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At least 739 records · Page 41

Development of techniques for advanced optical contamination measurement with internal reflection spectroscopy, phase 2, volume 2

Attenuated total reflectance spectra of individual contaminants in space simulation chambers are presented as well as spectra of mixtures and figures exhibiting the effects of film thickness on reflectance spectra. Detailed calibration spectra were made for three selected concentrations (film thickness) for two contaminants and for one concentration for all contaminants.

Hayes, J. D.↗

Determination of contamination character of materials in space technology testing

The contamination characters of selected materials used in space technology testing. Specific materials were subjected to a thermal vacuum environment, and the outgases were collected on a cold test mirror surface. Approximately one-half of the surface of the mirror was subjected to ultraviolet irradiation while the outgases were being deposited on the mirror. The purpose of these experiments was to determine the effect of ultraviolet irradiation on the contaminative character of outgases from selected materials. The degree of contamination was measured in terms of degradation of the optical properties of the test mirror and the amount of deposit per unit area on quartz crystal microbalances placed near the test mirror, and by means of quadrupole mass spectral measurements of outgases from the test samples.

Haynes, D. L.↗

Exhaust plume and contamination characteristics of a bipropellant (MMH/N2O4) RCS thruster

Results are presented for three recent tests in a series of thruster contamination experiments made in liquid helium-cooled environmental facility. The contaminating effects encountered on various materials, surfaces, and components, due to the exhaust products from a 5-pound thrust, bipropellant (MMH/N2O4) thruster are investigated. The angular distribution of plume effects around the periphery of the thruster established by transmittance changes of quartz samples over the wavelength range from 0.2 to 2.0 micrometer is studied, along with mass deposition rates at a specific location measured with a quartz crystal microbalance for three different experiments. Quadrupole mass spectrometer measurements of the exhaust products over the mass number range from 12 to 75; infrared transmittance measurements of contaminated samples for the wavelength range from 2.5 to 15 microns; and infrared transmittance measurements of residue from the thruster nozzle are also considered.

Spisz, E. W.↗

Determination of molecular contamination performance for space chamber tests

The limitations of chamber tests with regard to the molecular contamination of a spacecraft undergoing vacuum test were examined. The molecular flow conditions existing in the chamber and the parameters dictating the degree of contamination were analyzed. Equations and graphs were developed to show the fraction of molecules returning to the spacecraft out of those emitted and to show other chamber flow parameters as a function of chamber and spacecraft surface molecular pumping and geometric configuration. Type and location of instruments required to measure the outgassing, the degree of contamination, and the returning flows are also discussed.

Scialdone, J. J.↗

Evaluation of radioisotope tracer and activation analysis techniques for contamination monitoring in space environment simulation chambers

Radioisotope measurement techniques and neutron activation analysis are evaluated for use in identifying and locating contamination sources in space environment simulation chambers. The alpha range method allows the determination of total contaminant concentration in vapor state and condensate state. A Cf-252 neutron activation analysis system for detecting oils and greases tagged with stable elements is described. While neutron activation analysis of tagged contaminants offers specificity, an on-site system is extremely costly to implement and provides only marginal detection sensitivity under even the most favorable conditions.

Smathers, J. B.↗

The V-3 contamination test of the chamber A facility and a subsequent cryogenic/vacuum study of the V-3 test quartz crystal microbalance

The areas of orbital and ground contamination of flight experiment hardware have been well established. This report relates directly to results of vacuum chamber testing for the ground evaluation of flight experiment hardware performance. First, the data obtained during the V-3 contamination testing in the Johnson Space Center's Chamber A space simulation test facility are presented. Second, during the V-3 contamination tests, the MSFC Space Sciences Laboratory's quartz crystal microbalance exhibited two periods of anomalous readings. Therefore, a subsequent small chamber tests was conducted in a controlled cryogenic/vacuum environment. The objective was to reproduce with known parameters the anomalous behavior patterns of the V-3 test data. Analyses of the anomalous readings are made on the basis of these tests. Additionally, as a by-product of the small chamber tests, calibration curves then existing for the quartz crystal microbalance were empirically extended, and certain data-formatting aids were documented.

Moore, W. W., Jr.↗

Active cleaning techniques for removing contamination from optical surfaces in space

Research in developing an active cleaning technique for removing contaminants from optical surfaces in space is reported. In situ contamination/cleaning experiments were conducted on gold and platimum coated mirrors, which were contaminated by exposure to UV radiation in a 1,3, butadiene environment. Argon and oxygen plasma exposure cleaned the mirrors equally well. Silicone cleaning experiments were also conducted. Exposure of the contaminated mirrors to helium, oxygen, and hydrogen plasmas restored the reflectance at the shorter wavelengths and degraded it at the longer wavelengths.

Shannon, R. L.↗

Contamination assessment and control in scientific satellites

Techniques for assessment and control of the contamination environment for both particulates and condensible vapors in the vicinity of spacecraft are developed. An analysis of the deposition rate on critical surfaces is made considering sources within the line of sight of the surface in question as well as those obscured from the line of sight. The amount of contamination returned by collision with the surrounding atmosphere is estimated. Scattering and absorption from the induced atmosphere of gases and particulates around the spacecraft are estimated. Finally, design techniques developed for Skylab to reduce the contamination environment to an acceptable level are discussed.

Naumann, R. J.↗

Terrestrial contamination in Apollo lunar samples.

The contamination prevention procedures adopted for controlling the collection, processing, and analysis of the Apollo lunar samples in order to keep them free of significant levels of terrestrial organic matter are described. The organic contaminants actually found in the samples by the various investigators are summarized. It is shown that the program succeeded in providing investigators with samples containing less than 0.1 ppm total contamination.

Flory, D. A.↗

SMEAT atmosphere trace contaminants.

The atmosphere trace contaminant analysis support provided for the Skylab Medical Experiments Altitude Test (SMEAT) which was conducted from July 26 through September 20, 1972, at the JSC Crew Systems Division facility is discussed. Sample acquisition techniques and analytical instrumentation methodology utilized for identification and quantification of the trace contaminants are described. Emphasis is placed on the contaminants found, their occurrence patterns, and possible sources.

Schornick, J. L.↗

Active cleaning technique for removing contamination from optical surfaces in space

An active cleaning technique for removing contaminants from optical surfaces in space was investigated with emphasis on the feasibility of using plasma exposure as a means of in-situ cleaning. The major work accomplished includes: (1) development of an in-situ reflectometer for use in conjunction with the contaminant film deposition/cleaning facility; (2) completion of Apollo Telescope Mount (ATM) filter treatment experiments to assess the effects of plasma exposure on the UV transmittance; (3) attempts to correlate the atomic oxygen flux with cleaning rate; (4) completion of in-situ butadien contamination/plasma cleaning/UV reflectance measurement experiments; (5) carbon cleaning experiments using various gases; (6) completion of silicone contamination/cleaning experiments; and (7) experiments conducted at low chamber pressures to determine cleaning rate distribution and contamination of surfaces adjacent to those being cleaned.

Shannon, R. L.↗

Effects of low-pressure air on oxygen contamination and lithium corrosion of a tantalum alloy, T-111, at 980 and 1260 C

The effects were studied of low-pressure air on contamination and corrosion in the tantalum alloy T-111/lithium system at 980 and 1260 C. Capsules of T-111 containing lithium were exposed to six vacuum levels between 1 x 10 to the 8th power and 0.0003 torr by controlled air leakage into a vacuum system. Capsules exposed at 980 C and 0.0002 torr failed from intragranular oxidation. The remainder of the capsules completed the 96-hour tests. The depth of oxygen contamination was greater at 980 C than at 1260 C. Tests made at 0.0001 and 0.00001 torr levels caused large increases in the oxygen content of the T-111. Tests at 0.000001 torr or less produced no significant contamination. No lithium corrosion of the T-111 was observed under any of the conditions.

Gahn, R. F.↗

Assessment of the probability of contaminating Mars

New methodology is proposed to assess the probability that the planet Mars will by biologically contaminated by terrestrial microorganisms aboard a spacecraft. Present NASA methods are based on the Sagan-Coleman formula, which states that the probability of contamination is the product of the expected microbial release and a probability of growth. The proposed new methodology extends the Sagan-Coleman approach to permit utilization of detailed information on microbial characteristics, the lethality of release and transport mechanisms, and of other information about the Martian environment. Three different types of microbial release are distinguished in the model for assessing the probability of contamination. The number of viable microbes released by each mechanism depends on the bio-burden in various locations on the spacecraft and on whether the spacecraft landing is accomplished according to plan. For each of the three release mechanisms a probability of growth is computed, using a model for transport into an environment suited to microbial growth.

Judd, B. R.↗

Study to define points of entry for potential contaminants in limestone aquifers

Visual examinations of both prints and transparencies from ERTS 1 and U-2 aircraft imagery provided a method for discovering possible points of entry of potential contaminants into the limestone aquifer in Madison County, Alabama. Knowledge of the locations at which contaminants could enter the aquifer is an important consideration in water quality management, particularly for regions that depend, at least partially, on ground water for their water supply. ERTS 1 imagery recorded on December 28, 1972 in the Multispectral Scanner-5 (MSS-5) and MSS-7 bands, and a false-color composite of the MSS-4 (green), MSS-5 (red), and MSS-7 (near infrared) bands were the principal materials used, along with thermography recorded by an RS-7 infrared scanner onboard a U-2 aircraft. The results of the study are discussed in detail, providing information on prominent lineations and major fracture trends which are related to aquifer contamination. Maps depicting the observations are also presented.

Doyle, F. L.↗

Test evaluation of potential heatshield contamination of an outer planet probe's gas sampling system

The feasibility of retaining the heat shield for outer planet probes was investigated as a potential source of atmospheric sample contamination by outgassing. The onboard instruments which are affected by the concept are the pressure sensor, temperature sensor, IR detector, nephelometer, and gas sampling instruments. It was found that: (1) The retention of the charred heatshield and the baseline atmospheric sampling concepts are compatible with obtaining noncontaminated atmospheric samples. (2) Increasing the sampling tube length so that it extends beyond the viscous boundary layer eliminates contamination of the atmospheric sample. (3) The potential for contamination increases with angle of attack.

Kessler, W. C.↗

Analytical study of spacecraft deposition contamination by internal reflection spectroscopy

The in-situ vacuum chamber designed around the IRE was tested under vacuum. The contamination analyzer system was tested using two liquid contaminant materials. The analysis of the contaminants on the SL-4 rendezvous window shows that the material has methyl silicone, hydroxyl, and carbonyl radicals. The analysis of the outgassing material from Shuttle TPS shows silicone as the primary product.

Mookherji, T. K.↗

Evaluation and study of advanced optical contamination, deposition, measurement, and removal techniques

A program is described to design, fabricate and install an experimental work chamber assembly (WCA) to provide a wide range of experimental capability. The WCA incorporates several techniques for studying the kinetics of contaminant films and their effect on optical surfaces. It incorporates the capability for depositing both optical and contaminant films on temperature-controlled samples, and for in-situ measurements of the vacuum ultraviolet reflectance. Ellipsometer optics are mounted on the chamber for film thickness determinations, and other features include access ports for radiation sources and instrumentation. Several supporting studies were conducted to define specific chamber requirements, to determine the sensitivity of the measurement techniques to be incorporated in the chamber, and to establish procedures for handling samples prior to their installation in the chamber. A bibliography and literature survey of contamination-related articles is included.

Linford, R. M. F.↗

Value contamination avoidance devices

Mechanical redesign methods were used to minimize contamination damage of conventional fluid components and a contamination separator device was developed for long term reusable space vehicles. These were incorporated into an existing 50.8 mm poppet valve and tested for damage tolerance in a full size open loop flow system with gaseous and liquid nitrogen. Cyclic and steady flow conditions were tested with particles of 125 to 420 micrometers aluminum oxide dispersed in the test fluids. Nonflow life tests (100,000 cycles) were made with two valve configurations in gaseous hydrogen. The redesigned valve had an acceptable cycle life and improved tolerance to contamination damage when the primary sealing surfaces were coated with thin coatings of hard plastic (Teflon S and Kynar). Analytical studies and flow testing were completed of four different versions of the separator. overall separation efficiencies in the 55-90% range were measured with these non-optimum configurations.

Endicott, D. L.↗