow in these geometries are used to determine appropriate techniques for reduction of the infrared images, thereby delineating regions of disbonds. These models are also used to determine the optimum heating and measurement times for maximizing the contrast between bonded and unbonded structures. Good agreement is found between these results and experimental measurements, and a comparison of the two are presented. Also presented are results of measurements on samples with fabricated defects which show the technique is able to clearly indicate regions of disbonds. Measurements on an airframe also clearly image subsurface structure.

Winfree, William P.↗

An Autonomous Instrument Package for Providing 'Pathfinder' Network Measurements on the Surface of Mars

The investigations of the interior and atmosphere of Mars have been identified as high scientific priorities in most planetary exploration strategy document since the time of Viking. Most recently, the National Academy of Sciences has recommended a long-lived Mars network mission as its second highest scientific priority for Mars (after sample return) for the purpose of performing seismological investigations of the interior and studying the activity and composition of the atmosphere. Despite consistent recommendations by advisory groups, Mars network missions (MESUR, Marsnet, InterMarsnet, NetLander/MSR 05, NetLander/Premier 07, NetLander/?? 09) have undergone a strikingly consistent 'Phoenix' cycle of death and rebirth over the past 15 years, and there are still no confirmed plans to address the interior and atmosphere of Mars. The latest attempt is the NetLander mission. The objective of NetLander is to place a network of four landers on Mars to perform detailed measurements of the seismicity and atmospheric pressure, temperature, wind, humidity, and opacity (as well as provide images, subsurface radar sounding profiles, and electric/magnetic field measurements). However, this mission has recently encountered major programmatic difficulties within CNES and NASA. NASA has already cancelled its participation and the mission itself is facing imminent cancellation if CNES cannot solve programmatic issues associated with launching the mission in 2009. In this presentation we will describe an approach that could move us closer to realizing the goals of a Mars network mission and will secure at least one geophysical and meteorological observatory in 2009.

W B Banerdt↗

Pulsed-Source Interferometry in Acoustic Imaging

A combination of pulsed-source interferometry and acoustic diffraction has been proposed for use in imaging subsurface microscopic defects and other features in such diverse objects as integrated-circuit chips, specimens of materials, and mechanical parts. A specimen to be inspected by this technique would be mounted with its bottom side in contact with an acoustic transducer driven by a continuous-wave acoustic signal at a suitable frequency, which could be as low as a megahertz or as high as a few hundred gigahertz. The top side of the specimen would be coupled to an object that would have a flat (when not vibrating) top surface and that would serve as the acoustical analog of an optical medium (in effect, an acoustical "optic").

Shcheglov, Kirill↗

NASA Tech Briefs, June 2014

Topics include: Real-Time Minimization of Tracking Error for Aircraft Systems; Detecting an Extreme Minority Class in Hyperspectral Data Using Machine Learning; KSC Spaceport Weather Data Archive; Visualizing Acquisition, Processing, and Network Statistics Through Database Queries; Simulating Data Flow via Multiple Secure Connections; Systems and Services for Near-Real-Time Web Access to NPP Data; CCSDS Telemetry Decoder VHDL Core; Thermal Response of a High-Power Switch to Short Pulses; Solar Panel and System Design to Reduce Heating and Optimize Corridors for Lower-Risk Planetary Aerobraking; Low-Cost, Very Large Diamond-Turned Metal Mirror; Very-High-Load-Capacity Air Bearing Spindle for Large Diamond Turning Machines; Elevated-Temperature, Highly Emissive Coating for Energy Dissipation of Large Surfaces; Catalyst for Treatment and Control of Post-Combustion Emissions; Thermally Activated Crack Healing Mechanism for Metallic Materials; Subsurface Imaging of Nanocomposites; Self-Healing Glass Sealants for Solid Oxide Fuel Cells and Electrolyzer Cells; Micromachined Thermopile Arrays with Novel Thermo - electric Materials; Low-Cost, High-Performance MMOD Shielding; Head-Mounted Display Latency Measurement Rig; Workspace-Safe Operation of a Force- or Impedance-Controlled Robot; Cryogenic Mixing Pump with No Moving Parts; Seal Design Feature for Redundancy Verification; Dexterous Humanoid Robot; Tethered Vehicle Control and Tracking System; Lunar Organic Waste Reformer; Digital Laser Frequency Stabilization via Cavity Locking Employing Low-Frequency Direct Modulation; Deep UV Discharge Lamps in Capillary Quartz Tubes with Light Output Coupled to an Optical Fiber; Speech Acquisition and Automatic Speech Recognition for Integrated Spacesuit Audio Systems, Version II; Advanced Sensor Technology for Algal Biotechnology; High-Speed Spectral Mapper; "Ascent - Commemorating Shuttle" - A NASA Film and Multimedia Project DVD; High-Pressure, Reduced-Kinetics Mechanism for N-Hexadecane Oxidation; Method of Error Floor Mitigation in Low-Density Parity-Check Codes; X-Ray Flaw Size Parameter for POD Studies; Large Eddy Simulation Composition Equations for Two-Phase Fully Multicomponent Turbulent Flows; Scheduling Targeted and Mapping Observations with State, Resource, and Timing Constraints;

Source record↗

Method and Apparatus for Computed Imaging Backscatter Radiography

Systems and methods of x-ray backscatter radiography are provided. A single-sided, non-destructive imaging technique utilizing x-ray radiation to image subsurface features is disclosed, capable of scanning a region using a fan beam aperture and gathering data using rotational motion.

Shedlock, Daniel↗

Radio-interferometric imaging of the subsurface emissions from the planet Mercury

The distribution of total and polarized intensities from Mercury's subsurface layers have been mapped using VLA observations. The first detection of a hot pole along the Hermean equator is reported and modeled as black-body reradiation from preferential diurnal heating. These observations appear to rule out any internal sources of heat within Mercury. Polarized emission from the limb of the planet is also found, and is understood in terms of the dielectric properties of the Hermean surface.

Burns, J. O.↗