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Sources of soft X-rays uses alpha particles to fluoresce light elements such as boron, carbon, and magnesium. X-ray wavelengths are varied by changing target. Technique supplies broad range of monoenergetic X-rays whose energy can be adjusted very easily.
This paper reviews and discusses future directions in analytical electron microscopy for microchemical analysis using X-ray and Electron Energy Loss Spectroscopy (EELS). The technique of X-ray microanalysis, using the ratio method and k(sub AB) factors, is outlined. The X-ray absorption correction is the major barrier to the objective of obtaining I% accuracy and precision in analysis. Spatial resolution and Minimum Detectability Limits (MDL) are considered with present limitations of spatial resolution in the 2 to 3 microns range and of MDL in the 0.1 to 0.2 wt. % range when a Field Emission Gun (FEG) system is used. Future directions of X-ray analysis include improvement in X-ray spatial resolution to the I to 2 microns range and MDL as low as 0.01 wt. %. With these improvements the detection of single atoms in the analysis volume will be possible. Other future improvements include the use of clean room techniques for thin specimen preparation, quantification available at the I% accuracy and precision level with light element analysis quantification available at better than the 10% accuracy and precision level, the incorporation of a compact wavelength dispersive spectrometer to improve X-ray spectral resolution, light element analysis and MDL, and instrument improvements including source stability, on-line probe current measurements, stage stability, and computerized stage control. The paper reviews the EELS technique, recognizing that it has been slow to develop and still remains firmly in research laboratories rather than in applications laboratories. Consideration of microanalysis with core-loss edges is given along with a discussion of the limitations such as specimen thickness. Spatial resolution and MDL are considered, recognizing that single atom detection is already possible. Plasmon loss analysis is discussed as well as fine structure analysis. New techniques for energy-loss imaging are also summarized. Future directions in the EELS technique will be the development of new spectrometers and improvements in thin specimen preparation. The microanalysis technique needs to be simplified and software developed so that the EELS technique approaches the relative simplicity of the X-ray technique. Finally, one can expect major improvements in EELS imaging as data storage and processing improvements occur.
The UW CMa is a close, eclipsing binary composed of an O7f primary with a stron wind and a less luminous O-type companion. It was found that UW CMa a variable X-ray source, whose X-ray variations are in phase with its optical light curve. Since both components of the binary system are O stars, accretion by a compact object is ruled out as a mechanism for generating X-rays. The UW CMa represents a new class of X-ray binaries, in which X-rays result from the collision of a wind from one star with the surface or wind of the other star. It is hypothesised that the impact of a wind against a star generates a shock wave about 0.25 stellar radii above the stellar surface, and material behind the shock front, heated to bout 10 million degrees, radiates the X-ray apparent X-ray variability is due to its location between the two stars, where it undergoes eclipses. The high temperature region maintains an ionization cavity in the wind, as detected with IUE. The ionization cavity is the source of depletion of absorbing ions in the wind between the two stars.
The Analytical Electron Microscope (AEM) equipped with a wavelength-dispersive spectrometer (WDS) should have the ability to resolve peaks which normally overlap in the spectra from an energy-dispersive spectrometer (EDS). With a WDS it should also be possible to measure lower concentrations of elements in thin foils due to the increased peak-to-background ratio compared with EDS. The WDS will measure X-ray from the light elements (4 less than Z less than 1O) more effectively. This paper addresses the possibility of interfacing a compact WDS with a focussing circle of approximately 4 cm to a modem AEM with a high-brightness (field emission) source of electrons.
The interaction of alpha particles with matter is employed in a compact instrument that could provide rather complete in-situ chemical analyses of surfaces and thin atmospheres of extraterrestrial bodies. The instrument is a miniaturized and improved version of the Surveyor lunar instrument. The backscattering of alpha particles and (alpha, p) reactions provide analytical data on the light elements (carbon-iron). An X-ray mode that detects the photons produced by the alpha sources provides sensitivity and resolution for the chemical elements heavier than about silicon. The X-rays are detected by semiconductor detectors having a resolution between 150 and 250 eV at 5.9 keV. Such an instrument can identify and determine with good accuracy 99 percent of the atoms (except hydrogen) in rocks. For many trace elements, the detecting sensitivity is a few ppm. Auxiliary sources could be used to enhance the sensitivities for elements of special interest. The instrument could probably withstand the acceleration involved in semi-hard landings.
New UBVRI photometry of Mrk 421 obtained during periods of X-ray satellite observations are presented. An X-ray light curve for 1977 November from the HEAO A-1 experiment is also given. The decomposition of the UBVR fluxes into a compact nonthermal component and an extended galactic component shows that there are coordinated variations in the optical nonthermal and X-ray emission. The data are consistent with the hypothesis that the mini-BL Lac object is emitting by the synchrontron-self-Compton process. The host galaxy of this composite source has properties like those of a giant elliptical.
Fluorescence-mode X-ray absorption spectroscopy (XAS) at high photon energies requires detectors with high stopping power and excellent energy resolution to measure weak element-specific signals. Traditional silicon-based detectors suffer from poor efficiency above ∼20 keV, while most high-Z materials such as cadmium telluride, cadmium zinc telluride, and gallium arsenide have focused predominantly on imaging applications with limited spectroscopic resolution. In contrast, germanium combines excellent stopping power with superior intrinsic energy resolution due to its low Fano factor and favorable charge transport properties, making it ideal for high-resolution spectroscopy in the 15 keV to 100 keV range. To address these requirements, we report on the development, fabrication, and performance evaluation of Gepta-EX, a compact multi-channel high-purity germanium (HPGe) detector system for fluorescence-mode XAS. The Gepta-EX system features a monolithic seven-channel HPGe pixel array integrated with low-noise CUBE charge-sensitive preamplifiers, housed within a thermally isolated compact cryostat operating near 90 K. The detector achieves energy resolutions of 218 eV at 5.9 keV (from a 55 Fe source) and 373 eV at 59.5 keV (from a 241 Am source), with uniform performance across all channels. By avoiding the escape peak interference commonly associated with silicon detectors and providing stable, high-resolution performance, Gepta-EX represents a powerful tool for high-energy X-ray spectroscopy.
The orbital inclination of the Cyg XR-1/HDE 226868 system was determined by Dolan and Tapia (1989) to be 62 deg (+5 deg, -37 deg) from polarimetric observations. Together with the spectroscopic mass function of the binary, this corresponds to a mass of 6.3 solar masses for the X-ray source. Numerical simulations show that there is no straightforward way to removing tidal deformation polarization (TDP) from polarimetric observations of close binaries. A reanalysis of the data shows that the existence of TDP in the Stokes parameter light curves observed from Cyg XR-1 does not significantly bias the mass derived to larger values. The mass of Cyg XR-1 must be significantly larger than 5 solar masses. This fact alone does not require Cyg XR-1 to be a black hole, however. Recent theoretical investigations of possible equations of state of matter at nuclear density show that the maximum mass of a compact object which is not a black hole may be much greater than 5 solar masses.
Eighteen X-ray light curves of the 104-sec periodicity in the Taurus X-ray nova A 0535+26 are analyzed which were obtained by SAS-3 in six energy intervals between 1 and 35 keV during the period from May 30 to June 2, 1975. It is shown that the pulse structure is relatively simple at energies above 19 keV, but develops a complex series of five irregularly spaced maxima at lower energies. The energy spectrum averaged over the 104-sec period is found to be extremely hard, with a best-fit temperature of about 30 keV for the exponential spectrum, an excess at about 15 keV, and a steepening above 20 keV. It is suggested that A 0535+26 may be a compact object in a binary system containing the peculiar Be star HDE 245770. The transient behavior could arise due to episodic mass loss by the primary or because the compact object is in a highly eccentric orbit about the companion, with appreciable mass transfer occurring only at periastron.
A new theoretical treatment of the evolution of highly compact binary systems is presented. The evolution is calculated until almost the entire mass of the secondary has been transferred to the primary or lost from the system. It is assumed that gravitational radiation from the system is the cause of mass transfer. It is found that the structure of the mass-losing star can be approximated by an n = 3/2 polytrope, and as a result a relatively large number of different cases can be explored and some general conclusions drawn. An explanation is found for the existence of a cutoff in the orbital period distribution among the cataclysmic variables and light is shed upon the possible generic relationships among cataclysmic variables, the low-mass X-ray binaries, and the spectrally soft transient X-ray sources.
Sixteen Einstein X-ray sources in the field of the Large Magellanic Cloud (LMC) that appear non-extended in the IPC detector have recently been accurately positioned with the HRI to make optical follow-up studies feasible. At least twelve of these are not associated with the LMC, including one Seyfert galaxy at a redshift of 0.076 and eleven late type galactic foreground stars, some showing photometric behavior typical for RS CVn and BY Dra variables. Two sources are identified with faint blue variable objects, one of them has been observed to exhibit He II 4686 and variable Balmer emission lines being reminiscent of the low mass X-ray binary LMC X-2. The IPC source 1E0501438-7037.6 is probably associated with the LMC OB star Sk-70 36 which has been found to show ellipsoidal light variations with a period of 6.94 d. The results strongly suggest that a gap in the X-ray binary luminosity function of the LMC exists between 10 to the 36th and 10 to the 38th ergls.
High-quality and prebunched electron beams can produce coherent x-rays with high intensity and narrow bandwidth, which are essential for modern light sources. An all-optical scheme based on plasma-based acceleration for producing bright electron beams that are prebunched on the nanometer scale is proposed. By using a density modulation created by two low intensity counterpropagating lasers, the phase velocity of the plasma wake excited by an intense driver laser in a uniform plasma can be modulated at a frequency twice that of the colliding lasers, thus turning the injection on and off. The injected electrons are microbunched at the Doppler-shifted modulated wavelength, corresponding to the phase velocity of the gradually expanding wakefield. It is demonstrated that by controlling the properties of the drive and colliding lasers, beams with exotic prebunched structures can be produced, which may have critical applications in ultrafast high power x-rays. This extremely compact, all-optical scheme for producing ultrabright prebunched electron beams may therefore enable novel applications for ultrafast x-ray users and arouse general interest in various fields.
High-energy particle colliders and X-ray free-electron lasers demand electron beams with qualities currently achieved only in kilometer-scale radio-frequency accelerators. Plasma accelerators promise a compact alternative but have faced challenges in delivering the needed beam quality at relevant energies. Here, we demonstrate that a plasma-wakefield accelerator operating in the nonlinear regime acts as a transformer to simultaneously boost the energy and brightness of an electron bunch injected from the plasma. Using a 10-GeV drive bunch and a three-stage meter-scale plasma source, we generated electron bunches exceeding 20 GeV with sub-percent energy spread, 2 mm·mrad normalized emittance, and multi-kA peak current. A significant number of drive-bunch electrons lost over 90% of their energy, a prerequisite for high energy-conversion efficiency. This demonstration of an energy transformer ratio exceeding two and a brightness enhancement over an order of magnitude opens a path towards cost-effective accelerators for future colliders and light sources.
Modern synchrotron x-ray beamlines demand reflective optics with higher surface profile accuracy to achieve diffraction-limited focusing. This necessitates advanced metrology instruments capable of delivering repeatable measurements in the nanometer to sub-nanometer range. Slope ranges exceeding 15 mrad (0.86°) and greater pose significant challenges for mirror metrology using conventional interferometric methods. Here, to address this, we present a new relative angle determinable stitching interferometry instrument featuring a parallel flexure-based mechanical design. This approach enhances vibration and thermal stability while maintaining a compact and lightweight system. Initial measurements of a cylindrical mirror with a 16 m radius of curvature and a slope range of 5 mrad demonstrate nanometer-level repeatability. Comprehensive system characterization suggests the potential for achieving sub-nanometer repeatability with further refinement to the instrument.
Recent advances in laboratory X-ray applications require high-performance optical components that achieve exceptional imaging resolution and beam uniformity within compact experimental setups. Montel mirrors have become a preferred solution due to their unique dual-reflection focusing mechanism and a space-efficient design. Here, in this study, we present an effective manufacturing process for producing Montel mirrors tailored to focus laboratory X-ray beams. The mirrors were fabricated from single-crystal silicon substrates, chosen for their high mechanical stability and compatibility with precision polishing techniques. Our approach begins with the integration of a deterministic chemo-mechanical polishing (CMP)-based pre-shaping step followed by ion beam figuring (IBF), significantly improving manufacturing efficiency. Subsequently, our custom-developed advanced metrology and IBF techniques were employed for fabricating an off-axis, elliptical cylinder Montel mirror system with a 6-mrad total slope, with stringent optical specifications. While post-IBF processes, including multilayer coating, dicing, and gluing, introduced minor surface errors, yet their impact on performance remained negligible. The Montel mirrors manufactured with the optimized process exhibited significantly improved beam uniformity and a reduced focal spot size. These findings validate our approach as a viable solution for high-precision Montel mirror fabrication and facilitate further advancements in laboratory X-ray applications.
In the present article, we provide compelling evidence that minor (1 wt%) additions of micron and nanometre-sized LiF particles in MgO decompose leading to free Li diffusing into MgO surfaces enhancing vacancy production during direct current sintering. The addition of nanometre-sized LiF particles leads to a > 500 °C reduction in the sintering temperature and over 99 % theoretical density of final consolidated compacts. Correlating differential scanning calorimetry with in-situ x-ray diffraction, together with Schottky calculations, post sintering electron microscopy and laser induced breakdown spectroscopy, we uncover critical insights into this impressive reduction in sintering temperature. Our quantitative analysis reveals that MgO and LiF interact at low temperatures with the diffusion of Li into the surface of MgO particles due to the intrinsic structural disorder of the LiF and MgO crystallites. Nanometre-sized LiF particles were found to react the most at low temperatures due to their increased structural disorder. Our multimodal characterization points to a Li-promoted densification and sintering mechanism. This impressive reduction in sintering temperature can be harnessed to promote low-temperature fabrication of MgO-based composites for technological applications.
The chemical interactions in Fe–HfH 2 metal matrix composites (MMCs) are studied across multiple length scales to elucidate the decomposition of the parent phases and corresponding reaction zone physics during direct current sintering. Fe–HfH 2 composites were synthesized with increasing as-mixed hydride contents of Fe–25% HfH 2 , Fe–40% HfH 2 , Fe–55% HfH 2 , and Fe–70% HfH 2 (all in vol. %) to demonstrate the ability to achieve sintered MMCs with target hydride contents. Samples were probed across multiple length scales through a multi-modal workflow employing x-ray diffraction, scanning electron microscopy and segmentation analysis, and synchrotron techniques including hard x-ray fluorescence mapping and nanoprobe x-ray absorption near-edge structure measurements. Under the selected sintering temperature and pressure conditions, hydrogen evolution is seen to evolve through parallel paths: thermal decomposition from during the transformation of HfH 2 to HfH x<2 and through subsequent reaction with the Fe matrix leading to intermetallic phase formation. Specifically, HfFe and HfFe 2 intermetallic formation accelerates the release of hydrogen with a subsequent HfO 2 phase forming at grain boundaries. For this MMC, the consumption or loss of hydrogen can be considerable in compacts with initial hydride loading of 25%–40% HfH 2 approaching 83% hydrogen loss for the lower volume fraction composites. Increasing the volume fraction of HfH 2 to 70% enhanced the retained hydrogen content to 53% and attributed to the reduced interfacial area intrinsic to the increased HfH 2 loading in this MMC.
The infrared emission data, obtained on 260 binary systems by the all-sky IRAS survey in wavelengths between 12 and 100 microns, are reported. Of all the 260 sources, which contained compact objects including white dwarfs, neutron stars, or possibly black holes, only 32 contained detectable IR radiation. The X-ray emitting Be-type stars (gamma-Cas and X Per) were found to have their energy flux proportional to frequency in the range of the log nu values of 12.7-14.7. However, the GS304-1 flux distribution is unique, in that its flux rises by several orders of magnitude as the wavelength changes from 4000 A to 60 microns. A static dust cloud was detected, with a radius of about 1 AU, which has formed around the classical nova RR Pic since its 1925 eruption. The post-eruption far-IR light curve of a classical nova provides strong evidence for IR emissions from both dust grains formed during the eruption and dust grains existing from previous eruptions.