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Pressure-gage calibration, mass-spectrometer leak detector measures leakage rates up to 300 times greater than its normal limit. Approach utilizes constant-volume displacement characteristic of mechanical vacuum pump. Vacuum system must be small for calibration measurement validity and reduction of outgassing.
Several vacuum applications of copper foams in the density range 2-5% and pore sizes of 0.5-0.7 mm are discussed, such as a foreline hydrocarbon trap in a mechanical vacuum pump, a molecular-flow resistor, a diffuser, and a water injector. Other suggested applications include the use of foam copper in the form of an externally heated plug to remove traces of oxygen from inert gases bled into a vacuum system through a stainless steel line and the use of the porous surface for minimizing release of secondary electrons from electrodes in the path of charged particle beams.
Lead/tin solder coating on pipe threads serves as seal in non-critical vacuum systems. Pipe-thread seal is less expensive than weld or knife-edge flanges. Can also be used in place of sealing tape.
Valve cap seated on an O-ring lifts to relieve positive pressure. Is attached to vacuum system by screw-on housing. Caps are loosely tied to pipe with twine or thin wire to make recovery simple.
A molecular beam facility to simulate the space environment of a spacecraft at low orbit was designed with the intent of studying the effect on the properties of optical elements of oxygen atoms impacting at orbital velocity. The four-stage differentially pumped molecular beam facility includes a variety of oxygen atom beam sources which cover a wide range of velocities (1 km/sec to approximately 8 km/sec), in addition to the ultra-clean experimental environmental of an ultra-high vacuum chamber and an optical diagnostic set-up. The primary oxygen atom beam source used to obtain the 8 km/sec O atoms is an arc heated source. It consists of a modified commercially available plasma torch. The modifications include attachments which provide for a nozzle which is used to expand the atomic beam into the vacuum system, and exhaust channels to dispose of excess torch gas. The torch operates in the 'nontransferred' mode of operation, that is the electric arc is confined within the torch. A plasma is formed in helium by a dc arc. A small amount of O2 is injected downstream from the arc where it is thermally dissociated by the hot He into oxygen atoms. The high temperature and isentropic expansion give the oxygen atoms their velocity. Using seeded beam techniques, oxygen atom beams of approximately 3.5 and approximately 1.5 km/sec, respectively, are obtained.
A residual gas analyzer (RGA), a device for measuring the amounts and species of various gases present in a vacuum system is discussed. In a recent update of the RGA, it was shown that the use of microprocessors could revolutionize data acquisition and data reduction. This revolution is exemplified by the Inficon 1Q200 RGA which was selected to meet the needs of this update. The Inficon RGA and the Zilog microcomputer were interfaced in order the receive and format the digital data from the RGA. This automated approach is discussed in detail.
A passive hydrogen maser employing a smaller microwave cavity than previous masers is described. The volume of the entire resonator package, including a conventional source, hexapole state selector, and four magnetic shields, is estimated at 20 liters. The techniques for constructing the ceramic cavity, coating it with FEP, and attaching the endcaps to achieve a stable container (to allow its use as a single vacuum system) are described in detail. Frequency stability measurements were made of four such masers, against an NBS-4 cesium primary standard, against each other, and against eight commercial cesium clocks; frequency stability level is reported as 1.7 x 10 to the -12th tau exp -1/2 from 1 to 100,000 sec, and no drift above 1 x 10 to the -15th/day was found. Pressure and temperature effects on frequency stability were found at the 1 x 10 to the -14th level. Noise behavior beyond 200,000 sec is characterized as random walk. The potential use of a compact stable maser as a clock is suggested.
Leakage suppressed despite O-ring wear. New design eliminates leakage in vacuum selector valve on Space Shuttle waste-control subsystem. Applied to improve sealing in laboratory and industrial vacuum systems and other plumbing involving switching among lines with pressure differentials of order of 1 atmosphere (0.1 MPa).
The graded interface between an ion-plated film and a substrate is discussed as well as the friction and wear properties of ion-plated gold. X-ray photoelectron spectroscopy (XPS) depth profiling and microhardness depth profiling were used to investigate the interface. The friction and wear properties of ion-plated and vapor-deposited gold films were studied both in an ultra high vacuum system to maximize adhesion and in oil to minimize adhesion. The results indicate that the solubility of gold on the substrate material controls the depth of the graded interface. Thermal diffusion and chemical diffusion mechanisms are thought to be involved in the formation of the gold-nickel interface. In iron-gold graded interfaces the gold was primarily dispersed in the iron and thus formed a physically bonded interface. The hardness of the gold film was influenced by its depth and was also related to the composition gradient between the gold and the substrate. The graded nickel-gold interface exhibited the highest hardness because of an alloy hardening effect. The effects of film thickness on adhesion and friction were established.
The design and operations of a low cost, high rate thermal cycling facility designed for LEO conditions is described. Thermal cycling facilities were constructed with various design criteria. Some were designed to duplicate as closely as possible the conditions a cell or module would encounter while in orbit about the Earth. A typical facility to perform this type of cycling was a large vacuum system with liquid nitrogen cooled walls. The cells were heated by an AMO spectrum solar simulator, then a shutter was closed allowing the cells to give up their heat to the cold walls. This system was good at duplicating the orbital conditions but was slow and very costly to operate. Other systems used a gas atmosphere and heated the cells with radiant heat and cooled the cells by moving them into close proximity to a cold plate. The systems greatly increased the cycle times. Other systems moved the heating and cooling atmosphere into and out of the test areas and achieved reasonable cycle rates. All these systems, however, are expensive to operate.
The influence from the ambient plasma on the arc characteristics of a negatively biased solar cell array was investigated. The arc characteristics examined were the peak current during an arc, the decay time as the arc terminates, and the charge lost during the arc. These arc characteristics were examined in a nitrogen plasma with charge densities ranging from 15,000 to 45,000 cu cm. Background gas pressures ranged from 8x1,000,000 to 6x100,000 torr. Over these ranges of parameters no significant effect on the arc characteristics were seen. Arc characteristics were also examined for three gas species: helium, nitrogen and argon. The helium arcs have higher peak currents and shorter decay times than nitrogen and argon arcs. There are slight differences in the arc characteristics between nitrogen and argon. These differences may be caused by the differences in mass of the respective species. Also, evidence is presented for an electron emission mechanism appearing as a precursor to solar array arcs. Occassionally the plasma generator could be turned off, and currents could still be detected in the vacuum system. When these currents are presented, arcs may occur.
An oblique focus intensified charge coupled device (ICCD) was constructed and operated in a vacuum system. Special gratings were obtained and an optical system set up to try to model a candidate UV spectrometer (Milieu Interstellaire et Intergalactique-MISIG), and to produce small enough images to test the theoretical subpixel resolution capability of the ICCD system. The efforts were only partly successful. Based on the results, a similar detector was built and flown successfully on a Princeton rocket program.
The deposition of semiconducting and insulating thin films at low temperatures using microwave technology was explored. The method of plasma formations, selection of a power source, the design of the microwave plasma cavity, the microwave circuitry, impedance matching, plasma diagnostics, the deposition chamber and the vacuum system were studied.
The influence from the ambient plasma on the arc characteristics of a negatively biased solar cell array was investigated. The arc characteristics examined were the peak current during an arc, the decay time as the arc terminates, and the charge lost during the arc. These arc characteristics were examined in a nitrogen plasma with charge densities ranging from 15,000 to 45,000 cu cm. Background gas pressures ranged from 8x1,000,000 to 6x100,000 torr. Over these ranges of parameters no significant effect on the arc characteristics were seen. Arc characteristics were also examined for three gas species: helium, nitrogen and argon. The helium arcs have higher peak currents and shorter decay times than nitrogen and argon arcs. There are slight differences in the arc characteristics between nitrogen and argon. These differences may be caused by the differences in mass of the respective species. Also, evidence is presented for an electron emission mechanism appearing as a precursor to solar array arcs. Occasionally the plasma generator could be turned off, and currents could still be detected in the vacuum system. When these currents are presented, arcs may occur.
Vacuum system chamber processing multilayer metallization on integrated circuits (IC's) performs four operations ordinarily done in separated equipment. Chamber etches holes, removes photoresist, cleans by sputter etching, and deposits final layer of metal. Combinedfunction chamber costs less than separate equipment. Chamber avoids exposing integrated circuits to room air and, to oxidation and dust, between steps. Eliminates time spent in transferring circuits from one apparatus to next.
A torsion oscillator is being developed to measure the viscosity of fluids at moderate temperatures (0-100 C) and pressures (0-10 MPa) at very low frequencies (0.5 Hz) and very low shear rates (0.05/sec). These conditions are required to measure the shear viscosity of fluids extremely close to the critical point. The oscillator, thermostat, vacuum system, and instrumentation were assembled and are undergoing debugging. Preliminary measurements indicate that the system has a noise corresponding to 0.2% of the viscosity of methanol-cyclohexane mixtures near the consolute point.
The NASA Lewis 1x1 foot supersonic wind tunnel is used to experimentally verify computational methods. This tunnel, which is continuous running, operates from laboratory-wide high pressure air and vacuum systems. As such, the air does not recirculate but makes a single pass through the tunnel. The Mach number is varied with interchangeable nozzle blocks and has a range from Mach 1.6 to 4.0. Dry and filtered air is available up to pressures of 3 atmospheres. The air enters the tunnel system through a plenum having flow straighteners and 6 fine mesh screens. The exit of the plenum provides smooth contraction with an area ratio of approximately 20 that, along with the screens, provides a uniform flow for the nozzle.
The graded interface between an ion-plated film and a substrate is discussed as well as the friction and wear properties of ion-plated gold. X-ray photoelectron spectroscopy (XPS) depth profiling and microhardness depth profiling were used to investigate the interface. The friction and wear properties of ion-plated and vapor-deposited gold films were studied both in an ultra high vacuum system to maximize adhesion and in oil to minimize adhesion. The results indicate that the solubility of gold on the substrate material controls the depth of the graded interface. Thermal diffusion and chemical diffusion mechanisms are thought to be involved in the formation of the gold-nickel interface. In iron-gold graded interfaces the gold was primarily dispersed in the iron and thus formed a physically bonded interface. The hardness of the gold film was influenced by its depth and was also related to the composition gradient between the gold and the substrate. The graded nickel-gold interface exhibited the highest hardness because of an alloy hardening effect. The effects of film thickness on adhesion and friction were established.