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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 289 records · Page 16

Multifunction Vacuum Chamber for IC Metallization

Vacuum system chamber processing multilayer metallization on integrated circuits (IC's) performs four operations ordinarily done in separated equipment. Chamber etches holes, removes photoresist, cleans by sputter etching, and deposits final layer of metal. Combinedfunction chamber costs less than separate equipment. Chamber avoids exposing integrated circuits to room air and, to oxidation and dust, between steps. Eliminates time spent in transferring circuits from one apparatus to next.

Routh, D. E.↗

Precise Viscosity Measurements Very Close to Critical Points

A torsion oscillator is being developed to measure the viscosity of fluids at moderate temperatures (0-100 C) and pressures (0-10 MPa) at very low frequencies (0.5 Hz) and very low shear rates (0.05/sec). These conditions are required to measure the shear viscosity of fluids extremely close to the critical point. The oscillator, thermostat, vacuum system, and instrumentation were assembled and are undergoing debugging. Preliminary measurements indicate that the system has a noise corresponding to 0.2% of the viscosity of methanol-cyclohexane mixtures near the consolute point.

Moldover, M. R.↗

Development of seeding techniques for small supersonic wind tunnel

The NASA Lewis 1x1 foot supersonic wind tunnel is used to experimentally verify computational methods. This tunnel, which is continuous running, operates from laboratory-wide high pressure air and vacuum systems. As such, the air does not recirculate but makes a single pass through the tunnel. The Mach number is varied with interchangeable nozzle blocks and has a range from Mach 1.6 to 4.0. Dry and filtered air is available up to pressures of 3 atmospheres. The air enters the tunnel system through a plenum having flow straighteners and 6 fine mesh screens. The exit of the plenum provides smooth contraction with an area ratio of approximately 20 that, along with the screens, provides a uniform flow for the nozzle.

Hingst, W. R.↗

Tribological characteristics of gold films deposited on metals by ion plating and vapor deposition

The graded interface between an ion-plated film and a substrate is discussed as well as the friction and wear properties of ion-plated gold. X-ray photoelectron spectroscopy (XPS) depth profiling and microhardness depth profiling were used to investigate the interface. The friction and wear properties of ion-plated and vapor-deposited gold films were studied both in an ultra high vacuum system to maximize adhesion and in oil to minimize adhesion. The results indicate that the solubility of gold on the substrate material controls the depth of the graded interface. Thermal diffusion and chemical diffusion mechanisms are thought to be involved in the formation of the gold-nickel interface. In iron-gold graded interfaces the gold was primarily dispersed in the iron and thus formed a physically bonded interface. The hardness of the gold film was influenced by its depth and was also related to the composition gradient between the gold and the substrate. The graded nickel-gold interface exhibited the highest hardness because of an alloy hardening effect. The effects of film thickness on adhesion and friction were established.

Miyoshi, K.↗

Ionization Chamber Measures Extreme Ultraviolet

Ionization chamber operates in nearly total photon absorption as stable, self-calibrating detector of ionizing extreme ultraviolet radiation. Working gas of instrument is neon; photoionization properties well known and readily applicable to absolute measurements. Designed for measurements of solar ultraviolet flux aboard sounding rocket, instrument used on Earth to measure ultraviolet radiation in vacuum systems. Ionization chamber collects positive neon ions and electrons produced by irradiation of neon gas by ultraviolet photons. Approximately one ion produced by each photon; consequently, photoionization current nearly proportional to photon flux.

Carlson, Robert W.↗

Cascaded-Blackbody Heat Radiators

New class of heat radiators made of metal or other conductive fin stock, fins of which are textured or covered with smaller fins. Measured from outside, effective emissivity of projected radiator surface greater than, and somewhat independent of, emissivity of flat surface made of same material. Special coatings to enhance emissivity not required, and emissivity not degraded significantly in long term by environmental effects. Intended orginally to radiate excess heat away from spacecraft, new radiators also used on Earth to dissipate heat in vacuum systems.

Keddy, Michael D.↗

Portable Airflow Meter

Compact hand-held instrument measures airflow. Consists of hot-wire anemometer probe in flow-straightening tube that reduces swirling. Configuration developed empirically to reduce length of instrument to practical dimension for use and storage in confined space. Two versions of new straightener only 17 and 18 in. long. Weighs less than 8 lb. and readily stored on Space Shuttle, developed to measure airflow in waster-collection system during flight. Used on Earth to measure airflow in ventilation systems, vacuum cleaners, and the like.

Burgett, Frank A.↗

Organic molecules on meteoritic solid substrates

The production of C1-C3 monocarboxylic acids from carbonaceous meteorites was investigated by the radiolysis of air-free CO2 and alkane solutions, utilizing a Cs-137 gamma-ray source. Samples were first loaded on a vacuum system, irradiated, and then analyzed by the Hewlett Packard model 5890A gas chromatograph. Moreover, the samples were irradiated with and without added ferrous iron.

Sweeney, Michael A.↗

U.S. Laboratory Module - Its capabilities and accommodations to support user payloads

The U.S. Laboratory Module of the Space Station is discussed, focusing on user accommodations. The configuration and subsystems capabilities of the module are described, including the power, thermal, environmental control, and data management subsystems, the vacuum system, process materials management, and laboratory support equipment. The experimental facilities included in the laboratory are listed. The experiment operations planned for the laboratory are examined and compared with the experimental activities in other manned space laboratories.

Powell, Luther E.↗

Photon sputtering of H2O ices: A preliminary report

A preliminary measurement of the total yields of ejected ions and electrons from H2O ices has been carried out using the He I 584 A resonance line as the incident photon beam. The H2O ices were prepared at 77 K in an ultrahigh vacuum system. The total yield of the ejected ion species and electrons was determined to be 8.8x10(exp -5) and 4.2x10(exp -4), respectively.

Wu, C. Y. Robert↗

Sealing Out-Of-Round Tubes With O-Rings

Glass or ceramic tubes out-of-round sealed effectively by ordinary O-rings in caps of modified hydraulic fittings. In typical connection, O-ring squeezed between two surfaces having inward-opening slants of 5 degrees or 10 degrees. Slanted surfaces force ring inward, compressing it around tube. Connector metal fitting, tightened by hand around O-ring, seals O-ring against tube as much as 1/16 in. out of round. Modified connectors seal glass or ceramic tubes against gas or vacuum leakage in furnaces, vacuum systems, and tubes for glassblowing equipment.

Shlichta, Paul J.↗

Complete the development and construction of a spaceborne hydrogen maser clock

The objective, to complete the development of an engineering model of a spaceborne hydrogen maser, was successfully achieved. A layout of the maser and detail drawings of the physics package was completed during the first 7 months of the contract. A computer model was made for the maser's thermal design. Using numerical computations, heater resistances were established for 7 temperature controlled zones. The physics package includes: a vacuum manifold that houses four sorption pumps capable of scavenging hydrogen for 4 years, a titanium vacuum tank housing the cavity, metallic seals for all vacuum joints, an RF dissociator within the vacuum envelope, a two-layer printed circuit solenoid and four layers of moly-permalloy magnetic shields. Problems were encountered and overcome in the procurements of the PC solenoid and the magnetic shields. After completion of the fabrication of the maser's components, the maser was assembled using these parts and other components made available by SAO, NRL, and NASA from earlier development work. In March, 1990, the vacuum system was assembled, and by May the maser assembly was completed. The magnetic shielding was poor and the shields were removed, reannealed by a local vendor, and the maser was reassembled. The maser began tests in early June and has been oscillating since that time. The test results of the maser are very good and a life test of the maser is being conducted. It is anticipated that the development and construction of a maser to be tested in space under a new contract from NASA's Marshall Space Flight Center will continue.

Vessot, Robert F. C.↗

Near-term, 100-kW class ion engines

A design approach for large area, high power ion engines is presented. This approach conceptually divides a single engine into a combination of smaller discharge chambers (or segments) configured to operate as a single large area engine. This segmented ion thruster (SIT) approach is shown to enable the immediate development of 100-kW class argon ion engines for operation at a specific impulse of 10,000 s. A combination of six 30-cm diameter ion chambers operating as a single engine can process over 100 kW. Such a segmented ion engine could be built today and would operate from a single power processor unit. The segmented engine design approach may also enable the development of megawatt class ion engines. Potential benefits of the segmented ion thruster design include: mitigation of the span-to-gap problem central to the development of large area, high power ion engines; reduction in hollow cathode emission current requirements; improved fault tolerance; and reduced vacuum system pumping speed requirements for engine development testing.

Brophy, John R.↗

The JPL Molecular Contamination Investigation Facility

The Molecular Contamination Investigation Facility (MCIF) is discussed in terms of its use for improving the far-UV performance of a camera and its broader applications. The MCIF incorporates two independent vacuum systems with sample isolation chambers and regulated heat exchangers as well as three quartz-crystal microbalances (QCMs) and a residual gas analyzer. One cryogenic QCM is heat sunk into an LN2 heat exchanger, while the others are thermoelectrically controlled and are heat sunk into a regulated heat exchanger. Outgas accumulation can be measured at three surface temperatures between -180 and 80 C simultaneously, and results are presented for the testing of 34 samples in a large-chambered system and 22 samples in a system with a smaller chamber. The MCIF results provide a database for fabrication processes, material selection, maximum bakeout temperatures, and the development of an ultraclean bakeout chamber.

Taylor, Daniel M.↗

Hydrophobic Porous Material Adsorbs Small Organic Molecules

Composite molecular-sieve material has pore structure designed specifically for preferential adsorption of organic molecules for sizes ranging from 3 to 6 angstrom. Design based on principle that contaminant molecules become strongly bound to surface of adsorbent when size of contaminant molecules is nearly same as that of pores in adsorbent. Material used to remove small organic contaminant molecules from vacuum systems or from enclosed gaseous environments like closed-loop life-support systems.

Sharma, Pramod K.↗

Study of the space environmental effects on spacecraft engineering materials

The space environment in which the Space Station Freedom and other space platforms will orbit is truly a hostile environment. For example, the current estimates of the integral fluence for electrons above 1 Mev at 2000 nautical miles is above 2 x 10(exp 10) electrons/sq cm/day. and the proton integral fluence is above 1 x 109 protons/sq cm/day. At the 200 - 400 nautical miles, which is more representative of the altitude which will provide the environment for the Space Station, each of these fluences will be proportionately less; however, the data indicates that the radiation environment will obviously have an effect on structural materials exposed to the environment for long durations. The effects of this combined environment is the issue which needs to be understood for the long term exposure of structures in space. In order to better understand the effect of these hostile phenomena on spacecraft, several types of studies are worth performing in order to simulate at some level the effect of the environment. For example the effect of protons and electrons impacting structural materials are easily simulated through experiments using the Van de Graff and Pelletron accelerators currently housed in the Environmental Effects Facility at MSFC. Proton fluxes with energies of 700 Kev-2.5 Mev can be generated and used to impinge on sample targets to determine the effects of the particles. Also the Environmental Effects Facility has the capability to generate electron beams with energies from 700 Kev to 2.5 Mev. These facilities will be used in this research to simulate space environmental effects from energetic particles. Ultraviolet radiation, particularly in the ultraviolet (less than 400 nm wavelength) is less well characterized at this time. The Environmental Effects Facility has a vacuum system dedicated to studying the effects of ultraviolet radiation on specific surface materials. This particular system was assembled in a previous study (NAS8-38609) in order to perform a variety of experiments on materials proposed for the Space Station. That system has continued to function as planned and has been used in carrying out portions of the proposed study.

Obrien, Susan K.↗

Study of the space environmental effects on spacecraft engineering materials

The issue of the effects of the space environment on spacecraft needs to be understood for the long term exposure of structures in space. In order to better understand the effect of these hostile phenomena on spacecraft, several types of studies are worth performing in order to simulate at some level the effect of the environment. For example the effect of protons and electrons impacting structural materials are easily simulated through experiments using the Van de Graff and Pelletron accelerators currently housed at MSFC. Proton fluxes with energies of 700 KeV - 2.5 MeV can be generated and used to impinge on sample targets to determine the effects of the particles. Also the Environmental Effects Facility at MSFC has the capability to generate electron beams with energies from 700 KeV to 2.5 MeV. These facilities will be used in this research to simulate space environmental effects from energetic particles. Ultraviolet radiation, particularly less than 400 nm wavelength, is less well characterized at this time. The Environmental Effects Facility has a vacuum system dedicated to studying the effects of ultraviolet radiation on specific surface materials. This particular system was assembled in a previous study in order to perform a variety of experiments on materials proposed for the Space Station. That system has continued to function as planned and has been used in carrying out portions of the proposed study.

Obrien, Susan K.↗

Apparatus Measures Permeation Of Gases Through Coupons

Apparatus measures permeation of any variety of commercially available pure or mixed gases through polymeric or other material coupons of various thicknesses. Permeability measured at wide range of temperatures and pressures. Includes residual-gas-analyzer (RGA) sensor head and associated circuitry, and vacuum system. Also includes manifold with valves, through which gas of interest allowed to permeate through test coupon before traveling downstream to evacuated RGA sensor head. Temperature of test coupon monitored by thermocouple and maintained at specified value above ambient by use of electrical heating mantle or below ambient by use of bath of ethylene glycol, water, and dry ice.

Adam, Steven J.↗