Measurement of electron temperature and number density in shock-tunnel flows. II
NO ion dissociative recombination rate coefficient determined in high temperature air plasma from electron temperature and number density measurements
Dunn, M. G.↗
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Is the common definition of the Mie-Grueneisen equation of state inconsistent
Anharmonic models are used to describe the high temperatures and the electronic effects characteristic of shock wave phenomena and planetary interiors. It is found that a generalized Grueneisen function dependent on temperature and volume is necessary for the self-consistent application of the Mie-Grueneisen equation at the physical conditions encountered in shock wave phenomena or in the interior of planets. It is noted that at temperatures of a few thousand degrees Kelvin, by deriving the function in terms of anharmonic lattice dynamics, the difference between gamma and gamma(th) is of the same order of a magnitude as gamma. This leads to the conclusions that (1) gamma is not a function of temperature and (2) gamma?gamma(th) does not explain either the equation of state of planetary interiors or high-temperature shock wave phenomena.
Mulargia, F.↗
Topological phase transition to a hidden charge density wave liquid
Charge density waves (CDWs), electronic crystals that form within a host solid, have long been speculated to melt into a spatially textured electronic liquid. Though they have not been previously detected, liquid CDWs may nonetheless be fundamental to the phase diagrams of many correlated electron systems, including high temperature superconductors and quantum Hall states. In one of the most promising candidate materials capable of hosting a liquid CDW, 1T-TaS2, a structural phase transition impedes its observation. Here, by irradiating the material with a femtosecond light pulse, we circumvent the structural phase transition to reveal how topological defect dynamics govern the otherwise invisible CDW correlations. Upon photoexcitation, the CDW diffraction peaks broaden azimuthally, initially revealing a hexatic state. At higher temperatures, photoexcitation completely destroys translational and orientational order and only a ring of diffuse scattering is observed, a key signature of a liquid CDW. Our work provides compelling evidence for a defect-unbinding transition to a CDW liquid and presents a protocol for uncovering states that are hidden by other transitions in thermal equilibrium.
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
Thermoelectric and Thermionic Conversion Technology
Applied research and technology efforts in thermoelectric and thermionic programs were recommended that will enable space power systems for the nation's future space missions. Specifically it was argued that the effort in thermoelectric materials technology be broadened with the objective of obtaining a material with a Figure of Merit greater than 1.0 x 10(-3)/K for hot junction temperatures of 1100 to 1500 K. The recommended effort in thermionics is to pursue technology programs that will result in an understanding and lifetime prediction methodologies for fuel-emitter and sheath-insulator behavior as a function of operating time and temperature. Also it is recommended that an effort be initiated that combines the thermoelectric, thermionic and power electronic technologies into a program to develop the technology for high temperature, high radiation resistant, and high current electronic switches.
Mondt, J. F.↗
LERCIP 2004 Summary
This summer I am continuing my project from the previous two summers. My work involves ohmic contacts to N-type silicon carbide (Sic) devices. My mentor, Dr. Robert Okojie, is developing the technology behind high performance sensors and actuators for harsh environments. Sic is useful because it is able to operate at temperatures up to 600 C and it is resistant to radiation damage. This allows sensors and electronics to be placed in new locations, such as inside a jet engine or in space application without using heavy shielding. Ultimately this results in more efficient, smarter engine technology, reduced launch weights for spacecraft, and high power and high temperature electronics. A fundamental part of Sic devices is the ohmic contact. The contact is the interface between the semiconductor (Sic) and external circuitry. The current flowing in and out the devices is through the contact. Ensuring that these contacts remain ohmic (linear I-V behavior) allows us to fabricate devices that do not waste power at the metallurgical junction. Another key part is maintaining a low contact resistance. It is desired to maintain minimum energy loss by avoiding a rectifying electrical characteristic. My project is to develop and implement a testing procedure for measuring the contact resistance while the device is operating at high temperature. It is important to measure the contacts while simulating the true operating environment as closely as possible. For this reason, measurements are taken while the device is heated at intervals up to 600 C in air. To test the long tern reliability of the devices, the high temperature measurements are repeated after heating the sample for long intervals in air. A new set of data is gathered after heating for a total of 100, 200 and then 400 hours. The current as a function of voltage and the contact resistance was measured using the four point probe technique. The four point probe method is chosen because it measures contact resistance while eliminating error due to wire resistance and calibration issues.
DeAngelis, David↗
Vacuum ultraviolet sensitive total radiation gage system.
Windowless total radiation gauge for shock tube measurements of high temperature gas radiance
SHOCK TUNNEL↗
Characterization of γ′/γ″ compact and sandwich type precipitates during long-term high-temperature exposure in Ni-based superalloys
Here, the formation of γ′/γ″ co-precipitates is investigated in Ni-based superalloys with a varying Ti/Al ratio and Ta content and their stability is studied using long-term high-temperature exposure. Transmission electron microscopy and atom probe tomography analyses demonstrate that both higher Ti/Al ratios and increased Ta promote γ″ phase formation, leading to sandwich and compact structures. The compact co-precipitation significantly reduces γ′ precipitate coarsening during 10,000 h exposure at 700°C by restricting elemental diffusion, particularly of aluminum, from the γ matrix to the γ′ phase. For the alloy without a compact structure, and only γʹ precipitates, at the beginning of the exposure, the coarsening rate over 10,000 h was 3.5 times faster than for the alloy with compact γʹ/γʺ precipitates. Evidence of destabilization of the compact morphology was found to occur between 5,000 and 10,000 h exposure and originated from the extensive formation and growth of δ platelets that extended throughout the grains. Thus, the outer layer of the compact, which consists of γʺ, was subjected to the γ″ to δ phase transformation.
gamma double prime↗
First observations from the Kr multi-monochromatic x-ray imager for time and spatially resolved diagnosis of hot implosion cores
This paper presents initial findings from the recently deployed Kr multi-monochromatic x-ray imager (Kr MMI) at the Omega laser facility. The experiment focuses on exploring implosion dynamics in exploding pusher capsules at three distinct initial gas fill densities. Utilizing time-gated and spatially integrated measurements, core size, electron temperature (Te), and electron densities (ne) are extracted through the analysis of the spectral region encompassing the Kr He α and its satellite lines. A comprehensive spectral database, incorporating atomic kinetics, spectroscopic-quality radiation transport, and Stark broadened line shapes, has been developed for rigorous data analysis. These measurements underscore the utility of the new Kr MMI instrument, which, combined with sophisticated analysis techniques, enables the diagnosis of plasma conditions at Te>2000 eV, thereby extending the capabilities beyond the prior Ar MMI design. This is an important stepping stone for achieving time-gated and space-resolved diagnostics of electron temperature, electron density, and heat transport in high temperature implosion cores.
73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
Solar particle composition measurements
The composition of solar particle events, that is the relative abundance of different elements, was studied, using nuclear emulsion detectors flown on board sounding rockets. These observations were extended to elements as heavy as iron. A model is discussed in which the particles in a flare are stripped of electrons in the high temperature of a flare region, and subsequently are accelerated presumably by magnetic fields.
Reames, D. V.↗
Correlation of creep rate with microstructural changes during high temperature creep
The techniques of electron microscopy were used to examine the microstructural changes which occur during primary creep for two important types of engineering alloys: (1) alloys strengthened by solid-solution additions, and (2) dispersion-strengthened alloys. The metals chosen for study are unalloyed titanium, Ti-6Al-4V, and the cobalt-base alloy, Haynes 188. Results to date on NGR 47-004-108 show that development of prior dislocation substructure in Haynes 188 by 10% prestrain and annealing for one hour at 1800 F increases the time to reach 0.5% creep strain at 1600 F by more than an order of magnitude for creep stresses from 3 to 20 ksi. For creep at 1800 F, similar results were obtaind for stresses above 7 ksi, but the prior substructure decreases creep resistance below 7 ksi. This effect appears to be related to instability of grain structure at 1800 F in prestrained material.
Young, C. T.↗
A theoretical study of heterojunction and graded band gap type solar cells
The work performed concentrated on including multisun effects, high temperature effects, and electron irradiation effects into the computer analysis program for heterojunction and graded bandgap solar cells. These objectives were accomplished and the program is now available for such calculations.
Chiang, J. P. C.↗
Periodic annealing of radiation damage in GaAs solar cells
Continuous annealing of GaAs solar cells is compared with periodic annealing to determine their relative effectiveness in minimizing proton radiation damage. It is concluded that continuous annealing of the cells in space at 150 C can effectively reduce the proton radiation damage to the GaAs solar cells. Periodic annealing is most effective if it can be initiated at relatively low fluences (approximating continuous annealing), especially if low temperatures of less than 200 C are to be used. If annealing is started only after the fluence of the damaging protons has accumulated to a high value 10 to the 11th power sq/pcm), effective annealing is still possible at relatively high temperatures. Finally, since electron radiation damage anneals even more easily than proton radiation damage, substantial improvements in GaAs solar cell life can be achieved by incorporating the proper annealing capabilities in solar panels for practical space missions where both electron and proton radiation damage have to be minimized.
Loo, R. Y.↗
O IV temperature determination for NGC 7662
A novel method is presented for the determination of electron temperatures in the high excitation zones of planetary nebulae and active galactic nuclei, using the ratio of the O IV line at 25.87 microns to those near 1400 A to calculate a temperature within the He III zone of the galaxy NGC 7662. The observed fluxes yield a lower bound to the temperature of 14,730 K, which is noted to be significantly higher than the O III temperature of about 12,000 K.
Shure, M. A.↗
Ultraviolet and optical spectroscopy of Cn 1-1 (= HDE 330036)
Ultraviolet and optical spectra of Cn 1-1 are presented. This stellar object has strong emission lines superposed on the absorption spectrum of an F5 III-IV star. It has been called both a symbolic star and a planetary nebula. Optical spectra taken over a period of two years do not show any variations in radial velocities. The radial velocities of the absorptionand emission-line spectra appear to be the same. The ultraviolet and optical spectra did not show variations in appearance over the period of observations. The interstellar extinction and distance are estimated by various methods, and values of c = 0.4 and d = 450 pc are adopted. The emission-line region is characterized by high-electron density and temperature and by enhancements over solar values in C/O and N/O. It is proposed that Cn 1-1 is a dense planetary nebula involved in a binary system. If so, the enhancements in abundances derived from the observations suggest that the planetary nebula is associated with a relatively massive progenitor star.
Lutz, J. H.↗
An Overview of MCC and Its Research
Viewgraphs on Microelectronics and Computer Technology Corporation (MCC) are presented. The MCC is a cooperative enterprise whose mission is to strengthen and sustain America's competitiveness in information technologies. Their objective is excellence in meeting broad industry needs through application-driven research, development, and timely deployment of innovative technology. Research programs include: software technology; VLSI/computer aided design; packaging/interconnect; electronic applications of high temperature superconductors; and advanced computing technology.
Lundstrom, Stephen F.↗
Superconductivity in Russia: Update and prospects
The research projects and new technological developments that have occured in Russia are highlighted in this document. Some of the research discussed includes: x-ray structure analysis of YBCO superconducting single crystals and accompanying phase transformations; the role of electron-electron interaction in High Temperature Superconductors (HTSC); the formation of Cooper pairs in crystals; the synthesis and research on a new family of superconductors based on complex copper and mercury oxides (HgBa2CuO4 + alpha and HgBa2CaCu2O6 + alpha); methods for the extraction of higher (up to C200) fullerenes and metalfullerenides has been developed; and process of production of Josephson junctions and development of SQUID's.
Ozhogin, V.↗
Identification of Gravity-Related Effects on Crystal Growth From Melts With an Immiscibility Gap
This work involves an experimental-numerical approach to study the effects of natural and Marangoni convections on solidification of single crystals from a silicate melt with a liquid-liquid immiscibility gap. Industrial use of crystals grown from silicate melts is becoming increasingly important in electronic, optical, and high temperature structural applications. Even the simplest silicate systems like Al203-SiO2 have had, and will continue to have, a significant role in the development of traditional and advanced ceramics. A unique feature of crystals grown from the silicate systems is their outstanding linear electro-optic properties. They also exhibit exceptionally high optical rotativity. As a result, these crystals are attractive materials for dielectric, optical, and microwave applications. Experimental work in our laboratory has indicated that directional solidification of a single crystal mullite appears to be preceded by liquid-liquid phase separation in the melt. Disruption of the immiscible state results in crystallization of a two phase structure. There is also evidence that mixing in the melt caused by density-driven convection can significantly affect the stability of the immiscible liquid layers and result in poly-crystalline growth. On earth, the immiscible state has only been observed for small diameter crystals grown in float zone systems where natural convection is almost negligible. Therefore, it is anticipated that growth of large single crystals from silicate melts would benefit from microgravity conditions because of the reduction of the natural convective mixing. The main objective of this research is to determine the effects of transport processes on the phase separation in the melt during growth of a single crystal while addressing the following issues: (1) When do the immiscible layers form and are they real?; (2) What are the main physical characteristics of the immiscible liquids?; and (3) How mixing by natural or Marangoni convection affects the stability of the phase separated melt.
Kassemi, M.↗
REQUIREMENTS FOR HIGH TEMPERATURE MATERIALS FOR SPACE VEHICLES
High temperature materials for space - electronic work function, thermoelectric properties, and corrosion resistance of alkali metals
ALKALI METAL↗