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Advances in Small Particle Handling of Astromaterials in Preparation for OSIRIS-REx and Hayabusa2: Initial Developments

The Astromaterials Acquisition and Curation office at NASA Johnson Space Center has established an Advanced Curation program that is tasked with developing procedures, technologies, and data sets necessary for the curation of future astromaterials collections as envisioned by NASA exploration goals. One particular objective of the Advanced Curation program is the development of new methods for the collection, storage, handling and characterization of small (less than 100 micrometer) particles. Astromaterials Curation currently maintains four small particle collections: Cosmic Dust that has been collected in Earth's stratosphere by ER2 and WB-57 aircraft, Comet 81P/Wild 2 dust returned by NASA's Stardust spacecraft, interstellar dust that was returned by Stardust, and asteroid Itokawa particles that were returned by the JAXA's Hayabusa spacecraft. NASA Curation is currently preparing for the anticipated return of two new astromaterials collections - asteroid Ryugu regolith to be collected by Hayabusa2 spacecraft in 2021 (samples will be provided by JAXA as part of an international agreement), and asteroid Bennu regolith to be collected by the OSIRIS-REx spacecraft and returned in 2023. A substantial portion of these returned samples are expected to consist of small particle components, and mission requirements necessitate the development of new processing tools and methods in order to maximize the scientific yield from these valuable acquisitions. Here we describe initial progress towards the development of applicable sample handling methods for the successful curation of future small particle collections.

Snead, C. J.↗

Curating NASA's Past, Present, and Future Astromaterial Sample Collections

The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (hereafter JSC curation) is responsible for curating all of NASA's extraterrestrial samples. JSC presently curates 9 different astromaterials collections in seven different clean-room suites: (1) Apollo Samples (ISO (International Standards Organization) class 6 + 7); (2) Antarctic Meteorites (ISO 6 + 7); (3) Cosmic Dust Particles (ISO 5); (4) Microparticle Impact Collection (ISO 7; formerly called Space-Exposed Hardware); (5) Genesis Solar Wind Atoms (ISO 4); (6) Stardust Comet Particles (ISO 5); (7) Stardust Interstellar Particles (ISO 5); (8) Hayabusa Asteroid Particles (ISO 5); (9) OSIRIS-REx Spacecraft Coupons and Witness Plates (ISO 7). Additional cleanrooms are currently being planned to house samples from two new collections, Hayabusa 2 (2021) and OSIRIS-REx (2023). In addition to the labs that house the samples, we maintain a wide variety of infra-structure facilities required to support the clean rooms: HEPA-filtered air-handling systems, ultrapure dry gaseous nitrogen systems, an ultrapure water system, and cleaning facilities to provide clean tools and equipment for the labs. We also have sample preparation facilities for making thin sections, microtome sections, and even focused ion-beam sections. We routinely monitor the cleanliness of our clean rooms and infrastructure systems, including measurements of inorganic or organic contamination, weekly airborne particle counts, compositional and isotopic monitoring of liquid N2 deliveries, and daily UPW system monitoring. In addition to the physical maintenance of the samples, we track within our databases the current and ever changing characteristics (weight, location, etc.) of more than 250,000 individually numbered samples across our various collections, as well as more than 100,000 images, and countless "analog" records that record the sample processing records of each individual sample. JSC Curation is co-located with JSC's Astromaterials Research Office, which houses a world-class suite of analytical instrumentation and scientists. We leverage these labs and personnel to better curate the samples. Part of the cu-ration process is planning for the future, and we refer to these planning efforts as "advanced curation". Advanced Curation is tasked with developing procedures, technology, and data sets necessary for curating new types of collections as envi-sioned by NASA exploration goals. We are (and have been) planning for future cu-ration, including cold curation, extended curation of ices and volatiles, curation of samples with special chemical considerations such as perchlorate-rich samples, and curation of organically- and biologically-sensitive samples.

Zeigler, R. A.↗

Lessons Learned From Designing and Building Low Organic Outgassing Cleanrooms for NASA OSIRIS-REx and Hayabusa2 Curation Facility

NASA Johnson Space Center Astromaterials Acquisition and Curation Office completed construction and commissioning of the OSIRIS-REx and Hayabusa2 cleanroom laboratory suites along with new precision cleaning and advanced curation laboratories consisting of ISO Class 5, 6, and 7 cleanrooms. The new curation facilities are designed for initial receiving, basic characterization, curation processing, and preliminary examination of carbonaceous asteroidal material. The facilities are also designed to enable long-term pristine sample storage to preserve the scientific integrity of each sample to enable future research by the international science community. The scientific study of organics is critical for both missions. The OSIRIS-REx mission instituted a stringent contamination control plan for low organics. Given these mission requirements and long-term storage preservation requirements, cleanroom construction materials were carefully selected to not hinder the scientific search for amino acids and the study of organics in the samples. Cleanroom candidate construction materials were researched for the HVAC system, floors, walls, ceiling, and plenum areas. The team chose several candidate materials that were further tested for their specific outgassing characteristics using ASTM E-595 per ASTM E-2312. The information gained provided the foundation for the final design selection of the cleanroom materials. While material selection is important before and during the facility design phase, the construction phase is where these choices are implemented by the prime construction contractor through final product and material submittals. These submittals are the last check point and changes are often submitted due to engineering/construction conflicts, especially when renovating an existing building. Any new material or equipment/product change must be identified and scrutinized for low particulate shedding and outgassing properties. In some cases, quick testing of new material is required, and compromises must be made in real-time. Careful selection and implementation of cleanroom materials significantly reduced organic and inorganic contamination beyond normal cleanroom baselines.

astromaterials curation↗

Lessons Learned From Designing and Building Low Organic Outgassing Cleanrooms for NASA OSIRIS-REx and Hayabusa2 Curation Facility

NASA Johnson Space Center Astromaterials Acquisition and Curation Office completed construction and commissioning of the OSIRIS-REx and Hayabusa2 cleanroom laboratory suites along with new precision cleaning and advanced curation laboratories consisting of ISO Class 5, 6, and 7 cleanrooms. The new curation facilities are designed for initial receiving, basic characterization, curation processing, and preliminary examination of carbonaceous asteroidal material. The facilities are also designed to enable long-term pristine sample storage to preserve the scientific integrity of each sample to enable future research by the international science community. The scientific study of organics is critical for both missions. The OSIRIS-REx mission instituted a stringent contamination control plan for low organics. Given these mission requirements and long-term storage preservation requirements, cleanroom construction materials were carefully selected to not hinder the scientific search for amino acids and the study of organics in the samples. Cleanroom candidate construction materials were researched for the HVAC system, floors, walls, ceiling, and plenum areas. The team chose several candidate materials that were further tested for their specific outgassing characteristics using ASTM E-595 per ASTM E-2312. The information gained provided the foundation for the final design selection of the cleanroom materials. While material selection is important before and during the facility design phase, the construction phase is where these choices are implemented by the prime construction contractor through final product and material submittals. These submittals are the last check point and changes are often submitted due to engineering/construction conflicts, especially when renovating an existing building. Any new material or equipment/product change must be identified and scrutinized for low particulate shedding and outgassing properties. In some cases, quick testing of new material is required, and compromises must be made in real-time. Careful selection and implementation of cleanroom materials significantly reduced organic and inorganic contamination beyond normal cleanroom baselines.

astromaterials curation↗

Lessons Learned From the Construction of a Portable Cleanroom for NASA OSIRIS-REx Mission Deintegration

NASA Johnson Space Center (JSC) Infrastructure and Astromaterials Acquisition & Curation Office completed construction and commissioning of the OSIRIS-REx (OREx) Deintegration portable cleanroom at the Utah Test and Training Range (UTTR). The new portable cleanroom was designed to receive the OREx sample return capsule from the landing point on the range to an ISO7 environment. Scientists used the portable clean-room to deintegrate the sample canister from the sample return capsule. Once separated, the sample canister was put in a container under nitrogen purge for transportation to B31 at the Johnson Space Center for astromaterial sample extraction, preliminary analysis, and long-term curation. The portable cleanroom was built by a subcontractor at their facility and then deconstructed to be transported to the remote location at UTTR. Since construction was completed in a remote location all tools and materials had to be transported from contractor site in Dallas, TX. The cleanroom was constructed within an existing facility, which provided conditioned air, electric power, and protection from the elements. Careful coordination was required between the host facility, cleanroom contractor, mission scientists, and JSC facilities and curation personnel. An existing anteroom at JSC was transported to UTTR and added to the portable cleanroom after there was concern about contamination without one for personnel entry/exit. The scientific study of organics is critical for the mission, so a stringent contamination control plan was implemented for low organics. Given these mission requirements the cleanroom construction materials were carefully selected to not hinder the scientific search for amino acids and the study of organics in the samples. The same cleanroom contractor that built the long-term astromaterial curation cleanroom back at JSC Houston, TX was selected to build the portable cleanroom and instructed to use the same materials. The cleanroom had double doors to open and allow the sample return capsule to fit into the cleanroom on its stand and be transferred to a clean stand already in the cleanroom. The portable cleanroom successfully completed its mission and the sample canister was safely deintegrated and transported to JSC under nitrogen purge.

astromaterials curation↗

Portable Cleanroom for NASA OSIRIS-REx Mission Deintegration

NASA Johnson Space Center (JSC) Infrastructure and Astromaterials Acquisition & Curation Office completed construction and commissioning of the OSIRIS-REx (OREx) Deintegration portable cleanroom at the Utah Test and Training Range (UTTR). The new portable cleanroom was designed to receive the OREx sample return capsule from the landing point on the range to an ISO7 environment. Scientists used the portable clean-room to deintegrate the sample canister from the sample return capsule. Once separated, the sample canister was put in a container under nitrogen purge for transportation to B31 at the Johnson Space Center for astromaterial sample extraction, preliminary analysis, and long-term curation. The portable cleanroom was built by a subcontractor at their facility and then deconstructed to be transported to the remote location at UTTR. Since construction was completed in a remote location all tools and materials had to be transported from contractor site in Dallas, TX. The cleanroom was constructed within an existing facility, which provided conditioned air, electric power, and protection from the elements. Careful coordination was required between the host facility, cleanroom contractor, mission scientists, and JSC facilities and curation personnel. An existing anteroom at JSC was transported to UTTR and added to the portable cleanroom after there was concern about contamination without one for personnel entry/exit. The scientific study of organics is critical for the mission, so a stringent contamination control plan was implemented for low organics. Given these mission requirements the cleanroom construction materials were carefully selected to not hinder the scientific search for amino acids and the study of organics in the samples. The same cleanroom contractor that built the long-term astromaterial curation cleanroom back at JSC Houston, TX was selected to build the portable cleanroom and instructed to use the same materials. The cleanroom had double doors to open and allow the sample return capsule to fit into the cleanroom on its stand and be transferred to a clean stand already in the cleanroom. The portable cleanroom successfully completed its mission and the sample canister was safely deintegrated and transported to JSC under nitrogen purge.

astromaterials curation↗

Priority Science Targets for Future Sample Return Missions within the Solar System Out to the Year 2050

The Astromaterials Acquisition and Curation Office (henceforth referred to herein as NASA Curation Office) at NASA Johnson Space Center (JSC) is responsible for curating all of NASA's extraterrestrial samples. JSC presently curates 9 different astromaterials collections: (1) Apollo samples, (2) LUNA samples, (3) Antarctic meteorites, (4) Cosmic dust particles, (5) Microparticle Impact Collection [formerly called Space Exposed Hardware], (6) Genesis solar wind, (7) Star-dust comet Wild-2 particles, (8) Stardust interstellar particles, and (9) Hayabusa asteroid Itokawa particles. In addition, the next missions bringing carbonaceous asteroid samples to JSC are Hayabusa 2/ asteroid Ryugu and OSIRIS-Rex/ asteroid Bennu, in 2021 and 2023, respectively. The Hayabusa 2 samples are provided as part of an international agreement with JAXA. The NASA Curation Office plans for the requirements of future collections in an "Advanced Curation" program. Advanced Curation is tasked with developing procedures, technology, and data sets necessary for curating new types of collections as envisioned by NASA exploration goals. Here we review the science value and sample curation needs of some potential targets for sample return missions over the next 35 years.

McCubbin, F. M.↗

Adaptive Curation at NASA Johnson Space Center: Preparing for Artemis Samples by Leveraging Proven Practices and Innovative Solution

The proper curation of returned astromaterial samples is essential to ensure that high-quality scientific investigations can be conducted for decades, enabling future generations to address evolving research questions. The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (hereafter JSC Curation) is responsible for curating all of NASA’s extraterrestrial samples. Under the governing document, NASA Procedural Requirement (NPR) 7100.5 “Curation of Extraterrestrial Materials”, JSC Curation is charged with “The curation of all extraterrestrial material under NASA control, including future NASA missions.” The Directive goes on to define Curation as including “...documentation, preservation, preparation, and distribution of samples for research, education, and public outreach.” JSC Curation has a long-standing legacy of curating extraterrestrial materials, including but not limited to Apollo and Luna lunar samples, Genesis solar wind samples, Stardust comet samples, asteroid samples (Hayabusa1, Hayabusa2, and OSIRIS-REx), and Antarctic Meteorite samples from a variety of parent bodies. Building on this foundation, the Artemis program introduces new challenges and opportunities for sample curation, requiring both the application of proven practices and the development of innovative solutions. The Artemis Collection will be curated using established protocols refined through decades of experience with Apollo and subsequent sample collections, including but not limited to the utilization of cleanrooms, custom nitrogen gloveboxes, specialized storage containers and tools; all of which have strict material utilization and prohibition requirements. These practices provide a robust framework for contamination control, documentation, and long-term preservation. However, Artemis samples may present unique scientific and operational requirements, including enhanced contamination control measures (relative to Apollo) driven by evolving science objectives. To meet these needs, JSC Curation is actively developing new technologies and protocols that extend beyond traditional approaches, ensuring that the integrity of samples is maintained under increasingly stringent standards. One critical area of innovation is the development of cold sample curation capabilities. Certain Artemis samples, particularly those from Permanently Shadowed Regions (PSRs) and cold environments, are expected to contain ices and volatile components that require preservation and handling at sub-zero or even cryogenic temperatures. JSC Curation is leveraging best practices from the cold and cryogenic sample industries, as well as other government agencies and academic experts, to design facilities and handling procedures that maintain sample integrity while enabling scientific access. The goal is to develop capabilities to allow researchers to investigate volatiles and other temperature-sensitive materials while minimizing chemical and physical alterations from their returned state. In summary, adaptive curation at JSC combines the reliability of proven methodologies with forward-looking innovations to meet the scientific and operational demands of Artemis. Through enhanced contamination control, advanced cold curation capabilities, and an understanding of known and evolving future science priorities, NASA is preparing to maximize the scientific return from Artemis samples and preserve their value for generations of researchers.

Andrea D Harrington↗

Applicability and Utility of the Astromaterials X-Ray Computed Tomography Laboratory at Johnson Space Center

The Astromaterials Acquisition and Curation Office at NASA’s Johnson Space Center is responsible for curating all of NASA’s astromaterial sample collections (i.e. Apollo samples, Luna Samples, Antarctic Meteorites, Cosmic Dust Particles, Microparticle Impact Collection, Genesis solar wind atoms, Stardust comet Wild-2 particles, Stardust interstellar particles, and Hayabusa asteroid Itokawa particles) [1-3]. To assist in sample curation and distribution, JSC Curation has recently installed an X-ray computed tomography (XCT) scanner to visualize and characterize samples in 3D. [3] describes the instrumental set-up and the utility of XCT to astromaterials curation. Here we describe some of the current and future projects and illustrate the usefulness of XCT in studying astromaterials.

Eckley, S. A.↗

JSC Advanced Curation: Research and Development for Current Collections and Future Sample Return Mission Demands

Curation of NASA's astromaterials sample collections is a demanding and evolving activity that supports valuable science from NASA missions for generations, long after the samples are returned to Earth. For example, NASA continues to loan hundreds of Apollo program samples to investigators every year and those samples are often analyzed using instruments that did not exist at the time of the Apollo missions themselves. The samples are curated in a manner that minimizes overall contamination, enabling clean, new high-sensitivity measurements and new science results over 40 years after their return to Earth. As our exploration of the Solar System progresses, upcoming and future NASA sample return missions will return new samples with stringent contamination control, sample environmental control, and Planetary Protection requirements. Therefore, an essential element of a healthy astromaterials curation program is a research and development (R&D) effort that characterizes and employs new technologies to maintain current collections and enable new missions - an Advanced Curation effort. JSC's Astromaterials Acquisition & Curation Office is continually performing Advanced Curation research, identifying and defining knowledge gaps about research, development, and validation/verification topics that are critical to support current and future NASA astromaterials sample collections. The following are highlighted knowledge gaps and research opportunities.

Fries, M. D.↗

The Acquisition, Containment, and Curation of Mars Samples on Earth

The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (henceforth AACO) is responsible for receiving and curating all of NASA’s extraterrestrial samples, current and future (as per NASA Policy Directive (NPD) 7100.10E “Curation of Extraterrestrial Materials”). As such, the AACO coordinates sample capture, containment, and transportation to the curation facility as well as documents, preserves, prepares, and distributes all of the samples within NASA’s astromaterial collections for research, education, and public outreach. Since the lunar rock and soil samples returned during the Apollo Program, NASA’s first Class V Restricted Earth Return Missions, the AACO curates six other astromaterials collections. Lessons learned from each collection and respective missions (e.g. Apollo, Genesis, Stardust) as well as advancements in science and technology have informed the AACO’s plan for acquiring and curating Martian samples. Given the nature of the collection, a mobile and modular facility is recommended. The two broad requirements a Mars sample facility must maintain are: 1) the ability to contain the samples to protect the public from exposure of an “unknown unknown” biological agent and 2) ensure the scientific integrity of the samples are maintained (while maximizing scientific outcome). Although Apollo samples were eventually deemed safe and released to the scientific community for evaluation, there is no guarantee that this will be the case for Martian samples. Therefore, the facility in which the samples will be contained and investigated must be modular and able to accommodate an array of instrumentation that could be highly variable depending on the initial scientific outcomes. Furthermore, in order to facilitate proper sample capture and containment upon landing as well as sample distribution to other laboratories with proper containment, a mobile facility is a valuable investment.

Harrington, Andrea D.↗

Fungal Exposure to Meteorite Thin Sections: Developing an Experimental to Observe Biogeochemical Changes

The Astromaterials Acquisition & Curation Office maintains collections of meteorite samples collected as part of the Antarctic Search for Meteorites (ANSMET) program. The chief goal of the curation department is to maintain these meteorites in pristine condition. The Astromaterials Research and Exploration Science (ARES) Directorate has implemented a microbial monitoring program for the meteorite collections that has resulted in the isolation of >100 fungal isolates [1], however it is currently unknown if these isolates could present danger to the collections through bioweathering or secretion of organic compounds. We grew a strain of Fusarium oxysporium isolated from nitrogen gas filters feeding the Meteorite Lab nitrogen gas in the presence of a H5 meteorite thin section to determine if this fungus has the capability of altering the mineral structure of this common meteorite. This first trial was to determine and understand the effects of Fusarium oxysporum growth on the iron content within H5 chondrites and evaluate what additional components are needed in the development of future trial runs. This experiment determined new considerations for handling samples, the nature of microscopic scans before and after the incubation period, and the quality of the samples utilized for the experiment. The results of this experiment were promising and warrant further investigation with a more refined process and timeline.

Barbre, K. S. R.↗

ARES Biennial Report 2012 Final

Since the return of the first lunar samples, what is now the Astromaterials Research and Exploration Science (ARES) Directorate has had curatorial responsibility for all NASA-held extraterrestrial materials. Originating during the Apollo Program (1960s), this capability at Johnson Space Center (JSC) included scientists who were responsible for the science planning and training of astronauts for lunar surface activities as well as experts in the analysis and preservation of the precious returned samples. Today, ARES conducts research in basic and applied space and planetary science, and its scientific staff represents a broad diversity of expertise in the physical sciences (physics, chemistry, geology, astronomy), mathematics, and engineering organized into three offices (figure 1): Astromaterials Research (KR), Astromaterials Acquisition and Curation (KT), and Human Exploration Science (KX). Scientists within the Astromaterials Acquisition and Curation Office preserve, protect, document, and distribute samples of the current astromaterials collections. Since the return of the first lunar samples, ARES has been assigned curatorial responsibility for all NASA-held extraterrestrial materials (Apollo lunar samples, Antarctic meteorites - some of which have been confirmed to have originated on the Moon and on Mars - cosmic dust, solar wind samples, comet and interstellar dust particles, and space-exposed hardware). The responsibilities of curation consist not only of the longterm care of the samples, but also the support and planning for future sample collection missions and research and technology to enable new sample types. Curation provides the foundation for research into the samples. The Lunar Sample Facility and other curation clean rooms, the data center, laboratories, and associated instrumentation are unique NASA resources that, together with our staff's fundamental understanding of the entire collection, provide a service to the external research community, which relies on access to the samples. The curation efforts are greatly enhanced by a strong group of planetary scientists who conduct peerreviewed astromaterials research. Astromaterials Research Office scientists conduct peer-reviewed research as Principal or Co-Investigators in planetary science (e. g., cosmochemistry, origins of solar systems, Mars fundamental research, planetary geology and geophysics) and participate as Co-Investigators or Participating Scientists in many of NASA's robotic planetary missions. Since the last report, ARES has achieved several noteworthy milestones, some of which are documented in detail in the sections that follow. Within the Human Exploration Science Office, ARES is a world leader in orbital debris research, modeling and monitoring the debris environment, designing debris shielding, and developing policy to control and mitigate the orbital debris population. ARES has aggressively pursued refinements in knowledge of the debris environment and the hazard it presents to spacecraft. Additionally, the ARES Image Science and Analysis Group has been recognized as world class as a result of the high quality of near-real-time analysis of ascent and on-orbit inspection imagery to identify debris shedding, anomalies, and associated potential damage during Space Shuttle missions. ARES Earth scientists manage and continuously update the database of astronaut photography that is predominantly from Shuttle and ISS missions, but also includes the results of 40 years of human spaceflight. The Crew Earth Observations Web site (http://eol.jsc.nasa.gov/Education/ESS/crew.htm) continues to receive several million hits per month. ARES scientists are also influencing decisions in the development of the next generation of human and robotic spacecraft and missions through laboratory tests on the optical qualities of materials for windows, micrometeoroid/orbital debris shielding technology, and analog activities to assess surface science operations. ARES serves as host to numerous students and visiting scientists as part of the services provided to the research community and conducts a robust education and outreach program. ARES scientists are recognized nationally and internationally by virtue of their success in publishing in peer-reviewed journals and winning competitive research proposals. ARES scientists have won every major award presented by the Meteoritical Society, including the Leonard Medal, the most prestigious award in planetary science and cosmochemistry; the Barringer Medal, recognizing outstanding work in the field of impact cratering; the Nier Prize for outstanding research by a young scientist; and several recipients of the Nininger Meteorite Award. One of our scientists received the Department of Defense (DoD) Joint Meritorious Civilian Service Award (the highest civilian honor given by the DoD). ARES has established numerous partnerships with other NASA Centers, universities, and national laboratories. ARES scientists serve as journal editors, members of advisory panels and review committees, and society officers, and several scientists have been elected as Fellows in their professional societies. This biennial report summarizes a subset of the accomplishments made by each of the ARES offices and highlights participation in ongoing human and robotic missions, development of new missions, and planning for future human and robotic exploration of the solar system beyond low Earth orbit.

Stansbery, Eileen↗

The Importance of Contamination Knowledge in Curation - Insights into Mars Sample Return

The Astromaterials Acquisition and Curation Office at NASA Johnson Space Center (JSC), in Houston, TX (henceforth Curation Office) manages the curation of extraterrestrial samples returned by NASA missions and shared collections from international partners, preserving their integrity for future scientific study while providing the samples to the international community in a fair and unbiased way. The Curation Office also curates flight and non-flight reference materials and other materials from spacecraft assembly (e.g., lubricants, paints and gases) of sample return missions that would have the potential to cross-contaminate a present or future NASA astromaterials collection.

Harrington, A. D.↗

Lunar Processing Cabinet 2.0: Retrofitting Gloveboxes into the 21st Century

In 2014, the Apollo 16 Lunar Processing Glovebox (cabinet 38) in the Lunar Curation Laboratory at NASA JSC received an upgrade including new technology interfaces. A Jacobs - Technology Innovation Project provided the primary resources to retrofit this glovebox into the 21st century. NASA Astromaterials Acquisition & Curation Office continues the over 40 year heritage of preserving lunar materials for future scientific studies in state-of-the-art facilities. This enhancement has not only modernized the contamination controls, but provides new innovative tools for processing and characterizing lunar samples as well as supports real-time exchange of sample images and information with the scientific community throughout the world.

Calaway, M. J.↗

Using X-Ray Computed Tomography as a Tool for Preliminary Examination Tool of Current and Future Extraterrestrial Sample Return Missions

The Astromaterials Acquisition and Curation Office at the Johnson Space Center is the past, present, and future home of all of NASA’s astromaterials sample collections. The primary goals of the curation office are to maintain the long-term integrity of the samples and ensure that the samples are distributed for scientific study in a fair, timely, and responsible manner, thus maximizing the return on each sample. Part of the curation process is planning for the future. To this end, we perform fundamental research in advanced curation initiatives to better prepared for future sample return missions. Advanced Curation is tasked with developing procedures, technology, and data sets necessary for curating new sample collections, or getting new results from existing sample collections. As part of these advanced curation efforts, we have installed and are operating a Nikon XTH 320 X-ray Computed Tomography(XCT) system in the JSC curation office with four interchangeable X-ray sources, a large-area detector, and a heavy-duty stage. These instrument characteristics allow us exceptional flexibility to analyze a wide range of sample sizes, from sub-mm soil particles to rocks >10 cm in diameter. The penetrative nature of the XCT scans allows for astromaterials samples to be analyzed within sealed low-density containers (e.g., Teflon bags), preserving the pristinity of the samples. We have begun scanning of the Apollo and Antarctic Meteorite sample suites in order to non-destructively map out lithic clasts (and other features) within the samples. The data from these scans will be made available to scientists via the JSC curation website and the Astromaterials Curation Newsletter. We anticipate sample requests from these “new” lithic clasts identified in these “old” samples. We also anticipate that XCT analyses like these would be useful for future sample return missions, like the OSIRIS REx mission, as well as future sample return missions.

Zeigler, Ryan↗

Planning Related to the Curation and Processing of Returned Martian Samples

The Astromaterials Acquisition and Curation Office (henceforth referred to herein as NASA Curation Office) at NASA Johnson Space Center (JSC) is responsible for curating all of NASA’s extraterrestrial samples. Under the governing document, NASA Policy Directive (NPD) 7100.10E “Curation of Extraterrestrial Materials”, JSC is charged with “the curation of all extraterrestrial material under NASA control, including future NASA missions.” The Directive goes on to define Curation as including “…documentation, preservation, preparation, and distribution of samples for research, education, and public outreach.” Here we describe some of the ongoing planning efforts in curation as they pertain to the return of martian samples in a future, as of yet unplanned, mission.

McCubbin, Francis M.↗

The NASA OSIRIS-REx Sample Catalog: Samples Returned from Investigators

OSIRIS-REx is a sample return mission that collected carbon-rich material from B-type asteroid Bennu. After landing on September 24th, 2023, the science canister was transported to NASA Johnson Space Center (JSC) in Houston, Texas where it was opened and samples were processed by the curation team in pristine sample nitrogen gloveboxes. As the sample analysis phase of the OSIRIS-REx mission concludes, the Sample Analysis Team (SAT) has returned the majority of mission samples to NASA JSC curation and will return the remaining samples on a defined timetable. The curation team processed and documented as many of these samples as possible to include in the spring 2026 catalog update and are steadily working to process hundreds of more samples to include in the fall 2026 catalog update.

OSIRIS-REx↗