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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 127 records · Page 7
All sourcesNASA NTRSDOE OSTI
NASA NTRS1994

Qualification test results for blue-red reflecting solar covers

Recent market forces and design innovations have spurred the development of solar cell covers that significantly reduce the solar absorptance for a cell array. GaAs cells, using Ge as the substrate host material, can have a significantly higher output if the solar absorptance of the cell array is reduced. New optical coating design techniques have allowed the construction of covers that reflect the ultraviolet energy (below 350 nm) and the near infrared energy (above 900 nm) resulting in the beneficial reduction in absorptance. Recent modeling suggests three or more present output increase due to the lowered temperature with such a device. Within the last several months we have completed the testing of production samples of these new covers in a qualification series that included the usual environmental effects associated with the routine testing of solar cell covers and the combined effects of protons, electrons and solar UV as would be encountered in space. For the combined effects testing the samples were exposed to 300 sun days equivalent UV, 5 x 10(exp 14)/sq cm of 0.5 MeV protons and 10(exp 15)/sq cm of 1.0 MeV electrons. Measurements of the reflectance, transmission, emittance and other appropriate parameters were made before and after the testing. As measured by the averaged transmission over the cell operating band, the change in transmission for the samples was less than or about equal to 1 percent. The details of the testing and the results in terms of transmission, reflectance and emittance are discussed in the paper.

Beauchamp, W. T.↗
NASA NTRS1998

Ceramic Fairings for A Hypersonic Flight Experiment

Fairings composed of Rigid Fibrous Insulations (RSI) were fabricated, instrumented, and coated using techniques that were recently developed at NASA Ames Research Center. These RSI components are part of a specific assembly of materials which were built onto a wing of a Pegasus flight vehicle. The assembly was designed to collect aerothermal data during a designated mission to deliver a satellite to earth orbit. The objective of the flight experiment is to validate the theory of boundary layer transition at flight speeds in excess of Mach 3. The actual flight experiment is scheduled to occur during the summer of 1998. Fabrication and installation methodologies will be discussed with a brief description of the wing glove assembly.

Churchward, Rex↗
NASA NTRS2019

Application and Development of Atomic Layer Deposition Techniques to Improve Thermo-Optical Coatings for Spacecraft Thermal Control and Advanced Optical Instruments

A key technology development driver in environmental control systems and next generation optics are discussed utilizing thin film development borrowed from the semiconductor industry. The optical and physical properties of spacecraft radiator coatings are dictated by orbital environmental conditions. For example, coatings must adequately dissipate charge buildup when orbital conditions, such as polar, geostationary or gravity neutral, result in surface charging. Current dissipation techniques include depositing a layer of ITO (indium tin oxide) on the radiator surface in a high temperature process. The application of these enhanced coatings must be such that the properties in question are tailored to mission-specific requirements. The multi-billion-dollar semiconductor industry has adopted Atomic Layer Deposition (ALD) for self-assembly and atomic-scale placement. ALD is a cost-effective nanoadditive-manufacturing technique that allows for the conformal coating of substrates with atomic control in a benign temperature and pressure environment. By using ALD, modification of these coatings can be accomplished during coating application preprocessing. The preprocessing is rendered directly on the coating dry pigment before binding. Through the introduction of paired precursor gases, thin films can be deposited on a myriad of substrates ranging from glass, polymers, aerogels, metals, powders, and other high aspect-ratio micro- and nano- structures. By providing atomic-level control, where single layers of atoms can be deposited, the fabrication of metal transparent films, precise nano-laminates, and coatings of nano-channels and pores is achievable. A method has been demonstrated for the ALD of In2O3 and films on a variety of substrates from Si(100) wafers, glass slides, and on Z93P pigments resulting in a direct spaceflight application. Results will be presented that verify the chemical composition of ALD pigments and charge dissipation properties when the pigment goes through its binding and coating process and we present early results of ALD for carbon nanotube formation and encapsulation.

Dwivedi, Vivek H.↗
NASA NTRS1981

Processing modifications for improved propellants - Coated oxidizers

The present investigation is concerned with a technique which makes it possible to improve greatly the performance of composite propellants by alleviating the combustion instability problem. The technique involves the coating of the oxidizer crystals (typically ammonium perchlorate) with a suitably selected chemical. For each application the chemical for the coating is chosen on the basis of a screening procedure including the employment of differential scanning calorimetry and the use of a thermogravimetric analyzer. It is particularly important that the coat chemicals have good thermochemical stability at temperatures up to the normal surface temperature of the propellant during time-independent combustion (typically 800 to 900 K). At higher temperatures, sudden degradation should occur over a vary narrow temperature range (10-20 C).

Helmy, A. K.↗
NASA NTRS1994

Emittance characterization of thermal control paints, coatings and surfaces using a calorimetric technique

Thermal control surfaces are used in every spacecraft thermal management system to dissipate heat through radiant heat transfer. This paper describes the thermal performance of several thermal control paints, coatings, and surfaces, as characterized by a calorimetric vacuum emissometer. The emissometer is designed to measure the functional emittance of a surface based on heat transfer from an underlying substrate to the surface and from the surface or near surface to a surrounding cold wall. Emittance measurements were made between 200 and 350 K. Polished aluminum, used here as a standard, was found to have a total hemispherical emittance of 0.06, as expected. A velvet black paint, also used here as a standard, was found to have an emittance of 0.94 at room temperature. Other surfaces of interest included a polyurethane-based black paint designated Z-306, a highly polished 316L stainless steel, and an atomic oxygen beam-textured carbon-carbon composite.

Jaworske, Donald A.↗
NASA NTRS2003

Development of Advanced Thermal and Environmental Barrier Coatings Using a High-Heat-Flux Testing Approach

The development of low conductivity, robust thermal and environmental barrier coatings requires advanced testing techniques that can accurately and effectively evaluate coating thermal conductivity and cyclic resistance at very high surface temperatures (up to 1700 C) under large thermal gradients. In this study, a laser high-heat-flux test approach is established for evaluating advanced low conductivity, high temperature capability thermal and environmental barrier coatings under the NASA Ultra Efficient Engine Technology (UEET) program. The test approach emphasizes the real-time monitoring and assessment of the coating thermal conductivity, which initially rises under the steady-state high temperature thermal gradient test due to coating sintering, and later drops under the cyclic thermal gradient test due to coating cracking/delamination. The coating system is then evaluated based on damage accumulation and failure after the combined steady-state and cyclic thermal gradient tests. The lattice and radiation thermal conductivity of advanced ceramic coatings can also be evaluated using laser heat-flux techniques. The external radiation resistance of the coating is assessed based on the measured specimen temperature response under a laser- heated intense radiation-flux source. The coating internal radiation contribution is investigated based on the measured apparent coating conductivity increases with the coating surface test temperature under large thermal gradient test conditions. Since an increased radiation contribution is observed at these very high surface test temperatures, by varying the laser heat-flux and coating average test temperature, the complex relation between the lattice and radiation conductivity as a function of surface and interface test temperature may be derived.

Zhu, Dongming↗
NASA NTRS1985

SEM visualization of glycosylated surface molecules using lectin-coated microspheres

There are several techniques currently used to localize glycosylated surface molecules by scanning electron microscopy (Grinnell, 1980; Molday, 1976; Linthicum and Sell, 1975; Nicolson, 1974; Lo Buglio, et al, 1972). A simple and rapid method, using a modification of Grinnell's technique is reported here. Essentially, microspheres coated with Concavalin A are used to bind to glycosylated regions of the palatal shelf epithelium and are visualized in the scanning electron microscope (SEM).

Non-NASA Center↗
NASA NTRS1985

High time service evaluation of thermal barrier coatings on the Rolls-Royce RB211 engine

One of the main concerns of airline operators for the use of thermal barrier coatings (TBC) in the turbine is that the coating will spall and cause a premature engine removal. Even though much cyclic data is available on TBCs, high time data is much harder and expensive to come by. The typical 150 h type test used to qualify hardware, or modifications, falls far short of the 5 to 10,000 hour experience desired. One way to obtain data demonstrating the longevity of TBCs is through a service evaluation program on a commercial engine. For a meaningful evaluation of the TBC system it must be applied to a component which operates in a typical hot end environment. In addition the component performance should not suffer if the coating is lost. For these reasons Rolls-Royce chose to coat the IP turbine nozzle guide vanes, and run these in an RB211 engine. Two ceramic top coats and several different bond coats were tested in a rainbow fashion on several engines. Three layer magnesium zirconate was used as a base line. Various yttria stabilized zirconia ceramics were used. Top MCrAlY bond coats were applied by various techniques. Some of the coated vanes have now accumulated ofer 5000 hours. The results are presented from the first sets with 2500 and 4200 hours of service respectively.

Toriz, F. Chris↗
NASA NTRS1986

Detecting Pores in SiC Coatings

Liquid-penetrant/fluorescence technique reveals cracks and pinholes in protective coatings. Developed for checking quality of overcoatings on silicon carbide layers on advanced carbon/carbon substrates. Technique similar to other liquid-penetrant/fluorescence techniques used to make pores visible. Porous areas absorb more suspension and therefore accumulate more fluorescent particles. They fluoresce more brightly than their surroundings.

Hamilton, A. B.↗
NASA NTRS1971

Induction plasma calcining of pigment particles for thermal control coatings

Induction plasma heating techniques were studied for calcining zinc orthotitanate particles for use in thermal control coatings. Previous studies indicated that the optimum calcining temperature is between 1400 and 1750 C. An intermediate temperature (1670 C) was chosen as a reference point for running a temperature series at the reference point and 220 C on both sides. The effect of varying chamber temperature on the reflectance spectra, before and after vacuum UV irradiation, is presented. The correlation between Zn2Ti04 paramagnetic resonance activity and its susceptibility to vacuum UV damage is discussed.

Farley, E. P.↗
NASA NTRS1984

Mechanical property measurements of plasma-sprayed thermal-barrier coatings subjected to oxidation

Techniques have been developed for measuring the tensile properties of plasma-sprayed coatings which are used in thermal barrier applications. The measurements have included the average Young's modulus, bond strength and elongation at failure. The oxidation behavior of the bond coat plays an important role in the integrity and adhesion of plasma-sprayed thermal barrier coatings. This work studies the nature of the high temperature degradation on the mechanical properties of the coating. Furnace tests have been carried out on U-700 alloy with bond coats of NiCrAlY or NiCrAlZr and an overlay of ZrO2-8 percent Y2O3. Weight gain measurements on the coatings have been examined with relation to the adhesion strength and failure observations. The results from an initial study are reported in this work.

Berndt, C. C.↗
NASA NTRS1970

Simple bonding technique for high-temperature ceramic coatings

Coatings, consisting of zirconia powder bonded with orthophosphoric acid and a small amount of hydrofluoric acid, are hard, strong, and refractory, resist thermal shock, and provide good thermal protection. After the aqueous coating is applied to a metallic surface, only a 600 deg F cure is required before service.

Accountius, O. E.↗
NASA NTRS1980

Continuous coating of silicon-on-ceramic

Growth of sheet silicon on low-cost substrates has been demonstrated by the silicon coating with inverted meniscus (SCIM) technique. A mullite-based ceramic substrate is coated with carbon and then passed over a trough of molten silicon with a raised meniscus. Solidification occurs at the trailing edge of the downstream meniscus, producing a silicon-on-ceramic (SOC) layer. Meniscus shape and stability are controlled by varying the level of molten silicon in a reservoir connected to the trough. The thermal conditions for growth and the crystallographic texture of the SOC layers are similar to those produced by dip-coating, the original technique of meniscus-controlled growth. The thermal conditions for growth have been analyzed in some detail. The analysis correctly predicts the velocity-thickness relationship and the liquid-solid interface shape for dip-coating, and appears to be equally applicable to SCIM-coating. Solar cells made from dip-coated SOC material have demonstrated efficiencies of 10% on 4-sq cm cells and 9.9% on 10-sq cm cells.

Heaps, J. D.↗
NASA NTRS2008

Thermal Barrier and Protective Coatings to Improve the Durability of a Combustor Under a Pulse Detonation Engine Environment

Pulse detonation engine (PDE) concepts are receiving increasing attention for future aeronautic propulsion applications, due to their potential thermodynamic cycle efficiency and higher thrust to density ratio that lead to the decrease in fuel consumption. But the resulting high gas temperature and pressure fluctuation distributions at high frequency generated with every detonation are viewed to be detrimental to the combustor liner material. Experimental studies on a typical metal combustion material exposed to a laser simulated pulse heating showed extensive surface cracking. Coating of the combustor materials with low thermal conductivity ceramics is shown to protect the metal substrate, reduce the thermal stresses, and hence increase the durability of the PDE combustor liner material. Furthermore, the temperature fluctuation and depth of penetration is observed to decrease with increasing the detonation frequency. A crack propagation rate in the coating is deduced by monitoring the variation of the coating apparent thermal conductivity with time that can be utilized as a health monitoring technique for the coating system under a rapid fluctuating heat flux.

Ghosn, Louis J.↗